CN104906607B - A kind of multifunction pouring taper sterilizing equipment and sterilization process - Google Patents
A kind of multifunction pouring taper sterilizing equipment and sterilization process Download PDFInfo
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- CN104906607B CN104906607B CN201510355985.4A CN201510355985A CN104906607B CN 104906607 B CN104906607 B CN 104906607B CN 201510355985 A CN201510355985 A CN 201510355985A CN 104906607 B CN104906607 B CN 104906607B
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Abstract
The invention discloses a kind of sterilizings of multifunction pouring taper to equip, it includes vertical sterilization cylinder, trumpet cooler, circulating pump, catch basin A, plate-type condenser, surge tank, vacuum pump and catch basin B, and vertical sterilization cylinder includes cylinder, fly knife device, ozone inlet, outlet valve, stack shell drain port, multiple coil agitating paddle, temperature sensor, cover drain port, ozone discharge outlet, gas outlet, speed reducer, top spray mouth, feed inlet and jacket steam import.The invention also discloses a kind of sterilization process, including high-temp steam sterilizing technique, low temperature alcohol sterilization process, room temperature ozone sterilization technique and dry materials operating procedure.Multiple coil agitating paddle is set in cylinder, agitating paddle is free to rotate, so that material is uniformly mixed, fly knife device can prevent material caking, conglomeration, and in sterilization process, recyclable organic solvent simultaneously recycles, cylinder interlayer and agitating paddle interlayer can be passed through steam or hot water simultaneously, abundant heating and thermal insulation is carried out to material, temperature amplitude of accommodation range is big, is suitble to different sterilizings or heating temperature requirement.
Description
Technical field
The present invention relates to a kind of sterilizings of multifunction pouring taper to equip.
The invention further relates to a kind of techniques to be sterilized using multifunction pouring taper sterilizing equipment.
It can be used for sterilizing, drying for Chinese medicine and its preparation.Suitable for the sterilizing of the industries such as food, chemical industry, medicine, dry behaviour
Make.
Background technology
Chinese medicine and its preparation are made of a variety of drugs, and complicated component, especially pill, powder, raw material are mainly Chinese medicine
Medicine materical crude slice is used as medicine after crushing.It since medicinal material is planted, grows, harvesting, particularity, most of Chinese medicine material medicines such as processing are all different degrees of
With some moulds, bacterium and other pathogenic bacteria.In addition, the working condition of Chinese medicine preparation is relatively low, and mechanical equipment, packing timber
Material etc. is more simple and crude, and than great, opportunities for contamination is more, more so as to cause germ contamination chance for manual operations.It is necessary when sterilizing
The effective sterilizing methods of the comprehensive selections such as property, dosage form in conjunction with drug reasonably apply sterilization technology.
Traditional high pressure steam sterilization is one of most widely used sterilizing methods, and sterilization effect is simple and reliable, but uncomfortable
The sterilizing of Chinese medicine and its preparation for case of thermal instability, and traditional high pressure steam sterilization can make material lump, then crush
Process easily causes the loss and waste of secondary pollution and material；And60Although Co sterilizing methods be suitble to Chinese medicine containing heat-sensitive ingredients and
The sterilizing of preparation, but its problem of there is also the radiation of of high cost, overdose, country for60Co radiation sterilization be applied to Chinese medicine and
It is that should not use to have stringent dose of radiation requirement and kind specification, some herbal species in preparation60What Co sterilized.And
,60Co its safety that sterilize still has dispute in academia.
Problem above not only drastically influences the quality and safety of Chinese medicine preparation, and does not adapt to industry energy conservation emission reduction
Environmentally friendly construction object.Therefore, research is a kind of integrating a variety of sterilizing functions, energy-efficient sterilizing equipment and technique,
It is beneficial to improve the common problem of current tcm manufacturing process sterilizing, cost performance is provided for Chinese Traditional Medicine sterilization unit
High, the reliable convenient sterilizing installation of sterilizing and method, ensure drug quality and safety, while greatly saving cost and the energy disappears
Consumption.
