CN104891938A - Environment-friendly fire-resistant light decorative plate and preparation method thereof - Google Patents
Environment-friendly fire-resistant light decorative plate and preparation method thereof Download PDFInfo
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- CN104891938A CN104891938A CN201510259115.7A CN201510259115A CN104891938A CN 104891938 A CN104891938 A CN 104891938A CN 201510259115 A CN201510259115 A CN 201510259115A CN 104891938 A CN104891938 A CN 104891938A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/91—Use of waste materials as fillers for mortars or concrete
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Abstract
The invention discloses an environment-friendly fire-resistant light decorative plate, which comprises the following components, by weight part: 10-18 of plant fiber powder, 2-5 of serpentine powder, 5-10 of alumina, 3-8 of zinc oxide, 2-5 of boron nitride, 2-6 of sedum lineare, 1-3 of hollow glass bead, 1-5 of a cross-linking agent, 10-20 of short glass fiber, 2-6 of porous silicon oxide, 3-10 of magnesium chloride, and 5-10 of sodium pyrophosphate. The invention also discloses a preparation method of the environment-friendly fire-resistant light decorative plate. The fire-resistant light decorative plate provided in the invention is high in fire-resistant level and strength, and good in compactness, contains no harmful substance, and is light, convenient, and environment-friendly.
Description
Technical field:
The present invention relates to decoration material field, be specifically related to a kind of environmental protection fire-resistant light decorative sheet.
Background technology:
Decorative sheet is a kind of artificial board.It is with multiple special paper after chemical treatment, the thermoset laminated plastic made with High Temperature High Pressure cementing agent, plate mask has various wood grain or pattern, and light is smooth, bright in colour attractive in appearance, there is the physicals that higher wear-resisting, heat-resisting, cold-resistant, fire prevention etc. is good simultaneously.Wall, the roof in many senior rooms, make cabinet, cupboard, table, the bed be particular about, the worktable of precision instrument, and the shell of the experiment table in laboratory, televisor, receiving set and other broadcast telecommunication equipment, mostly adopts this novel decorative sheet.
The frequent generation of present fire, mostly causes because lagging material is not fire-resistant; And analyzing caving in of World Trade Centre in the calendar year 2001 U.S. 911 event according to associated specialist is not cause because clash into, but because clash on fire rear caused by support burnt just now.Therefore, the requirement of the country and people to building safety improves constantly, and the fire performance of decorative sheet industry is subject to severe challenge.
Summary of the invention:
The object of this invention is to provide a kind of environmental protection fire-resistant light decorative sheet, its fire-resistant rank is high, and intensity is high, light, and compactness is good, unharmful substance, environmental protection.
Another object of the present invention is to provide the preparation method of this environmental protection fire-resistant light decorative sheet, and its preparation method is simple, easy to operate.
For achieving the above object, the present invention is by the following technical solutions:
A kind of environmental protection fire-resistant light decorative sheet, with parts by weight, comprises following component:
Vegetable fibre powder 10-18 part, serpentine powder 2-5 part,
Aluminum oxide 5-10 part, zinc oxide 3-8 part,
Boron nitride 2-5 part, Linear Stonecrop Herb 2-6 part,
Hollow glass micropearl 1-3 part, linking agent 1-5 part,
Staple glass fibre 10-20 part, porous silica 2-6 part,
Magnesium chloride 3-10 part, trisodium phosphate 5-10 part.
Preferred as technique scheme, a kind of environmental protection fire-resistant light decorative sheet, with parts by weight, comprises following component:
12 parts, vegetable fibre powder, 3 parts, serpentine powder,
8 parts, aluminum oxide, 6 parts, zinc oxide,
Boron nitride 5 parts, Linear Stonecrop Herb 5 parts,
Hollow glass micropearl 2 parts, linking agent 3 parts,
Staple glass fibre 15 parts, porous silica 5 parts,
8 parts, magnesium chloride, trisodium phosphate 10 parts.
Preferred as technique scheme, described vegetable fibre powder is the vegetable fibre powdered material be made up of the stalk stem of the agricultural crop straws such as rice husk, straw, wheat straw, maize straw, Cotton Stalk, wood chip, bamboo bits or other plant, and its size is 200-300 order.
Preferred as technique scheme, the size of described serpentine powder is 20-50nm.
Preferred as technique scheme, described boron nitride is two-dimensional nano sheet, and its nanometer sheet thickness is 20-30nm.
