CN104904713A - Powder-shaped didecyldimethylammonium bromide disinfectant - Google Patents
Powder-shaped didecyldimethylammonium bromide disinfectant Download PDFInfo
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- CN104904713A CN104904713A CN201510381591.6A CN201510381591A CN104904713A CN 104904713 A CN104904713 A CN 104904713A CN 201510381591 A CN201510381591 A CN 201510381591A CN 104904713 A CN104904713 A CN 104904713A
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Abstract
The invention relates to powder-shaped didecyldimethylammonium bromide disinfectant. The powder-shaped didecyldimethylammonium bromide disinfectant is prepared through reacting didecyl methyl tertiary amine with methyl bromide to generate didecyldimethylammonium bromide, reacting with carbamide, drying and smashing. The powder-shaped didecyldimethylammonium bromide disinfectant has advantages that the product appearance is colorless powder, the product can be prepared into tablet, the transportation, carrying and use are very convenient to realize, the advantages are special in the insect disease prevention field, the disinfectant plays a role of fertilizing when carrying out insect disease prevention on the crop, fruit trees, vegetable and the like, and double effects are integrated; the powder-shaped didecyldimethylammonium bromide disinfectant solves the problem that the traditional disinfectant only plays roles of preventing insect and does not play a role of fertilizing for the crop, and moreover, the disinfectant can be prepared into tablet, the transportation, carrying and use are very convenient to realize, many practical problems are solved, and manpower and material resources are saved imperceptibly.
Description
Technical field
The present invention relates to powdery disinfectant preparation, be specifically related to a kind of didecyl Dimethy ammonium bromide powdery disinfectant.
Background technology
The effect that traditional disinfection agent is controlled worm in a crops insect protected and do not applied fertilizer, traditional disinfectant is inconvenient to transport, carry; Do not have a kind of reasonably disinfectant to make simple at present, cost is low, and has the double action of sterilization and fertilising, and facilitates transport to carry.
Summary of the invention
In order to solve the problem, the present invention proposes a kind of didecyl Dimethy ammonium bromide powdery disinfectant, solve traditional disinfection agent control worm in a crops insect protected and do not play the effect of fertilising, and can drug sheet be made, transport, carry with use procedure in very convenient, solve a lot of practical problem, virtually save manpower and materials.
In order to reach foregoing invention object, the present invention proposes following technical scheme:
Didecyl Dimethy ammonium bromide powdery disinfectant, described didecyl Dimethy ammonium bromide powdery disinfectant two ten alkyl monomethyl tertiary amines and monobromo methane reaction generate didecyl Dimethy ammonium bromide, and then react with carbonyl diamide, through drying, pulverize and obtaining.
The technological process of didecyl Dimethy ammonium bromide powdery disinfectant:
The first step: two ten alkyl methyl tertiary amines and monobromo methane reaction, the mol ratio of its reaction is: 1.01-1.05:1, react under base catalyst condition, range of reaction temperature is 65 DEG C-95 DEG C, its operating pressure controls at≤0.3Mpa, reaction time is 4-6 hour, and reaction terminates to be incubated 2-4 hour
Second step: the carbonyl diamide adding 12 moles after first step reaction terminates carries out complex reaction, reaction time 3-5 hour, and then material is sent into baking oven and dry, oven temperature controls at 100 DEG C-110 DEG C;
3rd step, finally carries out being ground into powder or being pressed into tablet dress.
Advantage of the present invention is this product appearance is colourless powder, drug sheet can be made, transport, carry with use procedure in very convenient, the advantage of its uniqueness is had in prevention and elimination of disease and pests, while crops, fruit tree, vegetables etc. carry out prevention and elimination of disease and pests, play the effect of fertilising, have the effect that economic benefits and social benefits are unified; Solve traditional disinfection agent control worm in a crops insect protected and do not play the effect of fertilising, and can drug sheet be made, transport, carry with use procedure in very convenient, solve a lot of practical problem, virtually saved manpower and materials.
Embodiment
Didecyl Dimethy ammonium bromide powdery disinfectant generates didecyl Dimethy ammonium bromide with two ten alkyl monomethyl tertiary amines and monobromo methane reaction, and then react with carbonyl diamide, through drying, pulverize and obtaining.
The technological process of didecyl Dimethy ammonium bromide powdery disinfectant:
The first step: two ten alkyl methyl tertiary amines and monobromo methane reaction, the mol ratio of its reaction is: 1.01-1.05:1, react under base catalyst condition, range of reaction temperature is 65 DEG C-95 DEG C, and its operating pressure controls at≤0.3Mpa, operating pressure can not more than 0.3Mpa, temperature can not more than 95 DEG C, otherwise product colour can deepen, and affect product quality, reaction time is 4-6 hour, and reaction terminates to be incubated 2-4 hour;
Second step: the carbonyl diamide adding 12 moles after first step reaction terminates carries out complex reaction, reaction time 3-5 hour, and then material is sent into baking oven and dry, oven temperature controls at 100 DEG C-110 DEG C.
Finally carry out being ground into powder or being pressed into tablet dress.