Invention content
The technical problem to be solved in the invention is to provide a kind of multifunction pouring taper sterilizing equipment.Equipment configuration letter
Single, vdiverse in function, sterilizing is conveniently, reliably.
The present invention also need to solve the technical issues of be to provide it is a kind of using multifunction pouring taper sterilizing equip sterilize
Technique.
To solve the technical problem of the present invention, the technical solution adopted by the present invention is：
A kind of multifunction pouring taper sterilizing equipment, it include vertical sterilization cylinder, trumpet cooler, circulating pump, catch basin A,
Plate-type condenser, surge tank, vacuum pump and catch basin B, the gas outlet of the vertical sterilization cylinder is connect with trumpet cooler, described
Trumpet cooler is connect with plate-type condenser, and the plate-type condenser is connect with surge tank, and the buffering pot bottom placement is catchmented
Slot B, the surge tank are connect with vacuum pump, equal at the cover drain port of the vertical sterilization cylinder, stack shell drain port and outlet valve
It is connect with catch basin A by pipeline, the catch basin A is connect with circulating pump.
Further, the vertical sterilization cylinder includes that cylinder, fly knife device, ozone inlet, outlet valve, stack shell are hydrophobic
Mouth, multiple coil agitating paddle, temperature sensor, cover drain port, ozone discharge outlet, gas outlet, speed reducer, top spray mouth,
Feed inlet and jacket steam import, the speed reducer driving multiple coil agitating paddle rotation, the multiple coil agitating paddle stretch into
In cylinder, the cylinder lateral wall is equipped with fly knife device, has top spray mouth, the temperature sensor peace on the cylinder cover
Loaded on cylinder lateral wall, the top and lower part of the cylinder have cover drain port and stack shell drain port, the top of the cylinder
Portion and bottom are respectively provided with feed inlet and outlet valve, and the cylinder lower part and top have ozone inlet and ozone discharge
Mouthful, it is provided with jacket steam import at the top of the cylinder.
A kind of technique to be sterilized using multifunction pouring taper sterilizing equipment, including high-temp steam sterilizing technique, low temperature
Alcohol sterilization process, room temperature ozone sterilization technique and dry materials operating procedure,
High-temp steam sterilizing technique, first by vacuum pump to being vacuumized in cylinder, then by collet chuck layer and multistage spiral shell
Rotation agitating paddle interlayer is passed through steam and carries out being preheated to 70-90 DEG C to material, then 105-125 DEG C of high pressure steaming is squeezed into cylinder
Vapour, material are fully contacted with wet-hot steam under the stirring action of multiple coil agitating paddle, reach 115 DEG C of sterilization process parameter
10-50min sterilizings are kept the temperature again, or are reached 121 DEG C of sterilization process parameter and kept the temperature 10-50min sterilizings, after sterilizing, cylinder again
Interior stopping is passed through steam, and by vacuum pump, to being vacuumized in cylinder, steam passes through interlayer and multiple coil agitating paddle interlayer pair
Material heats, and is dried under reduced pressure to material under the agitation of multiple coil agitating paddle, and temperature is maintained at 50-85 DEG C, and material is dry
It is dry to after specified moisture content, when in cylinder without vacuum can shut down the outlet valve opened positioned at cylinder bottom discharges, and sterilizes
Journey is completed；
Low temperature alcohol sterilization process is passed through hot bath to collet chuck layer and multiple coil agitating paddle interlayer first and is carried out to material
Preheating, then into cylinder, material sprays the alcohol of 70%~80% mass concentration, alcohol by the alcohol spray inlet on cover
Quality be the 5%~20% of material, under the stirring of multiple coil agitating paddle, alcohol fully with material mixing, then with water-bath pair
Material carries out insulated sterilizing 1-1.5 hours, carries out being dried under reduced pressure operation according to the above-mentioned process that is dried under reduced pressure after sterilizing, dry
Discharging can be shut down by finishing, and sterilization process is completed；
Room temperature ozone sterilization technique, need not heat material, and ozone first is from the ozone air inlet positioned at cylinder bottom
Mouth is constantly passed through in cylinder, and material comes into full contact under the continuous agitation of multiple coil agitating paddle with ozone, is first passed through
Ozone ensures that ozone concentration is continually fed into ozone two to ensure sterilization effect in cylinder first from the ozone discharge outlet discharge on cover
It sterilizes and finishes after hour, you can shut down discharging, sterilization process is completed；
Dry materials operating procedure, i.e., to being vacuumized in cylinder while collet chuck layer and agitating paddle interlayer water-bath are carried out to material
Heating, material are kept for 60-85 DEG C under the agitation of multiple coil agitating paddle, discharging can be shut down after reaching regulation moisture.
