CN104920492A - Low-volume spray containing eucalyptol - Google Patents
Low-volume spray containing eucalyptol Download PDFInfo
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- CN104920492A CN104920492A CN201510321322.0A CN201510321322A CN104920492A CN 104920492 A CN104920492 A CN 104920492A CN 201510321322 A CN201510321322 A CN 201510321322A CN 104920492 A CN104920492 A CN 104920492A
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- water
- spray
- eucalyptol
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- tea saponin
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention relates to a pesticide, in particular to a low-volume spray containing eucalyptol. The spray comprises, by mass, 5%-30% of eucalyptol, 5%-15% of tea saponin and the balance of water. In the preparation process, the water and the tea saponin are added into a mixing kettle to be evenly mixed, then the eucalyptol is added to be sufficiently dispersed into the mixed liquor of the water and the tea saponin, grinding is performed through a sand mill, sampling is performed, and after the sample is detected to be qualified, filling and packaging are performed. The water and the tea saponin serve as a carrier, so that the spray is safe to human and livestock, not likely to generate phytotoxicity to crops and environmentally friendly. The formula is simple and the water serves as the carrier, so that the cost is low, and the performance-cost ratio is high. The water consumption for diluting the spray is small, so that the spray is especially suitable for spraying in arid areas and water-deficient high mountain areas. The spray can be used for low-volume or ultra-low-volume spraying and has higher working efficiency compared with full-coverage spraying, so that the labor cost is lowered. The dripping loss of spray liquid is small, so that the pesticide utilization ratio is high, and environmental pollution is reduced.
Description
Technical field
The present invention relates to agricultural chemicals, especially relate to a kind of low-gallonage spraying agent containing eucalyptol.
Background technology
The medical treatment of diseases and pests of agronomic crop and sanitary insect pest, spray-on process is modal application method, is namely made into liquid with a certain amount of agricultural chemicals and appropriate water or oil, with spraying apparatus, medicine liquid spray is become droplet.By every mu of (667cm
2) number of spray liquid amount, spray-on process is often divided into conventional spray, low volume and ultra low volume spray.
1, conventional spray, agricultural chemicals dilutes with water, and extension rate is greater than 1000 times, every mu of (667cm
2) spouting liquid at 45 ~ 60L, be the conventional spray-on process in present stage China's plant protection field.This spray-on process spray amount is large, and work efficiency is not high, and liquid drippage runs off serious, and agricultural chemicals availability is less than 30%.
2, low volume, agricultural chemicals dilutes with water or oil, extension rate about 100 times, every mu of (667cm
2) spray liquid amount 2.6 ~ 10L, be called low volume.This spray-on process, spray amount is lower, and work efficiency is 5 ~ 10 times of conventional spray.Agricultural chemicals runs off few, and availability can reach more than 60%.
3, ultra low volume spray, agricultural chemicals with water or oil dilution, extension rate lower than 10 times, every mu of (667cm
2) spouting liquid is 0.5 ~ 2.5L, be called ultra low volume spray, spray amount is very low, and work efficiency is 10 ~ 50 times of conventional spray, and agricultural chemicals runs off seldom, and availability can reach more than 80%.
The control of China's plant protection field crop disease and insect, at present still based on conventional spray.Because its droplet is large, target produces spring, drippage runs off serious, and agricultural chemicals availability is not high, to environment, also can make that agricultural product agriculture is residual to exceed standard; Again because its spray amount is large, spraying work efficiency is low, and cost of labor is also high; Conventional spray agent dilute with water multiple is greater than 1000 times, and water consumption is large, is unfavorable for that arid and high mountain water-deficient area use.
It is worth mentioning that, conventional spray agent with dimethylbenzene etc. to the organic solvent of human body and bad environmental and petrochemical industry class surfactant for carrier, safety and the feature of environmental protection are all bad, all can produce harm to human body and crop, can not in order to low amounts and ultra low volume spray; For realizing the accurate high-efficiency prevention and control of diseases and pests of agronomic crop, reducing agricultural chemicals and running off, reducing the pollution to environment and agricultural product, improving agricultural chemicals availability, improve spraying work efficiency, the agent of research and development low-gallonage spraying, very necessary.
