CN104996443A - Low volume spray containing diafenthiuron and tolfenpxrad - Google Patents

Low volume spray containing diafenthiuron and tolfenpxrad Download PDF

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Publication number
CN104996443A
CN104996443A CN201510321520.7A CN201510321520A CN104996443A CN 104996443 A CN104996443 A CN 104996443A CN 201510321520 A CN201510321520 A CN 201510321520A CN 104996443 A CN104996443 A CN 104996443A
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CN
China
Prior art keywords
water
diafenthiuron
low volume
tolfenpyrad
tea saponin
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Pending
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CN201510321520.7A
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Chinese (zh)
Inventor
颜禧凯
颜禧童
颜禧旋
潘朝斌
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De Sheng Biotechnology Co Ltd Of Fujian Province
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De Sheng Biotechnology Co Ltd Of Fujian Province
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Priority to CN201510321520.7A priority Critical patent/CN104996443A/en
Publication of CN104996443A publication Critical patent/CN104996443A/en
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Abstract

The invention discloses low volume spray containing diafenthiuron and tolfenpxrad, and relates to pesticide. The low volume spray containing diafenthiuron and tolfenpxrad is composed of, by mass, 10%-50% of diafenthiuron, 1%-20% of tolfenpxrad, 5%-15% of tea saponin, and the balance water. During preparation, the water and the tea saponin are added into a deploying kettle to be evenly mixed, and then the diafenthiuron and the tolfenpxrad are added to be fully dispersed in mixed liquor of the water and the tea saponin; afterwards, a sand mill is used for grinding, sampling detection is qualified, and filling package is conducted. The water and the tea saponin are used as carriers, so that people and livestock are safe, no phytotoxicity on crops can be easily caused, and safety and environmental protection are achieved. The formula is simple, the water is used as the carrier, so that cost is low, and cost performance is high. The dilution water consumption of drugs is small, and the low volume spray is particularly suitable for mist spraying in dry and high mountain water-deficient areas. The low volume spray is used for low volume and ultra-low volume mist spraying, the work efficiency is high compared with constant quantity mist spraying, and labor cost is saved. Dripping loss of liquor is small, the pesticide utilization rate is high, and environmental pollution is reduced.