Preferred as technique scheme, the length of described staple glass fibre is 5-10mm.
Preferred as technique scheme, described linking agent is styrene-butadiene-styrene block copolymer.
A preparation method for environmental protection fire-resistant light decorative sheet, comprises the following steps:
(1) by vegetable fibre powder, serpentine powder, aluminum oxide, zinc oxide, boron nitride, hollow glass micropearl, staple glass fibre, porous silica mixing and stirring, mixed powder material is obtained;
(2) Linear Stonecrop Herb chopping and deionized water are mixed, be transferred in autoclave, at 100-120 DEG C, soak 5-10h, be cooled to room temperature, filter, obtain extracting solution, in extracting solution, add magnesium chloride, trisodium phosphate, stir until dissolution of solid, obtain mixing solutions;
(3) the mixed powder material mixing that mixing solutions step (2) obtained and step (1) obtain stirs, add linking agent, after continuing stirring, be transferred to autoclave, at 150-180 DEG C, reaction 10-15h, obtains mixing material;
(4) mixing material that step (4) obtains is put into mould, through 1000-2800t hydropress pressure 3-10min under normal temperature, make sheet material, and then maintenance 5-10h at 80-100 DEG C, obtain environmental protection fire-resistant light decorative sheet.
Preferred as technique scheme, in step (1), the mass ratio of Linear Stonecrop Herb and deionized water is 1:10-15.
Preferred as technique scheme, in step (3), the temperature of described reaction is 180 DEG C, and the time of described reaction is 12h.
Compared with prior art, the present invention has following beneficial effect:
The present invention adopts the compound such as serpentine powdered material, vegetable fibre powder, and crosslinking reaction occurs in autoclave, generates three-dimensional network space structure, there is extremely strong ultimate compression strength, adopt hollow glass micropearl, porous silica equal strength large, the material of light weight, resistivity against fire is good simultaneously;
Adding of Linear Stonecrop Herb, substantially increase the water-fast fire performance of decorative sheet, in addition, decorative sheet provided by the invention, preparation method is simple, and raw material is cheap and easy to get, and cost is low, and this decorative sheet is nontoxic, is conducive to environment protection.
Embodiment:
For a better understanding of the present invention, below by embodiment, the present invention is further described, and embodiment, only for explaining the present invention, can not form any restriction to the present invention.
Embodiment 1
A kind of environmental protection fire-resistant light decorative sheet, with parts by weight, comprises following component:
10 parts, vegetable fibre powder, 2 parts, serpentine powder,
5 parts, aluminum oxide, 3 parts, zinc oxide,
Boron nitride 2 parts, Linear Stonecrop Herb 2 parts,
Hollow glass micropearl 1 part, linking agent 1 part,
Staple glass fibre 10 parts, porous silica 2 parts,
3 parts, magnesium chloride, trisodium phosphate 5 parts.
Its preparation method comprises the following steps:
(1) by vegetable fibre powder, serpentine powder, aluminum oxide, zinc oxide, boron nitride, hollow glass micropearl, staple glass fibre, porous silica mixing and stirring, mixed powder material is obtained;
(2) Linear Stonecrop Herb chopping and deionized water are mixed, be transferred in autoclave, at 100 DEG C, soak 5h, be cooled to room temperature, filter, obtain extracting solution, in extracting solution, add magnesium chloride, trisodium phosphate, stir until dissolution of solid, obtain mixing solutions;
(3) the mixed powder material mixing that mixing solutions step (2) obtained and step (1) obtain stirs, and adds linking agent, is transferred to autoclave after continuing stirring, and at 150 DEG C, reaction 10h, obtains mixing material;
(4) mixing material that step (4) obtains is put into mould, through 1000t hydropress pressure 3min under normal temperature, make sheet material, then maintenance 5h at 80 DEG C, obtain environmental protection fire-resistant light decorative sheet.
Embodiment 2
A kind of environmental protection fire-resistant light decorative sheet, with parts by weight, comprises following component:
18 parts, vegetable fibre powder, 5 parts, serpentine powder,
10 parts, aluminum oxide, 8 parts, zinc oxide,
Boron nitride 5 parts, Linear Stonecrop Herb 6 parts,
Hollow glass micropearl 3 parts, linking agent 5 parts,
Staple glass fibre 20 parts, porous silica 6 parts,
10 parts, magnesium chloride, trisodium phosphate 10 parts.