Chinese patent CN102626116A discloses vegetative insecticide and preparation method thereof, each component and constituent mass percentage are: eucalyptol mother liquor 1-30%, emulsifier 5-20%, surplus are absolute ethyl alcohol, and preparation method comprises the following steps: the preparation of eucalyptol mother liquor and mixture.This invention is on the basis of a large amount of lab screening, to determine with blue gum proportioning, with Chinese herbal medicines such as rhizoma atractylodis for primary raw material, to extract and be processed into mother liquor, add the auxiliary agent such as emulsifier and absolute ethyl alcohol.
Obviously, existing medicament all adopts traditional organic solvent usually, all there is potential safety hazard, can not be used for the low-gallonage spraying of high-load liquid to human body, plant, environment etc.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of low-gallonage spraying agent containing eucalyptol is provided.
The present invention's raw material by mass percentage consists of: eucalyptol 5% ~ 30%, Tea Saponin 5% ~ 15%, and surplus is water.
The present invention's raw material composition is by mass percentage preferably: eucalyptol 5% ~ 20%, Tea Saponin 10% ~ 15%, surplus is water.
During use, with low-capacity atomizer spraying, dilute with water 1 ~ 100 times, for low amounts and ultra low volume spray, the medicine liquid spray amount 1 ~ 10L of every mu, for the control of plant pest and the dissipation of sanitary insect pest.
During preparation, water and Tea Saponin are added compounding kettle and mixes, then add eucalyptol, be well-dispersed in water and Tea Saponin mixed liquor, then with sand mill grinding, sample detection qualified, filling and package.
Compared with prior art, the present invention has the following advantages:
1. with water and natural tea saponin powder for carrier, to person poultry safety, be not easy to produce poisoning, safety and environmental protection to crop.
2. formula is simple, and be carrier with water, cost is low, and cost performance is high.
3. medicament thinned water amount is few, is particularly useful for the spraying of arid and high mountain water-deficient area.
4. can be used for low capacity and ultra low volume spraying, higher than conventional spray work efficiency, save cost of labor.
5. liquid drippage runs off few, and agricultural chemicals availability is high, reduces environmental pollution.
Embodiment
Comparative example 1. conventional spray agent (5% eucalyptol)
A. fill a prescription: by mass percentage, the organic solvents 85% such as eucalyptol 5%, agricultural surfactant 10%, dimethylbenzene.
B. technique: take the organic solvent 850kg such as eucalyptol 50kg, agricultural surfactant 100kg, dimethylbenzene respectively.First, the organic solvents such as dimethylbenzene are added in mixing kettle, then add eucalyptol, start agitating device fully miscible; Then, add agricultural surfactant, fully miscible to homogeneous phase transparent, be namely processed into the conventional spray agent of 1000kg containing 5% eucalyptol.
C. apply: dilute with water 1000 times, sprays with conventional spray device, every mu of (667cm
2) spray amount is 60L, agricultural chemicals availability is about 30%.
Embodiment 1. (5% eucalyptol)
A. fill a prescription: by mass percentage, eucalyptol 5%, Tea Saponin 15%, water 80%.
B. technique: take eucalyptol 50kg, natural tea saponin powder 150kg, water 800kg respectively.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add eucalyptol and mix, fully grind with sand mill, be namely processed into the low volume agent of 1000kg containing 5% eucalyptol.
C. apply: dilute with water 100 times, sprays with low volume device, every mu of (667cm
2) spray amount is 10L, agricultural chemicals availability is greater than about 60%, and nebulization efficiency is 10 times of conventional spray.
Table 1. comparative example 1 compares with embodiment 1
As can be seen from Table 1, the low volume agent of the embodiment of the present invention 1 is compared with the conventional spray agent of comparative example 1, and better, agricultural chemicals availability is high, and spray dilution water consumption is few for economy and the feature of environmental protection, is suitable for arid and the use of high mountain water-deficient area.
