CN104922929A - Natural medicine ultrasound continues extracting and concentrating device - Google Patents
Natural medicine ultrasound continues extracting and concentrating device Download PDFInfo
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- CN104922929A CN104922929A CN201510331354.9A CN201510331354A CN104922929A CN 104922929 A CN104922929 A CN 104922929A CN 201510331354 A CN201510331354 A CN 201510331354A CN 104922929 A CN104922929 A CN 104922929A
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Abstract
The invention relates to a natural medicine ultrasound continues extracting and concentrating device. The natural medicine ultrasound continues extracting and concentrating device comprises a medicine liquor extracting tank and further comprises a medicine liquor concentrating tank, a solvent condenser, a solvent recovery tank and a vacuum-pumping system; a heating jacket is installed outside the tank wall of the medicine liquor extracting tank, a water insulation box is installed in the heating jacket, two symmetrically-arranged ultrasonic wave vibrators are installed on the portions, outside the tank wall of the medicine liquor extracting tank, in the water insulation box, and the condenser is installed at the upper end of the medicine liquor extracting tank; the medicine liquor extracting tank is communicated with the medicine liquor extracting tank through a medicine liquor delivering pipe; the medicine liquor extracting tank is communicated with the solvent condenser through a solvent absorption pipe; the solvent condenser is connected with the solvent recovery tank through a solvent collecting pipe, and the solvent condenser is connected with the vacuum-pumping system. The natural medicine ultrasound continues extracting and concentrating device can be applied in industries including the pharmaceutical industry, the food processing industry and the chemical engineering separating industry, and the efficient production process of medicine multi-time extracting, continuous extracting and continuous concentrating under the condition that the solvent is entirely recycled is achieved; the production efficiency is improved, the manpower is saved, and the environment is avoided being polluted; the operability is strong, and the implementation is easy.
Description
Technical field
The invention belongs to drug ingedient extractive technique field, particularly relate to the ultrasonic continuous extraction enrichment facility of a kind of natural drug.
Background technology
At present, in the industries such as medicine, chemical industry and food, include technological improvement major part that effective constituent extracted and concentrated aspect just for each independent step, as accelerated extraction efficiency for extraction stage applied microwave, the means such as ultrasonic, the concentrated and Vacuum Concentration of the microwave proposed for enriching stage etc.; And domestic most of manufacturer is all that design manufactures separately separately for these two kinds of operations, be also separate operations, cause the significant wastage of extractant and material, and volatile extractant is easily to environment during operation.
Summary of the invention
The present invention is that to solve domestic most of manufacturer for these two kinds of operations be all that design manufactures separately separately, it is also concentrated during operation and extraction separate operations, cause the significant wastage of extractant and material, and volatile extractant easily provides a kind of structure natural drug that is simple, easy to install, that increase work efficiency ultrasonic continuous extraction enrichment facility to the technical problem of environment.
The technical scheme that the present invention takes for the technical problem existed in solution known technology is:
The ultrasonic continuous extraction enrichment facility of natural drug, comprises medicinal liquid extraction tank, also comprises concentration of liquid medicine tank, condenser for solvent, solvent recovery tank and pumped vacuum systems;
Described pumped vacuum systems comprises: reactor, vacuum pump and vacuum oil pump; The top cover of described reactor is provided with aspirating hole and vacuum meter; The aspirating hole of described reactor is connected with vacuum pipe, vacuum pipe is connected in parallel the bleeding point of vacuum pump and the bleeding point of vacuum oil pump; The bleeding point of described vacuum pump and the bleeding point of vacuum oil pump are all provided with valve;
Outside described medicinal liquid extraction tank tank skin, heating jacket is housed, described heating jacket is built with water proof box, and in described water proof box, outside described medicinal liquid extraction tank tank skin, symmetrically arranged two groups of ultrasonic oscillators are housed, condenser is equipped with in described medicinal liquid extraction tank upper end; Described medicinal liquid extraction tank is communicated with described concentration of liquid medicine tank by liquid carrier pipe; Described concentration of liquid medicine tank draws closed tube by solvent and is communicated with described condenser for solvent; Described condenser for solvent is connected with solvent recovery tank by solvent collection pipe, and described condenser for solvent is connected with described pumped vacuum systems; Described solvent recovery tank is connected with described medicinal liquid extraction tank by solvent delivery pipe, and described solvent delivery pipe is provided with valve; Described concentration of liquid medicine tank connects product storage tank, and described product storage tank is positioned at below described concentration of liquid medicine tank; The outlet of described liquid carrier pipe is located in described concentration of liquid medicine tank tank, and medical liquid atomizing shower nozzle is installed in the outlet of described liquid carrier pipe; Outside described concentration of liquid medicine tank, concentration tank heating jacket is housed.