Beneficial effects of the present invention：Multiple coil agitating paddle is set in cylinder, agitating paddle is free to rotate so that material mixes
Uniformly, no dead angle, fly knife device can prevent material caking, conglomeration, and in sterilization process, recyclable organic solvent simultaneously recycles,
Cylinder interlayer and agitating paddle interlayer can be passed through steam or hot water simultaneously, and abundant heating and thermal insulation, the temperature amplitude of accommodation are carried out to material
Range is big, is suitble to different sterilizings or heating temperature requirement.
Description of the drawings
Fig. 1 is the structural diagram of the present invention.
1, vertical sterilization cylinder, 2, fly knife device, 3, ozone inlet, 4, outlet valve, 5, stack shell drain port, 6, multiple coil
Agitating paddle, 7, temperature sensor, 8, cover drain port, 9, ozone discharge outlet, 10, gas outlet, 11, speed reducer, 12, top spray
Mouthful, 13, feed inlet, 14, jacket steam import, 15, trumpet cooler, 16, circulating pump, 17, catch basin A, 18, board-like condensation
Device, 19, surge tank, 20, vacuum pump, 21, catch basin B.
Specific implementation mode
The invention will be further described in the following with reference to the drawings and specific embodiments.Following embodiment is merely to illustrate this hair
It is bright, it is not limited to protection scope of the present invention.
With reference to figure 1, a kind of multifunction pouring taper of the invention sterilizing equipment, it includes vertical sterilization cylinder, trumpet cooler
15, circulating pump 16, catch basin A17, plate-type condenser 18, surge tank 19, vacuum pump 20 and catch basin B21, vertical sterilization cylinder 1
Gas outlet 10 is connect with trumpet cooler 15, and trumpet cooler 15 is connect with plate-type condenser 18, plate-type condenser 18 and buffering
Tank 19 connects, and catch basin B21 is placed in 19 bottom of surge tank, and surge tank 19 is connect with vacuum pump 20, and the cover of vertical sterilization cylinder 1 is dredged
It is connect with catch basin A17 by pipeline at the mouth of a river 8, stack shell drain port 5 and outlet valve 4, catch basin A17 connects with circulating pump 16
It connects.
Vertical sterilization cylinder includes cylinder 1, fly knife device 2, ozone inlet 3, outlet valve 4, stack shell drain port 5, multistage spiral shell
Revolve agitating paddle 6, temperature sensor 7, cover drain port 8, ozone discharge outlet 9, gas outlet 10, speed reducer 11, top spray mouth 12,
Feed inlet 13 and jacket steam import 14, speed reducer 11 drive multiple coil agitating paddle 6 to rotate, and multiple coil agitating paddle 6 stretches into
In cylinder 1,1 side wall of cylinder is equipped with fly knife device 2, and cylinder 1 is covered with top spray mouth 12, and temperature sensor 7 is installed on
1 side wall of cylinder, the top and lower part of cylinder 1 have cover drain port 8 and stack shell drain port 5, the top and bottom of cylinder 1
It is respectively provided with feed inlet 13 and outlet valve 4,1 lower part of cylinder and top have ozone inlet 3 and ozone discharge outlet 9, cylinder
1 top of body is provided with jacket steam import 14.