The preparation of embodiment 2,10% eucalyptol low volume agent and application thereof
A. fill a prescription: by mass percentage, eucalyptol 10%, Tea Saponin 12%, water 78%.
B. technique: take eucalyptol 100kg respectively, natural tea saponin powder 120kg, water 780kg.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add eucalyptol, fully mix, fully grind with sand mill, be namely processed into the low volume agent of 1000kg containing 10% eucalyptol.
C. apply: with dilution 80 times, spray with low-capacity atomizer, every mu of (667cm
2) spray amount 8L, agricultural chemicals availability about 65%, spraying work efficiency is 15 times of conventional spray.
The preparation of embodiment 3,15% eucalyptol low volume agent and application thereof
A. fill a prescription: by mass percentage, eucalyptol 15%, Tea Saponin 12%, water 73%.
B. technique: take eucalyptol 150kg respectively, natural tea saponin powder 120kg, water 730kg.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add eucalyptol, fully mix, fully grind with sand mill, be namely processed into the low volume agent of 1000kg containing 15% eucalyptol.
C. apply: with dilution 60 times, spray with low-capacity atomizer, every mu of (667cm
2) spray amount 6L, agricultural chemicals availability about 70%, spraying work efficiency is 20 times of conventional spray.
The preparation of embodiment 4,20% eucalyptol low volume agent and application thereof
A. fill a prescription: by mass percentage, eucalyptol 20%, Tea Saponin 12%, water 68%.
B. technique: take eucalyptol 20kg respectively, natural tea saponin powder 120kg, water 680kg.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add eucalyptol, fully mix, fully grind with sand mill, be namely processed into the low volume agent of 1000kg containing 20% eucalyptol.
C. apply: with dilution 40 times, spray with low-capacity atomizer, every mu of (667cm
2) spray amount 4L, agricultural chemicals availability about 75%, spraying work efficiency is 25 times of conventional spray.
The preparation of embodiment 5,25% eucalyptol low volume agent and application thereof
A. fill a prescription: by mass percentage, eucalyptol 25%, Tea Saponin 12%, water 63%.
B. technique: take eucalyptol 25kg respectively, natural tea saponin powder 120kg, water 630kg.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add eucalyptol, fully mix, fully grind with sand mill, be namely processed into the low volume agent of 1000kg containing 25% eucalyptol.
C. apply: with dilution 30 times, spray with low-capacity atomizer, every mu of (667cm
2) spray amount 3L, agricultural chemicals availability about 80%, spraying work efficiency is 30 times of conventional spray.
The preparation of embodiment 6,30% eucalyptol low volume agent and application thereof
A. fill a prescription: by mass percentage, eucalyptol 30%, Tea Saponin 12%, water 58%.
B. technique: take eucalyptol 30kg respectively, natural tea saponin powder 120kg, water 580kg.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add eucalyptol, fully mix, fully grind with sand mill, be namely processed into the low volume agent of 1000kg containing 30% eucalyptol.
C. apply: with dilution 20 times, spray with low-capacity atomizer, every mu of (667cm
2) spray amount 2L, agricultural chemicals availability about 85%, spraying work efficiency is 35 times of conventional spray.
The preparation of embodiment 7,15% eucalyptol low volume agent
Similar to Example 3, its difference is by mass percentage, eucalyptol 15%, Tea Saponin 10%, water 75%.
The preparation of embodiment 8,25% eucalyptol low volume agent
Similar to Example 5, its difference is by mass percentage, eucalyptol 25%, Tea Saponin 8%, water 67%.
The preparation of embodiment 9,30% eucalyptol low volume agent
Similar to Example 6, its difference is by mass percentage, eucalyptol 30%, Tea Saponin 5%, water 65%.
The present invention's low-capacity atomizer is sprayed, dilute with water 1 ~ 100 times, for low amounts and ultra low volume spray, and the medicine liquid spray amount 1 ~ 10L of every mu.Can be used for the control of plant pest and the dissipation of sanitary insect pest.
