CN104872333A - Manufacture method of cymose buckwheat rhizome seed tea powder - Google Patents
Manufacture method of cymose buckwheat rhizome seed tea powder Download PDFInfo
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- CN104872333A CN104872333A CN201510278365.5A CN201510278365A CN104872333A CN 104872333 A CN104872333 A CN 104872333A CN 201510278365 A CN201510278365 A CN 201510278365A CN 104872333 A CN104872333 A CN 104872333A
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- buckwheat rhizome
- cymose buckwheat
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Abstract
The invention discloses a manufacture method of cymose buckwheat rhizome seed tea powder. The manufacture method comprises the following steps: smashing cymose buckwheat rhizome seed, adding the smashed cymose buckwheat rhizome seed into 80% food-grade ethyl alcohol according to the mass ratio of 1:5, performing ultrasonic treatment in thermostatic waterbath at 40-60 DEG C and 250 w for 60 min, filtering to obtain filtrate, performing digestion on filter residue twice, mixing the filtrate obtained through twice, centrifuging the filtrate in a centrifugal machine at 3500 rpm for 20 min to obtain supernatant liquid, adding maltodextrin and beta-cyclodextrin in the supernatant liquid, and performing spray drying on the mixture to obtain the finished product. By drinking the cymose buckwheat rhizome seed tea powder, inflammation and respiratory diseases can be effectively relieved, and the excellent efficacy of preventing cardiovascular disease can be realized.
Description
Technical field
The present invention relates to the preparation method of a kind of cymose buckwheat rhizome seed tea treasure.
Background technology
Cymose buckwheat rhizome is polygonaceae plant, Fagopyrum, is one of wild-type buckwheat kind for many years.Another name Jinsuoyinkai ', iron-stone, RHIZOMA FAGOPYRI CYMOSI.Containing active ingredients such as rutin, Quercetin and epicatechins in cymose buckwheat rhizome fruit, wherein main based on rutin, Quercetin, epicatechin equal size are very micro-.Active ingredient in cymose buckwheat rhizome fruit mainly concentrates on seed fraction, in pericarp then not containing or content very micro-.
Summary of the invention
The present invention, by a series of processes such as ultrasonic, centrifugal, spraying dry, makes flavonoids useful to human body inside cymose buckwheat rhizome and polyphenols better dissolve in water, so that the nutriment of cymose buckwheat rhizome is fully absorbed by the body, does not cause the waste of resource.
The present invention is realized by the following technical scheme provided:
Make a cymose buckwheat rhizome seed tea treasure's method, step is as follows:
(1), select full seed, drying and not pulverizing containing the cymose buckwheat rhizome seed pulverizer of other impurity, the granularity of the cymose buckwheat rhizome seed after pulverizing is at 90 orders;
(2) food-grade ethanol of 80%, by weight 1: 5 is added, water bath with thermostatic control 40-60 degree Celsius of ultrasonic process, 60min, 250w;
(3) filtered by mixture in (2), filtrate is preserved;
(4) step (3) gained filter residue adds the food-grade ethanol of 80% by weight 1: 5, and water bath with thermostatic control is increased to 55-75 degree Celsius of ultrasonic process, 60min, 250w; Filter afterwards, filtrate is preserved;
(5) filtrate obtained twice merges, and carry out centrifugal treating, centrifugation time is 20min, and revolution is 3500r/min, obtains supernatant liquor;
(6) spraying dry is carried out, maltodextrin, beta-schardinger dextrin-is added in supernatant liquor, the beta-schardinger dextrin-of 0.3 gram of maltodextrin and 0.3 gram is added in the extract of every 100 grams of cymose buckwheat rhizome powder of seeds, EAT 160 degrees Celsius, the highest must not higher than 175 degrees Celsius, temperature of outgoing air is 85 ~ 90 degrees Celsius, material moisture≤5% after dry;
(7) the cymose buckwheat rhizome seed tea treasure after spraying dry packs, and can obtain the precious finished product of cymose buckwheat rhizome seed tea.
The tea treasure drunk made by the present invention can effectively reduce inflammation, breathing problem and have effect of good angiocardiopathy preventing.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail.