The key technical indexes of didecyl Dimethy ammonium bromide:
Chinese: didecyl Dimethy ammonium chloride powdery disinfectant;
English name: Didecyl dimethyl ammonium bromide powder disinfectant two;
Outward appearance and proterties: be colourless powder or colorless plate under normal temperature, completely water-soluble;
Specification: working substance content (%): >=99%;
Moisture (%) :≤1%;
PH value: 5-9.
The problem of didecyl Dimethy ammonium chloride powdery disinfectant feature and solution:
This product appearance is colourless powder, can drug sheet be made, transport, carry with use procedure in very convenient, in prevention and elimination of disease and pests, have the advantage of its uniqueness, while crops, fruit tree, vegetables etc. carry out prevention and elimination of disease and pests, play the effect of fertilising, have the effect that economic benefits and social benefits are unified.
Solve traditional disinfection agent control worm in a crops insect protected and do not play the effect of fertilising, and can drug sheet be made, transport, carry with use procedure in very convenient, solve a lot of practical problem, virtually saved manpower and materials.
The effect of didecyl Dimethy ammonium chloride powdery disinfectant:
The feature of this product is that low concentration can kill various virus fast at normal temperatures, bacterium, mould, fungi and pathogenic microorganisms, hospital can be widely used in, public place, family, pouity dwelling place, animal farm and rear cattle dairy farm etc., particularly to any textile and the equal non-corrosiveness of all kinds of apparatus, bactericidal effect and safety are much better than other general disinfectants, and be that under the condition of 1000PPM, fungicidal effectiveness weakens not at water hardness, still all kinds of pathogenic microorganisms can be killed when organic concentration is 5000PPM, environmental protection is played very large important, other materials are all superior in addition in other purposes such as wood preservation.
Claims (2)
1. didecyl Dimethy ammonium bromide powdery disinfectant, it is characterized in that described didecyl Dimethy ammonium bromide powdery disinfectant two ten alkyl monomethyl tertiary amines and monobromo methane reaction generate didecyl Dimethy ammonium bromide, and then react with carbonyl diamide, through drying, pulverize and obtaining.
2. didecyl Dimethy ammonium bromide powdery disinfectant according to claim 1, is characterized in that the technological process of didecyl Dimethy ammonium bromide powdery disinfectant:
The first step: two ten alkyl methyl tertiary amines and monobromo methane reaction, the mol ratio of its reaction is: 1.01-1.05:1, react under base catalyst condition, range of reaction temperature is 65 DEG C-95 DEG C, its operating pressure controls at≤0.3Mpa, reaction time is 4-6 hour, and reaction terminates to be incubated 2-4 hour;
Second step: the carbonyl diamide adding 12 moles after first step reaction terminates carries out complex reaction, reaction time 3-5 hour, and then material is sent into baking oven and dry, oven temperature controls at 100 DEG C-110 DEG C;
3rd step, finally carries out being ground into powder or being pressed into tablet dress.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510381591.6A CN104904713A (en) | 2015-07-03 | 2015-07-03 | Powder-shaped didecyldimethylammonium bromide disinfectant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510381591.6A CN104904713A (en) | 2015-07-03 | 2015-07-03 | Powder-shaped didecyldimethylammonium bromide disinfectant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104904713A true CN104904713A (en) | 2015-09-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510381591.6A Pending CN104904713A (en) | 2015-07-03 | 2015-07-03 | Powder-shaped didecyldimethylammonium bromide disinfectant |
Country Status (1)
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| CN (1) | CN104904713A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4450174A (en) * | 1982-05-27 | 1984-05-22 | Millmaster Onyx Group, Inc. | Decyl quaternary ammonium compounds |
| RU2158141C1 (en) * | 1999-06-17 | 2000-10-27 | Иванова Елена Борисовна | Disinfecting agent "veltal" |
| RU2217170C2 (en) * | 2002-02-08 | 2003-11-27 | Мельников Глеб Евгеньевич | Disinfecting agent |
| RU2229283C2 (en) * | 2002-07-08 | 2004-05-27 | Иванова Елена Борисовна | Substance of tonic and regenerative action applied in toilet, hygienic and cosmetic preparations |
| CN101914026A (en) * | 2010-08-13 | 2010-12-15 | 如皋市万利化工有限责任公司 | Process for preparing didecyl dimethyl ammonium chloride |
-
2015
- 2015-07-03 CN CN201510381591.6A patent/CN104904713A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4450174A (en) * | 1982-05-27 | 1984-05-22 | Millmaster Onyx Group, Inc. | Decyl quaternary ammonium compounds |
| RU2158141C1 (en) * | 1999-06-17 | 2000-10-27 | Иванова Елена Борисовна | Disinfecting agent "veltal" |
| RU2217170C2 (en) * | 2002-02-08 | 2003-11-27 | Мельников Глеб Евгеньевич | Disinfecting agent |
| RU2229283C2 (en) * | 2002-07-08 | 2004-05-27 | Иванова Елена Борисовна | Substance of tonic and regenerative action applied in toilet, hygienic and cosmetic preparations |
| CN101914026A (en) * | 2010-08-13 | 2010-12-15 | 如皋市万利化工有限责任公司 | Process for preparing didecyl dimethyl ammonium chloride |
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Application publication date: 20150916 |
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| RJ01 | Rejection of invention patent application after publication |