Its preparation method comprises the following steps:
(1) by vegetable fibre powder, serpentine powder, aluminum oxide, zinc oxide, boron nitride, hollow glass micropearl, staple glass fibre, porous silica mixing and stirring, mixed powder material is obtained;
(2) Linear Stonecrop Herb chopping and deionized water are mixed, be transferred in autoclave, at 120 DEG C, soak 10h, be cooled to room temperature, filter, obtain extracting solution, in extracting solution, add magnesium chloride, trisodium phosphate, stir until dissolution of solid, obtain mixing solutions;
(3) the mixed powder material mixing that mixing solutions step (2) obtained and step (1) obtain stirs, and adds linking agent, is transferred to autoclave after continuing stirring, and at 180 DEG C, reaction 15h, obtains mixing material;
(4) mixing material that step (4) obtains is put into mould, through 2800t hydropress pressure 10min under normal temperature, make sheet material, then maintenance 10h at 100 DEG C, obtain environmental protection fire-resistant light decorative sheet.
Embodiment 3
A kind of environmental protection fire-resistant light decorative sheet, with parts by weight, comprises following component:
12 parts, vegetable fibre powder, 2.5 parts, serpentine powder,
6 parts, aluminum oxide, 4 parts, zinc oxide,
Boron nitride 2.5 parts, Linear Stonecrop Herb 3 parts,
Hollow glass micropearl 1.5 parts, linking agent 2 parts,
Staple glass fibre 12 parts, porous silica 3 parts,
4 parts, magnesium chloride, trisodium phosphate 6 parts.
Its preparation method comprises the following steps:
(1) by vegetable fibre powder, serpentine powder, aluminum oxide, zinc oxide, boron nitride, hollow glass micropearl, staple glass fibre, porous silica mixing and stirring, mixed powder material is obtained;
(2) Linear Stonecrop Herb chopping and deionized water are mixed, be transferred in autoclave, at 103 DEG C, soak 6h, be cooled to room temperature, filter, obtain extracting solution, in extracting solution, add magnesium chloride, trisodium phosphate, stir until dissolution of solid, obtain mixing solutions;
(3) the mixed powder material mixing that mixing solutions step (2) obtained and step (1) obtain stirs, and adds linking agent, is transferred to autoclave after continuing stirring, and at 160 DEG C, reaction 11h, obtains mixing material;
(4) mixing material that step (4) obtains is put into mould, through 1500t hydropress pressure 4min under normal temperature, make sheet material, and then maintenance 6h at 85 DEG C, obtain environmental protection fire-resistant light decorative sheet.
Embodiment 4
A kind of environmental protection fire-resistant light decorative sheet, with parts by weight, comprises following component:
14 parts, vegetable fibre powder, 3 parts, serpentine powder,
7 parts, aluminum oxide, 5 parts, zinc oxide,
Boron nitride 3 parts, Linear Stonecrop Herb 4 parts,
Hollow glass micropearl 2 parts, linking agent 3 parts,
Staple glass fibre 14 parts, porous silica 4 parts,
5 parts, magnesium chloride, trisodium phosphate 7 parts.
Its preparation method comprises the following steps:
(1) by vegetable fibre powder, serpentine powder, aluminum oxide, zinc oxide, boron nitride, hollow glass micropearl, staple glass fibre, porous silica mixing and stirring, mixed powder material is obtained;
(2) Linear Stonecrop Herb chopping and deionized water are mixed, be transferred in autoclave, at 107 DEG C, soak 7h, be cooled to room temperature, filter, obtain extracting solution, in extracting solution, add magnesium chloride, trisodium phosphate, stir until dissolution of solid, obtain mixing solutions;
(3) the mixed powder material mixing that mixing solutions step (2) obtained and step (1) obtain stirs, and adds linking agent, is transferred to autoclave after continuing stirring, and at 165 DEG C, reaction 12h, obtains mixing material;
(4) mixing material that step (4) obtains is put into mould, through 1800t hydropress pressure 5min under normal temperature, make sheet material, and then maintenance 7h at 90 DEG C, obtain environmental protection fire-resistant light decorative sheet.
Embodiment 5
A kind of environmental protection fire-resistant light decorative sheet, with parts by weight, comprises following component:
16 parts, vegetable fibre powder, 3.5 parts, serpentine powder,
8 parts, aluminum oxide, 6 parts, zinc oxide,
Boron nitride 3.5 parts, Linear Stonecrop Herb 5 parts,
Hollow glass micropearl 2.5 parts, linking agent 4 parts,
Staple glass fibre 16 parts, porous silica 5 parts,
7 parts, magnesium chloride, trisodium phosphate 8 parts.