Above-mentioned fly knife device 2 is mainly made of motor and blade, can prevent material caking, conglomeration.
Wherein, vertical sterilizing barrel shape of the invention is inverted conical, is the main body of sterilizing equipment, is arranged in cylinder 1
It is hollow design to have multiple coil agitating paddle 6, multiple coil agitating paddle, there is the pipeline of connection vapour source and catch basin on cover,
Steam or hot water heating can be passed through in multiple coil agitating paddle.In cover upper connector formula condenser 15 to cylinder, ethyl alcohol can be steamed
Vapour is condensed.Vapour source can give simultaneously conical shell interlayer, in cylinder, steam is provided in multiple coil agitating paddle, can also give
Catch basin provides heat source.Catch basin can give conical tube interlayer body, in cylinder, cold bath or heat are provided in multiple coil agitating paddle
Water-bath.By ozone generator ozone is constantly provided into cylinder 1 to the ozone inlet 3 positioned at 1 bottom of cylinder.
Trumpet cooler 15 is connected to plate-type condenser 18, then is connected to vacuum pump 20 by surge tank 19.A kind of more work(
The equipment that can sterilize can to greatest extent be saved by the connection of pipeline and the work realization hot water of heat-exchanger pump or recycling for steam
The energy.
A kind of technique to be sterilized using multifunction pouring taper sterilizing equipment, including high-temp steam sterilizing technique, low temperature
Alcohol sterilization process, room temperature ozone sterilization technique and dry materials operating procedure,
High-temp steam sterilizing technique, first by vacuum pump 20 to being vacuumized in cylinder 1, then by collet chuck layer and multistage
Propeller interlayer is passed through steam and carries out being preheated to 70-90 DEG C to material, then 105-125 DEG C of high pressure is squeezed into cylinder 1
Steam, material are fully contacted with wet-hot steam under the stirring action of multiple coil agitating paddle 6, reach sterilization process parameter 115
10-50min sterilizings DEG C are kept the temperature again, or are reached 121 DEG C of sterilization process parameter and kept the temperature 10-50min sterilizings, after sterilizing, cylinder again
Stop being passed through steam in body 1, by vacuum pump, be vacuumized in 20 pairs of cylinders, steam passes through interlayer and multiple coil agitating paddle
Interlayer heats material, is dried under reduced pressure to material under the agitation of multiple coil agitating paddle 6, and temperature is maintained at 50-85 DEG C,
After dry materials to specified moisture content, the discharging opened positioned at cylinder bottom can be shut down when in cylinder without vacuum, 4 discharge,
Sterilization process is completed；
Low temperature（60-70℃）Alcohol sterilization process is passed through hot bath to collet chuck layer and multiple coil agitating paddle interlayer first
（60-70℃）Material is preheated, then the material sprinkling 70%~80% into cylinder by the alcohol spray inlet on cover
The alcohol of mass concentration, the quality of alcohol is the 5%~20% of material, under the stirring of multiple coil agitating paddle 6, alcohol fully with
Material mixing, then insulated sterilizing is carried out 1-1.5 hours to material with water-bath, after sterilizing according to it is above-mentioned be dried under reduced pressure process into
Row is dried under reduced pressure operation, and dry finish can shut down discharging, and sterilization process is completed；
Room temperature ozone sterilization technique, need not heat material, and ozone first is from the ozone air inlet positioned at cylinder bottom
Mouth 3 is constantly passed through in cylinder 1, and material comes into full contact under the continuous agitation of multiple coil agitating paddle with ozone, is first passed through
Ozone first from cover ozone discharge outlet 9 be discharged, ensure cylinder in ozone concentration to ensure sterilization effect, be continually fed into ozone
Sterilizing finishes after two hours, you can shuts down discharging, sterilization process is completed；
Dry materials operating procedure, i.e., to being vacuumized in cylinder while collet chuck layer and agitating paddle interlayer water-bath are carried out to material
Heating, material are kept for 60-85 DEG C under the agitation of multiple coil agitating paddle, discharging can be shut down after reaching regulation moisture.