Claims (2)
1., containing a low-gallonage spraying agent for eucalyptol, it is characterized in that raw material by mass percentage consists of: eucalyptol 5% ~ 30%, Tea Saponin 5% ~ 15%, surplus is water.
2. a kind of low-gallonage spraying agent containing eucalyptol as claimed in claim 1, it is characterized in that raw material by mass percentage consists of: eucalyptol 5% ~ 20%, Tea Saponin 10% ~ 15%, surplus is water.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2022199653A1 (en) * | 2021-03-26 | 2022-09-29 | 江南大学 | Method for preparing eucalyptol emulsion and application thereof in biopesticide |
US11980186B2 (en) | 2021-03-26 | 2024-05-14 | Jiangnan University | Preparation method of eucalyptol emulsion and application thereof in biopesticides |
Citations (7)
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CN1286031A (en) * | 1999-08-28 | 2001-03-07 | 冼启福 | Vegetative insecticidal germicidal agent |
CN101129478A (en) * | 2007-08-17 | 2008-02-27 | 王安林 | Wormkillers of methylamino avermectin benzoate for animals, method of preparing the same and application of the same |
CN102524319A (en) * | 2011-10-18 | 2012-07-04 | 浙江农林大学 | Multiple-effect nanoscale biopesticide water aqua and use thereof |
CN102626116A (en) * | 2011-06-23 | 2012-08-08 | 北京亚戈农生物药业有限公司 | Plant pesticide and its preparation method |
CN103583588A (en) * | 2013-11-12 | 2014-02-19 | 老知青集团有限公司 | Tea saponin biological insecticide and preparation method thereof |
CN104365687A (en) * | 2014-11-26 | 2015-02-25 | 曾少兰 | Sophocarpidine insecticide aqueous agent and preparation method thereof |
CN104430616A (en) * | 2014-11-27 | 2015-03-25 | 青岛崂乡茶制品有限公司 | Efficient-sterilization biopesticide |
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2015
- 2015-06-12 CN CN201510321322.0A patent/CN104920492A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1286031A (en) * | 1999-08-28 | 2001-03-07 | 冼启福 | Vegetative insecticidal germicidal agent |
CN101129478A (en) * | 2007-08-17 | 2008-02-27 | 王安林 | Wormkillers of methylamino avermectin benzoate for animals, method of preparing the same and application of the same |
CN102626116A (en) * | 2011-06-23 | 2012-08-08 | 北京亚戈农生物药业有限公司 | Plant pesticide and its preparation method |
CN102524319A (en) * | 2011-10-18 | 2012-07-04 | 浙江农林大学 | Multiple-effect nanoscale biopesticide water aqua and use thereof |
CN103583588A (en) * | 2013-11-12 | 2014-02-19 | 老知青集团有限公司 | Tea saponin biological insecticide and preparation method thereof |
CN104365687A (en) * | 2014-11-26 | 2015-02-25 | 曾少兰 | Sophocarpidine insecticide aqueous agent and preparation method thereof |
CN104430616A (en) * | 2014-11-27 | 2015-03-25 | 青岛崂乡茶制品有限公司 | Efficient-sterilization biopesticide |
Non-Patent Citations (3)
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刘步林: "《农药剂型加工技术》", 31 October 1998, 化学工业出版社 * |
沈立荣等,: ""油茶粕茶皂素作为农药助剂和生物农药的研究进展"", 《湖州职业技术学院学报》 * |
程伯瑛: "《设施蔬菜病虫害防治技术问答》", 31 January 2010, 金盾出版社 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2022199653A1 (en) * | 2021-03-26 | 2022-09-29 | 江南大学 | Method for preparing eucalyptol emulsion and application thereof in biopesticide |
US11980186B2 (en) | 2021-03-26 | 2024-05-14 | Jiangnan University | Preparation method of eucalyptol emulsion and application thereof in biopesticides |
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Application publication date: 20150923 |
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