Its preparation method comprises the following steps:
(1) by vegetable fibre powder, serpentine powder, aluminum oxide, zinc oxide, boron nitride, hollow glass micropearl, staple glass fibre, porous silica mixing and stirring, mixed powder material is obtained;
(2) Linear Stonecrop Herb chopping and deionized water are mixed, be transferred in autoclave, at 110 DEG C, soak 8h, be cooled to room temperature, filter, obtain extracting solution, in extracting solution, add magnesium chloride, trisodium phosphate, stir until dissolution of solid, obtain mixing solutions;
(3) the mixed powder material mixing that mixing solutions step (2) obtained and step (1) obtain stirs, and adds linking agent, is transferred to autoclave after continuing stirring, and at 170 DEG C, reaction 13h, obtains mixing material;
(4) mixing material that step (4) obtains is put into mould, through 2000t hydropress pressure 7min under normal temperature, make sheet material, and then maintenance 8h at 90 DEG C, obtain environmental protection fire-resistant light decorative sheet.
Embodiment 6
A kind of environmental protection fire-resistant light decorative sheet, with parts by weight, comprises following component:
17 parts, vegetable fibre powder, 4.5 parts, serpentine powder,
9 parts, aluminum oxide, 7 parts, zinc oxide,
Boron nitride 4.5 parts, Linear Stonecrop Herb 5.5 parts,
Hollow glass micropearl 2.5 parts, linking agent 4.5 parts,
Staple glass fibre 18 parts, porous silica 5.5 parts,
9 parts, magnesium chloride, trisodium phosphate 9 parts.
Its preparation method comprises the following steps:
(1) by vegetable fibre powder, serpentine powder, aluminum oxide, zinc oxide, boron nitride, hollow glass micropearl, staple glass fibre, porous silica mixing and stirring, mixed powder material is obtained;
(2) Linear Stonecrop Herb chopping and deionized water are mixed, be transferred in autoclave, at 115 DEG C, soak 9h, be cooled to room temperature, filter, obtain extracting solution, in extracting solution, add magnesium chloride, trisodium phosphate, stir until dissolution of solid, obtain mixing solutions;
(3) the mixed powder material mixing that mixing solutions step (2) obtained and step (1) obtain stirs, and adds linking agent, is transferred to autoclave after continuing stirring, and at 175 DEG C, reaction 14h, obtains mixing material;
(4) mixing material that step (4) obtains is put into mould, through 2500t hydropress pressure 9min under normal temperature, make sheet material, and then maintenance 9h at 95 DEG C, obtain environmental protection fire-resistant light decorative sheet.
Claims (10)
1. an environmental protection fire-resistant light decorative sheet, is characterized in that, with parts by weight, comprises following component:
Vegetable fibre powder 10-18 part, serpentine powder 2-5 part,
Aluminum oxide 5-10 part, zinc oxide 3-8 part,
Boron nitride 2-5 part, Linear Stonecrop Herb 2-6 part,
Hollow glass micropearl 1-3 part, linking agent 1-5 part,
Staple glass fibre 10-20 part, porous silica 2-6 part,
Magnesium chloride 3-10 part, trisodium phosphate 5-10 part.
2. a kind of environmental protection fire-resistant light decorative sheet as claimed in claim 1, is characterized in that, with parts by weight, comprise following component:
12 parts, vegetable fibre powder, 3 parts, serpentine powder,
8 parts, aluminum oxide, 6 parts, zinc oxide,
Boron nitride 5 parts, Linear Stonecrop Herb 5 parts,
Hollow glass micropearl 2 parts, linking agent 3 parts,
Staple glass fibre 15 parts, porous silica 5 parts,
8 parts, magnesium chloride, trisodium phosphate 10 parts.
3. a kind of environmental protection fire-resistant light decorative sheet as claimed in claim 1, it is characterized in that: described vegetable fibre powder is the vegetable fibre powdered material be made up of the stalk stem of the agricultural crop straws such as rice husk, straw, wheat straw, maize straw, Cotton Stalk, wood chip, bamboo bits or other plant, and its size is 200-300 order.
4. a kind of environmental protection fire-resistant light decorative sheet as claimed in claim 1, is characterized in that: the size of described serpentine powder is 20-50nm.