Further, the medicine liquid outlet of described medicinal liquid extraction tank is located at lower end, and described medicine liquid outlet is provided with filter screen, and described medicine liquid outlet is communicated with described concentration of liquid medicine tank by described liquid carrier pipe.
Further, described liquid carrier pipe is equipped with liquid delivery pump.
Further, described liquid carrier pipe is provided with electric heating cover.
Further, be provided with charge pump and tank stocked by solvent, described charge pump import is stocked tank through the first charge pipe with described solvent and is connected, and described charge pump outlet is connected with solvent recovery tank through the second charge pipe, and described solvent recovery tank is connected with described solvent tank through solvent recovery pipe.
Further, described first charge pipe is provided with the first threeway, described second charge pipe is provided with the second threeway, 3rd interface of described first threeway is connected by described solvent recovery pipe with the 3rd interface of described second threeway, the first interface of described first threeway and described solvent are stocked between tank and the first stop valve are housed, and between the first interface of described second threeway and described reinforced delivery side of pump, the second stop valve are housed.
Further, described pumped vacuum systems also comprises control system; Described vacuum meter is digital vacuum meter; Valve on the bleeding point of vacuum pump and the bleeding point of vacuum oil pump is all automatic valve;
The data signal input of the data signal output connection control system of numeral vacuum meter; The control signal output of control system connects the control signal input of the automatic valve on the bleeding point of vacuum pump and the bleeding point of vacuum oil pump respectively; The control signal output of control system also connects vacuum pump respectively and vacuum oil pump opens/stop control signal input.
The advantage that the present invention has and good effect are:
Compared with prior art, have the following advantages:
1, ultrasound-enhanced extraction and vacuum being strengthened concentrated two kinds of technical relations to get up to organically combine, realizing material from extracting concentrated continuous process, reach extraction, concentrated effect of carrying out continuously.Can as required to material to be extracted carry out one or many from extracting concentrated continuous process, and do not waste unnecessary solvent, save step and solvent; Realize repeatedly extracting medicine when solvent reclaims completely, continuously the High-efficient Production process of extraction, continuous concentration;
2, due to the application of two kinds of reinforcement techniques, apparatus of the present invention are significantly being increased for medicine and other gross efficiency extracting concentration process; Two unit operations are simply merged into a unit operations, realize the repeatedly extraction to medicine when solvent reclaims completely, in actual production, both improve production efficiency, saved manpower, turn avoid contaminated environment;
3, flow process of the present invention is easily understood, and equipment cost is low, is convenient to production practices.Device structure is simple, simple to operate, easy to implement.
The present invention had both been applicable to single-trial extraction, concentration process, was applicable to again repeatedly extraction, concentration process.The present invention can not only be widely used in the processing of pharmaceutical industry medicine, can also be applied to the industry such as food processing, chemical separating, realize the continuous extraction of effective ingredient in natural material, the High-efficient Production process of continuous concentration.
Accompanying drawing explanation
Fig. 1 is the ultrasonic continuous extraction enrichment facility structural representation of natural drug that the embodiment of the present invention provides;
In figure: 1, medicinal liquid extraction tank; 2, ultrasonic oscillator; 3, heating jacket; 4, material inlet; 5, condenser; 6, dregs of a decoction outlet; 7, filter screen; 8, liquid delivery pump; 9, vacuum system; 10, solvent recovery tank; 11, condenser for solvent; 12, medical liquid atomizing shower nozzle; 13, concentration of liquid medicine tank; 14, concentration tank heating jacket; 15, liquid carrier pipe electric heating cover; 16, product storage tank; 17, valve; 18, return valve; 19, liquid carrier pipe; 20, solvent draws closed tube, and 21, solvent collection pipe; 22, water proof box; 23, solvent delivery pipe; 24, tank stocked by solvent; 25, charge pump; 26, the first charge pipe; 27, the second charge pipe; 28, solvent recovery pipe; 29, the first threeway; 30, the second threeway; 31, the first stop valve; 32, the second stop valve.