The present invention compared with the prior art, has the following advantages that：
（1）Compared with conventional sterilization equipment, the equipment material filling amount of the invention is big, can improve production efficiency, simultaneously
Save floor space；
（2）Sterilization process is dynamic process, the material in cylinder can dynamic motion, inside set multiple coil agitating paddle, stir
Paddle is free to rotate so that material is uniformly mixed, no dead angle；
（3）Sterilization process material is prevented from caking, conglomeration, due to having grinding device in cylinder（Fly knife device）, can avoid passing
The methods of system steam sterilizing easily causes the problem of material caking, greatly improves the adaptability of equipment, is applicable in granular material, particle
The sterilizing-drying of the materials such as shape material, lump material operates；
（4）In sterilization process, recyclable organic solvent（Such as ethyl alcohol）, and recycle, reduce production cost；
（5）It can be required according to the sterilizing of different material, control different sterilization process conditions, to realize that high-temperature steam goes out
Bacterium, the sterilizing of low temperature alcohol and room temperature ozone sterilization；
（6）The material high suitable for heat-sensitive ingredients content, the material containing volatile ingredient, the labile object of heat
Material, the sterilizing containing the primary medicinal powder of the Chinese medicines such as oxidizable component material, extract powder, the prepared slices of Chinese crude drugs etc.；
（7）Cylinder interlayer and agitating paddle interlayer can be passed through steam or hot water simultaneously, and abundant heating and thermal insulation, temperature are carried out to material
It is big to spend amplitude of accommodation range, is suitble to different sterilizings or heating temperature requirement.
Claims (2)
1. a kind of multifunction pouring taper sterilizing equipment, it is characterised in that：It include vertical sterilization cylinder, trumpet cooler, circulating pump,
Catch basin A, plate-type condenser, surge tank, vacuum pump and catch basin B, the gas outlet of the vertical sterilization cylinder and trumpet cooler
Connection, the trumpet cooler are connect with plate-type condenser, and the plate-type condenser is connect with surge tank, the buffering pot bottom
Catch basin B is placed, the surge tank connect with vacuum pump, the cover drain port of the vertical sterilization cylinder, stack shell drain port and goes out
It is connect with catch basin A by pipeline at material valve, the catch basin A is connect with circulating pump；The vertical sterilization cylinder include cylinder,
It is fly knife device, ozone inlet, outlet valve, stack shell drain port, multiple coil agitating paddle, temperature sensor, cover drain port, smelly
Oxygen floss hole, gas outlet, speed reducer, top spray mouth, feed inlet and jacket steam import, the speed reducer drive multiple coil
Agitating paddle rotates, and the multiple coil agitating paddle stretches into cylinder, and the cylinder lateral wall is equipped with fly knife device, the cylinder cover
Upper that there is top spray mouth, the temperature sensor to be installed on cylinder lateral wall, the top and lower part of the cylinder have cylinder
Lid drain port and stack shell drain port are respectively provided with feed inlet and outlet valve, the cylinder lower part at the top and bottom of the cylinder
Ozone inlet and ozone discharge outlet are had with top, jacket steam import is provided at the top of the cylinder.