Description

A kind of low-gallonage spraying agent containing diafenthiuron and Tolfenpyrad
Technical field
The present invention relates to agricultural chemicals, especially relate to a kind of low-gallonage spraying agent containing diafenthiuron and Tolfenpyrad.
Technical background
The medical treatment of diseases and pests of agronomic crop and sanitary insect pest, spray-on process is modal application method, is namely made into liquid with a certain amount of agricultural chemicals and appropriate water or oil, with spraying apparatus, medicine liquid spray is become droplet.By every mu of (667cm 2) number of spray liquid amount, spray-on process is often divided into conventional spray, low volume and ultra low volume spray.
1, conventional spray, agricultural chemicals dilutes with water, and extension rate is greater than 1000 times, and every mu of spouting liquid, at 45 ~ 60L, is the conventional spray-on process in present stage China's plant protection field.This spray-on process spray amount is large, and work efficiency is not high, and liquid drippage runs off serious, and agricultural chemicals availability is less than 30%.
2, low volume, agricultural chemicals is with water or oil dilution, and extension rate about 100 times, every mu of spray liquid amount 5 ~ 15L, is called low volume.This spray-on process, spray amount is lower, and work efficiency is 5 ~ 10 times of conventional spray.Agricultural chemicals runs off few, and availability can reach more than 60%.
3, ultra low volume spray, agricultural chemicals is with water or oil dilution, and extension rate is lower than 10 times, and every mu of spouting liquid is 0.5 ~ 2.5L, is called ultra low volume spray, and spray amount is very low, and work efficiency is 10 ~ 50 times of conventional spray, and agricultural chemicals runs off seldom, and availability can reach more than 80%.
The control of China's plant protection field crop disease and insect, at present still based on conventional spray.Because its droplet is large, target produces spring, drippage runs off serious, and agricultural chemicals availability is not high, to environment, also can make that agricultural product agriculture is residual to exceed standard; Again because its spray amount is large, spraying work efficiency is low, and cost of labor is also high; Conventional spray agent dilute with water multiple is greater than 1000 times, and water consumption is large, is unfavorable for that arid and high mountain water-deficient area use.
It is worth mentioning that, conventional spray agent with dimethylbenzene etc. to the organic solvent of human body and bad environmental and petrochemical industry class surfactant for carrier, safety and the feature of environmental protection are all bad, all can produce harm to human body and crop, can not in order to low amounts and ultra low volume spray; For realizing the accurate high-efficiency prevention and control of diseases and pests of agronomic crop, reducing agricultural chemicals and running off, reducing the pollution to environment and agricultural product, improving agricultural chemicals availability, improve spraying work efficiency, the agent of research and development low-gallonage spraying, very necessary.
Chinese patent CN103271051A discloses a kind of Tolfenpyrad and the composite Pesticidal combination with synergistic function of diafenthiuron, said composition is made up of Tolfenpyrad and diafenthiuron two kinds of active ingredients and auxiliary agent or carrier, wherein the mass ratio of Tolfenpyrad and diafenthiuron is 30:1 ~ 1:30, and Tolfenpyrad and diafenthiuron gross mass mark is in the composition 5% ~ 80%.
Obviously, existing medicament all adopts traditional organic solvent usually, all there is potential safety hazard, can not be used for the low-gallonage spraying of high-load liquid to human body, plant, environment etc.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of low-gallonage spraying agent containing diafenthiuron and Tolfenpyrad is provided.
The present invention's raw material by mass percentage consists of: diafenthiuron 10% ~ 50%, Tolfenpyrad 1% ~ 20%, Tea Saponin 5% ~ 15%, and surplus is water.
The present invention's raw material composition is by mass percentage preferably: diafenthiuron 15% ~ 45%, Tolfenpyrad 5% ~ 15%, Tea Saponin 10% ~ 15%, surplus is water.
During use, with low-capacity atomizer spraying, dilute with water 1 ~ 100 times, for low amounts and ultra low volume spray, the medicine liquid spray amount 1 ~ 10L of every mu, for the control of plant pest and the dissipation of sanitary insect pest.
During preparation, water and Tea Saponin are added compounding kettle and mixes, then add diafenthiuron and Tolfenpyrad, be well-dispersed in water and Tea Saponin mixed liquor, then with sand mill grinding, sample detection qualified, filling and package.
Compared with prior art, the present invention has the following advantages:
1. with water and natural tea saponin powder for carrier, to person poultry safety, be not easy to produce poisoning, safety and environmental protection to crop.
2. formula is simple, and be carrier with water, cost is low, and cost performance is high.
3. medicament thinned water amount is few, is particularly useful for the spraying of arid and high mountain water-deficient area.
4. can be used for low capacity and ultra low volume spraying, higher than conventional spray work efficiency, save cost of labor.
5. liquid drippage runs off few, and agricultural chemicals availability is high, reduces environmental pollution.
Embodiment
Comparative example 1. conventional spray agent (20% diafenthiuron and Tolfenpyrad)
A. fill a prescription: by mass percentage, the organic solvents 70% such as diafenthiuron 15%, Tolfenpyrad 5%, agricultural surfactant 10%, dimethylbenzene.
B. technique: take the organic solvent 700kg such as diafenthiuron 150kg, Tolfenpyrad 50kg, agricultural surfactant 100kg, dimethylbenzene respectively.First, the organic solvents such as dimethylbenzene are added in mixing kettle, then add diafenthiuron and Tolfenpyrad, start agitating device fully miscible; Then, add agricultural surfactant, fully miscible to homogeneous phase transparent, be namely processed into the conventional spray agent that 1000kg contains 20% diafenthiuron and Tolfenpyrad.