Detailed description of the invention
For summary of the invention of the present invention, Characteristic can be understood further, hereby exemplify following examples, and coordinate accompanying drawing to be described in detail as follows.
As shown in Figure 1: the ultrasonic continuous extraction enrichment facility of a kind of natural drug, comprise the medicinal liquid extraction tank 1 being provided with material inlet 4 and dregs of a decoction outlet 6, it also comprises concentration of liquid medicine tank 13, condenser for solvent 11, solvent recovery tank 10 and pumped vacuum systems 9; Outside medicinal liquid extraction tank 1 tank skin, heating jacket 3 is housed, can heats it as medium with steam or conduction oil; Heating jacket 3, built with water proof box 22, is equipped with symmetrically arranged two groups of ultrasonic oscillators 2 outside water proof box 22 inner liquid medicine extractor 1 tank skin; Condenser 5 is equipped with in medicinal liquid extraction tank 1 upper end, allows the solvent volatilized in leaching process entirely reclaim; Recovered solvent can be put back in medicinal liquid extraction tank and again extract, and also can be used as recycling design and stores; The medicine liquid outlet of medicinal liquid extraction tank 1 is located at lower end, and medicine liquid outlet is provided with filter screen 7, the dregs of a decoction can be filtered, and obtains pure extract; Medicine liquid outlet is communicated with concentration of liquid medicine tank 13 by liquid carrier pipe 19; Liquid carrier pipe 19 is equipped with liquid delivery pump 8; Concentration of liquid medicine tank 13 draws closed tube 20 by solvent and is communicated with condenser for solvent 11; Condenser for solvent 11 is connected with solvent recovery tank 10 by solvent collection pipe 21, and condenser for solvent 11 is connected with pumped vacuum systems 9; Concentration of liquid medicine tank 13 connects product storage tank 16, and product storage tank 16 is positioned at below concentration of liquid medicine tank 13, utilizes gravity directly to collect concentrated medicament.
Described pumped vacuum systems 9 comprises: reactor, vacuum pump and vacuum oil pump; The top cover of described reactor is provided with aspirating hole and vacuum meter; The aspirating hole of described reactor is connected with vacuum pipe, vacuum pipe is connected in parallel the bleeding point of vacuum pump and the bleeding point of vacuum oil pump; The bleeding point of described vacuum pump and the bleeding point of vacuum oil pump are all provided with valve;
Described pumped vacuum systems 9 also comprises control system; Described vacuum meter is digital vacuum meter; Valve on the bleeding point of vacuum pump and the bleeding point of vacuum oil pump is all automatic valve;
The data signal input of the data signal output connection control system of numeral vacuum meter; The control signal output of control system connects the control signal input of the automatic valve on the bleeding point of vacuum pump and the bleeding point of vacuum oil pump respectively; The control signal output of control system also connects vacuum pump respectively and vacuum oil pump opens/stop control signal input.
As of the present invention perfect, solvent recovery tank 10 is connected with medicinal liquid extraction tank 1 by solvent delivery pipe 23, and establishes valve 17 on solvent delivery pipe 23; Recovered solvent imports in medicinal liquid extraction tank by Open valve, avoids and directly adds the injury of solvent due to solvent volatilization to human body.And on solvent collection pipe 21, return valve 18 is installed, for the amount regulating recycling design to enter medicinal liquid extraction tank.
The outlet of liquid carrier pipe 19 is located in concentration of liquid medicine tank 13 tank, and as of the present invention perfect further, medical liquid atomizing shower nozzle 12 is installed in the outlet of liquid carrier pipe 19, and concentration of liquid medicine tank carries out atomization process to the liquid that need concentrate, favourable concentrated.
Concentration tank heating jacket 14 is housed outside concentration of liquid medicine tank 13, as medium, it is heated with steam or conduction oil, be beneficial to acceleration concentration of liquid medicine further.
Perfect as a more step of the present invention, liquid carrier pipe 19 is provided with electric heating cover 15; To the medicine liquid heating entering concentration of liquid medicine tank 13, be conducive to improving concentrated speed and efficiency.