2. the technique to be sterilized using a kind of multifunction pouring taper sterilizing equipment described in claim 1, it is characterised in that：Packet
High-temp steam sterilizing technique, low temperature alcohol sterilization process, room temperature ozone sterilization technique and dry materials operating procedure are included,
High-temp steam sterilizing technique, first by vacuum pump to being vacuumized in cylinder, then by stirring collet chuck layer and multiple coil
It mixes paddle interlayer and is passed through steam and material is carried out to be preheated to 70-90 DEG C, then squeeze into 105-125 DEG C of high steam, object in cylinder
Material fully contacts with wet-hot steam under the stirring action of multiple coil agitating paddle, reaches 115 DEG C of sterilization process parameter and keep the temperature again
10-50min sterilizes, or reaches 121 DEG C of sterilization process parameter and keep the temperature 10-50min sterilizings again, after sterilizing, stops in cylinder
It is passed through steam, by vacuum pump, to being vacuumized in cylinder, steam adds material by interlayer and multiple coil agitating paddle interlayer
Heat is dried under reduced pressure material under the agitation of multiple coil agitating paddle, and temperature is maintained at 50-85 DEG C, dry materials to rule
After determining water content, outlet valve of the opening positioned at cylinder bottom can be shut down when in cylinder without vacuum and is discharged, sterilization process is completed；
Low temperature alcohol sterilization process is passed through hot bath to collet chuck layer and multiple coil agitating paddle interlayer first and is carried out in advance to material
Heat, then into cylinder, material sprays the alcohol of 70%~80% mass concentration by the alcohol spray inlet on cover, alcohol
Quality is the 5%~20% of material, under the stirring of multiple coil agitating paddle, alcohol fully with material mixing, then with water-bath to object
Material carries out insulated sterilizing 1-1.5 hours, carries out being dried under reduced pressure operation according to the above-mentioned process that is dried under reduced pressure after sterilizing, dry
Discharging can be shut down by finishing, and sterilization process is completed；
Room temperature ozone sterilization technique, need not heat material, and ozone is held from the ozone inlet positioned at cylinder bottom first
Continuous to be constantly passed through in cylinder, material comes into full contact under the continuous agitation of multiple coil agitating paddle with ozone, the ozone being first passed through
First from the ozone discharge outlet discharge on cover, ensure that ozone concentration is continually fed into ozone two hours to ensure sterilization effect in cylinder
Sterilizing finishes afterwards, you can shuts down discharging, sterilization process is completed；
Dry materials operating procedure, i.e., to being vacuumized in cylinder while collet chuck layer and agitating paddle interlayer water-bath carried out to material add
Heat, material are kept for 60-85 DEG C under the agitation of multiple coil agitating paddle, discharging can be shut down after reaching regulation moisture.
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| CN201510355985.4A CN104906607B (en) | 2015-06-25 | 2015-06-25 | A kind of multifunction pouring taper sterilizing equipment and sterilization process |
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| CN201510355985.4A CN104906607B (en) | 2015-06-25 | 2015-06-25 | A kind of multifunction pouring taper sterilizing equipment and sterilization process |
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| CN104906607B true CN104906607B (en) | 2018-11-09 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105253356B (en) * | 2015-11-19 | 2017-10-10 | 北京同仁堂健康药业（福州）有限公司 | A kind of maintenance process of easy bellding Chinese medicine |
| CN106620752A (en) * | 2017-01-05 | 2017-05-10 | 连云港佑源医药设备制造有限公司 | Sterilizing method for low temperature steam sterilized traditional Chinese medicine |
| CN107469113A (en) * | 2017-09-22 | 2017-12-15 | 江西中医药大学 | A kind of Chinese medicine sterilizing methods and horizontal bactericidal unit |
| CN108653757A (en) * | 2018-05-29 | 2018-10-16 | 江西中医药大学 | A kind of horizontal low temperature sterilizing installation and low temperature sterilization method |
| CN109620987B (en) * | 2019-01-25 | 2020-10-27 | 华东理工大学 | Low-temperature intermittent combined sterilization method for traditional Chinese medicine |
| CN109892678B (en) * | 2019-04-02 | 2021-01-26 | 佛山播恩生物科技有限公司 | Feed sterilizing equipment |
| CN110720582A (en) * | 2019-09-23 | 2020-01-24 | 厦门中纺大化纤材料有限公司 | Efficient sterilization method for vacuum circulating ozone |
| CN111066581B (en) * | 2019-12-11 | 2021-12-03 | 山西泓盛农业科技有限公司 | Edible mushroom culture medium sterilization equipment |
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