C. apply: dilute with water 1000 times, sprays with conventional spray device, and every mu of spray amount is 60L, and agricultural chemicals availability is about 30%.
Embodiment 1.20% diafenthiuron and the agent of Tolfenpyrad low volume
A. fill a prescription: by mass percentage, diafenthiuron 15%, Tolfenpyrad 5%, Tea Saponin 15%, water 65%.
B. technique: take diafenthiuron 150kg, Tolfenpyrad 50kg, natural tea saponin powder 150kg, water 650kg respectively.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add diafenthiuron and mix with Tolfenpyrad, fully grind with sand mill, be namely processed into the low volume agent that 1000kg contains 20% diafenthiuron and Tolfenpyrad.
C. apply: dilute with water 100 times, sprays with low volume device, and every mu of spray amount is 10L, and agricultural chemicals availability is greater than about 60%, and nebulization efficiency is 10 times of conventional spray.
Table 1. comparative example 1 compares with embodiment 1
As can be seen from Table 1, the low volume agent of the embodiment of the present invention 1 is compared with the conventional spray agent of comparative example 1, and better, agricultural chemicals availability is high, and spray dilution water consumption is few for economy and the feature of environmental protection, is suitable for arid and the use of high mountain water-deficient area.
The preparation of embodiment 2,30% diafenthiuron and the agent of Tolfenpyrad low volume and application thereof
A. fill a prescription: by mass percentage, diafenthiuron 25%, Tolfenpyrad 5%, Tea Saponin 12%, water 58%.
B. technique: take diafenthiuron 250kg respectively, Tolfenpyrad 50kg, natural tea saponin powder 120kg, water 580kg.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add diafenthiuron and Tolfenpyrad, fully mix, fully grind with sand mill, be namely processed into the low volume agent that 1000kg contains 30% diafenthiuron and Tolfenpyrad.
C. apply: with dilution 80 times, spray, every mu of spray amount 8L, agricultural chemicals availability about 65% with low-capacity atomizer, spraying work efficiency is 15 times of conventional spray.
The preparation of embodiment 3,40% diafenthiuron and the agent of Tolfenpyrad low volume and application thereof
A. fill a prescription: by mass percentage, diafenthiuron 35%, Tolfenpyrad 5%, Tea Saponin 11%, water 49%.
B. technique: take diafenthiuron 350kg, Tolfenpyrad 50kg, natural tea saponin powder 110kg, water 490kg respectively.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add diafenthiuron and Tolfenpyrad, fully mix, fully grind with sand mill, be namely processed into the low volume agent that 1000kg contains 40% diafenthiuron and Tolfenpyrad.
C. apply: with dilution 60 times, spray, every mu of spray amount 6L, agricultural chemicals availability about 70% with low-capacity atomizer, spraying work efficiency is 20 times of conventional spray.
The preparation of embodiment 4,50% diafenthiuron and Tolfenpyrad spray and application thereof
A. fill a prescription: by mass percentage, diafenthiuron 35%, Tolfenpyrad 15%, Tea Saponin 10%, water 40%.
B. technique: take diafenthiuron 350kg respectively, Tolfenpyrad 150kg, natural tea saponin powder 100kg, water 400kg.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add diafenthiuron and Tolfenpyrad, fully mix, fully grind with sand mill, be namely processed into the low volume agent that 1000kg contains 50% diafenthiuron and Tolfenpyrad.
C. apply: with dilution 40 times, spray, every mu of spray amount 4L, agricultural chemicals availability about 75% with low-capacity atomizer, spraying work efficiency is 25 times of conventional spray.
The preparation of embodiment 5,30% diafenthiuron and Tolfenpyrad spray and application thereof
A. fill a prescription: by mass percentage, diafenthiuron 10%, Tolfenpyrad 20%, Tea Saponin 5%, water 65%.
B. technique: take diafenthiuron 100kg respectively, Tolfenpyrad 200kg, natural tea saponin powder 50kg, water 650kg.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add diafenthiuron and Tolfenpyrad, fully mix, fully grind with sand mill, be namely processed into the low volume agent that 1000kg contains 30% diafenthiuron and Tolfenpyrad.
C. apply: with dilution 30 times, spray, every mu of spray amount 3L, agricultural chemicals availability about 80% with low-capacity atomizer, spraying work efficiency is 30 times of conventional spray.
The preparation of embodiment 6,51% diafenthiuron and Tolfenpyrad spray and application thereof
A. fill a prescription: by mass percentage, diafenthiuron 50%, Tolfenpyrad 1%, Tea Saponin 10%, water 39%.
B. technique: take diafenthiuron 500kg respectively, Tolfenpyrad 10kg, natural tea saponin powder 100kg, water 390kg.First, water is added in mixing kettle, then add Tea Saponin, start agitating device fully miscible; Then, add diafenthiuron and Tolfenpyrad, fully mix, fully grind with sand mill, be namely processed into the low volume agent that 1000kg contains 51% diafenthiuron and Tolfenpyrad.
C. apply: with dilution 20 times, spray, every mu of spray amount 2L, agricultural chemicals availability about 85% with low-capacity atomizer, spraying work efficiency is 35 times of conventional spray.
The preparation of embodiment 7,40% diafenthiuron and Tolfenpyrad spray and application thereof
Similar to Example 3, its difference is by mass percentage, diafenthiuron 30%, Tolfenpyrad 10%, Tea Saponin 8%, water 52%.
The preparation of embodiment 8,48% diafenthiuron and Tolfenpyrad spray and application thereof
Similar to Example 4, its difference is by mass percentage, diafenthiuron 40%, Tolfenpyrad 8%, Tea Saponin 8%, water 44%.
The present invention's low-capacity atomizer is sprayed, dilute with water 1 ~ 100 times, for low amounts and ultra low volume spray, and the medicine liquid spray amount 1 ~ 10L of every mu.Can be used for the control of plant pest and the dissipation of sanitary insect pest.