The course of work of the present invention is roughly as follows: add medicinal liquid extraction tank 1 by the drug powder of pulverizing from material inlet 4; Open valve 17, the solvent being stored in solvent recovery tank 10 li is added medicinal liquid extraction tank 1; Open vacuum system 9 to vacuumize to device; Open heating jacket 3 to medicinal liquid extraction tank heating, open ultrasonic oscillator 2 power supply and carry out ultrasound-enhanced extraction; Through the regular hour, open liquid delivery pump 8, liquid is carried; Open electric heating cover 15 to heat to the liquid in pipe, liquid carries out atomization process through medical liquid atomizing shower nozzle 12 after filter screen 7 filters in concentration of liquid medicine tank 13; The solvent volatilization of low melting point enters into condenser for solvent 11, condensed solvent enters solvent recovery tank 10, close vacuum system, make solvent enter medicinal liquid extraction tank 1 to continue to extract medicament effective component, repeatedly extract if do not need, return valve 18 can cut out, make solvent enter solvent recovery tank 10 and store, the medicament effective component of phase counterweight, in concentration of liquid medicine tank 13 bottom deposition, finally enters product storage tank 16.
The above is only to preferred embodiment of the present invention, not any pro forma restriction is done to the present invention, every according to technical spirit of the present invention to any simple modification made for any of the above embodiments, equivalent variations and modification, all belong in the scope of technical solution of the present invention.
Claims (7)
1. the ultrasonic continuous extraction enrichment facility of natural drug, comprises medicinal liquid extraction tank, it is characterized in that, also comprise concentration of liquid medicine tank, condenser for solvent, solvent recovery tank and pumped vacuum systems;
Described pumped vacuum systems comprises: reactor, vacuum pump and vacuum oil pump; The top cover of described reactor is provided with aspirating hole and vacuum meter; The aspirating hole of described reactor is connected with vacuum pipe, vacuum pipe is connected in parallel the bleeding point of vacuum pump and the bleeding point of vacuum oil pump; The bleeding point of described vacuum pump and the bleeding point of vacuum oil pump are all provided with valve;
Outside described medicinal liquid extraction tank tank skin, heating jacket is housed, described heating jacket is built with water proof box, and in described water proof box, outside described medicinal liquid extraction tank tank skin, symmetrically arranged two groups of ultrasonic oscillators are housed, condenser is equipped with in described medicinal liquid extraction tank upper end; Described medicinal liquid extraction tank is communicated with described concentration of liquid medicine tank by liquid carrier pipe; Described concentration of liquid medicine tank draws closed tube by solvent and is communicated with described condenser for solvent; Described condenser for solvent is connected with solvent recovery tank by solvent collection pipe, and described condenser for solvent is connected with described pumped vacuum systems; Described solvent recovery tank is connected with described medicinal liquid extraction tank by solvent delivery pipe, and described solvent delivery pipe is provided with valve; Described concentration of liquid medicine tank connects product storage tank, and described product storage tank is positioned at below described concentration of liquid medicine tank; The outlet of described liquid carrier pipe is located in described concentration of liquid medicine tank tank, and medical liquid atomizing shower nozzle is installed in the outlet of described liquid carrier pipe; Outside described concentration of liquid medicine tank, concentration tank heating jacket is housed.
2. the ultrasonic continuous extraction enrichment facility of natural drug according to claim 1, it is characterized in that, the medicine liquid outlet of described medicinal liquid extraction tank is located at lower end, and described medicine liquid outlet is provided with filter screen, and described medicine liquid outlet is communicated with described concentration of liquid medicine tank by described liquid carrier pipe.
3. the ultrasonic continuous extraction enrichment facility of natural drug according to claim 1, it is characterized in that, described liquid carrier pipe is equipped with liquid delivery pump.
4. the ultrasonic continuous extraction enrichment facility of natural drug according to claim 1, it is characterized in that, described liquid carrier pipe is provided with electric heating cover.
5. the ultrasonic continuous extraction enrichment facility of the natural drug according to Claims 1-4 any one, it is characterized in that, be provided with charge pump and tank stocked by solvent, described charge pump import is stocked tank through the first charge pipe with described solvent and is connected, described charge pump outlet is connected with solvent recovery tank through the second charge pipe, and described solvent recovery tank is connected with described solvent tank through solvent recovery pipe.
6. the ultrasonic continuous extraction enrichment facility of natural drug according to claim 5, it is characterized in that, described first charge pipe is provided with the first threeway, described second charge pipe is provided with the second threeway, 3rd interface of described first threeway is connected by described solvent recovery pipe with the 3rd interface of described second threeway, the first interface of described first threeway and described solvent are stocked between tank and the first stop valve are housed, and between the first interface of described second threeway and described reinforced delivery side of pump, the second stop valve are housed.