5. a kind of environmental protection fire-resistant light decorative sheet as claimed in claim 1, it is characterized in that: described boron nitride is two-dimensional nano sheet, its nanometer sheet thickness is 20-30nm.
6. a kind of environmental protection fire-resistant light decorative sheet as claimed in claim 1, is characterized in that: the length of described staple glass fibre is 5-10mm.
7. a kind of environmental protection fire-resistant light decorative sheet as claimed in claim 1, is characterized in that: described linking agent is styrene-butadiene-styrene block copolymer.
8. the preparation method of a kind of environmental protection fire-resistant light decorative sheet as described in as arbitrary in claim 1 to 7, is characterized in that, comprise the following steps:
(1) by vegetable fibre powder, serpentine powder, aluminum oxide, zinc oxide, boron nitride, hollow glass micropearl, staple glass fibre, porous silica mixing and stirring, mixed powder material is obtained;
(2) Linear Stonecrop Herb chopping and deionized water are mixed, be transferred in autoclave, at 100-120 DEG C, soak 5-10h, be cooled to room temperature, filter, obtain extracting solution, in extracting solution, add magnesium chloride, trisodium phosphate, stir until dissolution of solid, obtain mixing solutions;
(3) the mixed powder material mixing that mixing solutions step (2) obtained and step (1) obtain stirs, add linking agent, after continuing stirring, be transferred to autoclave, at 150-180 DEG C, reaction 10-15h, obtains mixing material;
(4) mixing material that step (4) obtains is put into mould, through 1000-2800t hydropress pressure 3-10min under normal temperature, make sheet material, then maintenance 5-10h at 80-100 DEG C, obtain environmental protection fire-resistant light decorative sheet.
9. the preparation method of a kind of environmental protection fire-resistant light decorative sheet as claimed in claim 8, is characterized in that: in step (1), and the mass ratio of Linear Stonecrop Herb and deionized water is 1:10-15.
10. the preparation method of a kind of environmental protection fire-resistant light decorative sheet as claimed in claim 8, is characterized in that: in step (3), and the temperature of described reaction is 180 DEG C, and the time of described reaction is 12h.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2017042281A1 (en) * | 2015-09-10 | 2017-03-16 | Est Innovation Group Ltd | Non-combustible organic material |
CN106634307A (en) * | 2016-12-26 | 2017-05-10 | 大连理工常熟研究院有限公司 | Colorful bioengineering wall coating |
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CN1323218C (en) * | 2005-01-11 | 2007-06-27 | 任文平 | Fiber composite partition wall board |
CN103819107A (en) * | 2014-01-07 | 2014-05-28 | 苏州市兴邦化学建材有限公司 | Half shell fiber concrete additive |
CN103874575A (en) * | 2011-10-12 | 2014-06-18 | 陶氏环球技术有限责任公司 | Panel with fire barrier |
CN103951369A (en) * | 2014-03-28 | 2014-07-30 | 安徽颐鑫节能材料有限公司 | Heat-preservation fireproof board and preparation method thereof |
CN104017413A (en) * | 2014-05-05 | 2014-09-03 | 苏州弗克新型建材有限公司 | Thermal insulation putty for internal walls and application method thereof |
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2015
- 2015-05-20 CN CN201510259115.7A patent/CN104891938A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1323218C (en) * | 2005-01-11 | 2007-06-27 | 任文平 | Fiber composite partition wall board |
CN103874575A (en) * | 2011-10-12 | 2014-06-18 | 陶氏环球技术有限责任公司 | Panel with fire barrier |
CN103819107A (en) * | 2014-01-07 | 2014-05-28 | 苏州市兴邦化学建材有限公司 | Half shell fiber concrete additive |
CN103951369A (en) * | 2014-03-28 | 2014-07-30 | 安徽颐鑫节能材料有限公司 | Heat-preservation fireproof board and preparation method thereof |
CN104017413A (en) * | 2014-05-05 | 2014-09-03 | 苏州弗克新型建材有限公司 | Thermal insulation putty for internal walls and application method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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WO2017042281A1 (en) * | 2015-09-10 | 2017-03-16 | Est Innovation Group Ltd | Non-combustible organic material |
CN106634307A (en) * | 2016-12-26 | 2017-05-10 | 大连理工常熟研究院有限公司 | Colorful bioengineering wall coating |
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Application publication date: 20150909 |