Claims (2)

1., containing a low-gallonage spraying agent for diafenthiuron and Tolfenpyrad, it is characterized in that its raw material by mass percentage consists of: diafenthiuron 10% ~ 50%, Tolfenpyrad 1% ~ 20%, Tea Saponin 5% ~ 15%, surplus is water.
2. a kind of low-gallonage spraying agent containing diafenthiuron and Tolfenpyrad as claimed in claim 1, is characterized in that its raw material by mass percentage consists of: diafenthiuron 15% ~ 45%, Tolfenpyrad 5% ~ 15%, Tea Saponin 10% ~ 15%, surplus is water.
CN201510321520.7A 2015-06-12 2015-06-12 Low volume spray containing diafenthiuron and tolfenpxrad Pending CN104996443A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101755752A (en) * 2009-12-29 2010-06-30 华南农业大学 Pesticide by mixing tea saponin with pyrrole and pyrazole pesticide
CN103238613A (en) * 2012-02-08 2013-08-14 陕西美邦农药有限公司 Insecticidal composition containing tolfenpyrad
CN103271051A (en) * 2013-04-27 2013-09-04 广东中迅农科股份有限公司 Tolfenpyrad-diafenthiuron composite insecticide composition having synergism
CN103609576A (en) * 2013-11-11 2014-03-05 丹阳市清云农业发展有限公司 Compound pesticide composition and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101755752A (en) * 2009-12-29 2010-06-30 华南农业大学 Pesticide by mixing tea saponin with pyrrole and pyrazole pesticide
CN103238613A (en) * 2012-02-08 2013-08-14 陕西美邦农药有限公司 Insecticidal composition containing tolfenpyrad
CN103271051A (en) * 2013-04-27 2013-09-04 广东中迅农科股份有限公司 Tolfenpyrad-diafenthiuron composite insecticide composition having synergism
CN103609576A (en) * 2013-11-11 2014-03-05 丹阳市清云农业发展有限公司 Compound pesticide composition and preparation method thereof

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