7. the ultrasonic continuous extraction enrichment facility of natural drug according to claim 1, it is characterized in that, described pumped vacuum systems also comprises control system; Described vacuum meter is digital vacuum meter; Valve on the bleeding point of vacuum pump and the bleeding point of vacuum oil pump is all automatic valve;
The data signal input of the data signal output connection control system of numeral vacuum meter; The control signal output of control system connects the control signal input of the automatic valve on the bleeding point of vacuum pump and the bleeding point of vacuum oil pump respectively; The control signal output of control system also connects vacuum pump respectively and vacuum oil pump opens/stop control signal input.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510331354.9A CN104922929A (en) | 2015-06-15 | 2015-06-15 | Natural medicine ultrasound continues extracting and concentrating device |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510331354.9A CN104922929A (en) | 2015-06-15 | 2015-06-15 | Natural medicine ultrasound continues extracting and concentrating device |
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| CN104922929A true CN104922929A (en) | 2015-09-23 |
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| CN201510331354.9A Pending CN104922929A (en) | 2015-06-15 | 2015-06-15 | Natural medicine ultrasound continues extracting and concentrating device |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105920872A (en) * | 2016-06-13 | 2016-09-07 | 宜春学院 | Natural drug ultrasonic continuous extraction and concentration device |
| CN106179123A (en) * | 2016-08-30 | 2016-12-07 | 无锡东恒新能源科技有限公司 | A kind of organic solvent extraction mechanism with vacuum extractor |
| CN108325235A (en) * | 2018-03-08 | 2018-07-27 | 陕西理工大学 | A kind of Chinese herbal medicine effective ingredients extraction filtering integrating device and method |
| CN109865304A (en) * | 2017-12-01 | 2019-06-11 | 田高 | The extraction process and extraction element of more substances in a kind of solution |
| CN112245961A (en) * | 2020-09-12 | 2021-01-22 | 临泉县清华地产中药材有限责任公司 | Extraction element of chinese-medicinal material |
| CN112717545A (en) * | 2020-12-09 | 2021-04-30 | 李高平 | Chinese medicinal material solution extraction processing device and Chinese patent medicine preparation method |
| CN113730932A (en) * | 2021-08-06 | 2021-12-03 | 北京东华原医疗设备有限责任公司 | Liquid medicine concentration device and liquid medicine concentration control method |
| CN114832405A (en) * | 2021-02-01 | 2022-08-02 | 朴然熙 | Electric concentration extraction device capable of quickly extracting and concentrating |
-
2015
- 2015-06-15 CN CN201510331354.9A patent/CN104922929A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105920872A (en) * | 2016-06-13 | 2016-09-07 | 宜春学院 | Natural drug ultrasonic continuous extraction and concentration device |
| CN106179123A (en) * | 2016-08-30 | 2016-12-07 | 无锡东恒新能源科技有限公司 | A kind of organic solvent extraction mechanism with vacuum extractor |
| CN109865304A (en) * | 2017-12-01 | 2019-06-11 | 田高 | The extraction process and extraction element of more substances in a kind of solution |
| CN108325235A (en) * | 2018-03-08 | 2018-07-27 | 陕西理工大学 | A kind of Chinese herbal medicine effective ingredients extraction filtering integrating device and method |
| CN112245961A (en) * | 2020-09-12 | 2021-01-22 | 临泉县清华地产中药材有限责任公司 | Extraction element of chinese-medicinal material |
| CN112717545A (en) * | 2020-12-09 | 2021-04-30 | 李高平 | Chinese medicinal material solution extraction processing device and Chinese patent medicine preparation method |
| CN112717545B (en) * | 2020-12-09 | 2022-07-29 | 江尔成 | Chinese medicinal material solution extraction processing device and Chinese patent medicine preparation method |
| CN114832405A (en) * | 2021-02-01 | 2022-08-02 | 朴然熙 | Electric concentration extraction device capable of quickly extracting and concentrating |
| CN114832405B (en) * | 2021-02-01 | 2024-01-05 | 朴然熙 | Electric concentrating and extracting device capable of fast extracting and concentrating |
| CN113730932A (en) * | 2021-08-06 | 2021-12-03 | 北京东华原医疗设备有限责任公司 | Liquid medicine concentration device and liquid medicine concentration control method |
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Application publication date: 20150923 |
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