Embodiment 1
(1) select full seed, drying and not pulverizing containing the cymose buckwheat rhizome seed pulverizer of other impurity, the granularity of the cymose buckwheat rhizome seed after pulverizing is at 90 orders;
(2) food-grade ethanol (food-grade ethanol of 80% can be joined with aseptic nontoxic alcoholometer) of 80% is added by weight 1: 5, water bath with thermostatic control 45 degrees Celsius of ultrasonic process, 60min, 250w;
(3) filtered by mixture in (2), filtrate is preserved;
(4) step (3) gained filter residue adds the food-grade ethanol of 80% by weight 1: 5, and water bath with thermostatic control is increased to 55 degrees Celsius of ultrasonic process, 60min, 250w; Filter afterwards, filtrate is preserved;
(5) filtrate obtained twice merges, and carry out centrifugal treating, centrifugation time is 20min, and revolution is 3500r/min, obtains supernatant liquor; The supernatant liquor of gained is through thin-layer chromatographic analysis, and containing 3.2 grams of Flavonoid substances in every 120 grams of these supernatant liquors, productive rate is 83.8%.
(6) spraying dry is carried out, maltodextrin, beta-schardinger dextrin-is added in supernatant liquor, the cyclodextrin of 0.3 gram of maltodextrin and 0.3 gram is added in the extract of every 100 grams of cymose buckwheat rhizome powder of seeds, EAT 160 degrees Celsius, the highest must not higher than 175 degrees Celsius, temperature of outgoing air is 85 ~ 90 degrees Celsius, material moisture≤5% after dry;
(7) the cymose buckwheat rhizome seed tea treasure after spraying dry packs, 2 grams every bag, can obtain the precious finished product of cymose buckwheat rhizome seed tea.
Embodiment 2
(1) select full seed, drying and not pulverizing containing the cymose buckwheat rhizome seed pulverizer of other impurity, the granularity of the cymose buckwheat rhizome seed after pulverizing is at 90 orders;
(2) food-grade ethanol (food-grade ethanol of 80% can be joined with aseptic nontoxic alcoholometer) of 80% is added by weight 1: 5, water bath with thermostatic control 60 degrees Celsius of ultrasonic process, 60min, 250w;
(3) filtered by mixture in (2), filtrate is preserved;
(4) step (3) gained filter residue adds the food-grade ethanol of 80% by weight 1: 5, and water bath with thermostatic control is increased to 75 degrees Celsius of ultrasonic process, 60min, 250w; Filter afterwards, filtrate is preserved;
(5) filtrate obtained twice merges, and carry out centrifugal treating, centrifugation time is 20min, and revolution is 3500r/min, obtains supernatant liquor; The supernatant liquor of gained is through thin-layer chromatographic analysis, and containing 3.35 grams of Flavonoid substances in every 120 grams of these supernatant liquors, productive rate is 87.8%.
(6) spraying dry is carried out, maltodextrin, beta-schardinger dextrin-is added in supernatant liquor, the cyclodextrin of 0.3 gram of maltodextrin and 0.3 gram is added in the extract of every 100 grams of cymose buckwheat rhizome powder of seeds, EAT 160 degrees Celsius, the highest must not higher than 175 degrees Celsius, temperature of outgoing air is 85 ~ 90 degrees Celsius, material moisture≤5% after dry;
(7) the cymose buckwheat rhizome seed tea treasure after spraying dry packs, 2 grams every bag, can obtain the precious finished product of cymose buckwheat rhizome seed tea.
Comparative example 1
(1) select full seed, drying and not pulverizing containing the cymose buckwheat rhizome seed pulverizer of other impurity, the granularity of the cymose buckwheat rhizome seed after pulverizing is at 90 orders;
(2) food-grade ethanol of 80% is added by weight 1: 5, water bath with thermostatic control 90 degrees Celsius of ultrasonic process, 60min, 250w;
(3) filtered by mixture in (2), filtrate is preserved;
(4) step (3) gained filter residue repeats lixiviate according to the condition of (2), (3), and filtrate is preserved;
(5) filtrate obtained twice merges, and carry out centrifugal treating, centrifugation time is 20min, and revolution is 3500r/min, obtains supernatant liquor; The supernatant liquor of gained is through thin-layer chromatographic analysis, and containing 1.9 grams of Flavonoid substances in every 120 grams of these supernatant liquors, productive rate is 50%.
(6) spraying dry is carried out, maltodextrin, beta-schardinger dextrin-is added in supernatant liquor, the cyclodextrin of 0.3 gram of maltodextrin and 0.3 gram is added in the extract of every 100 grams of cymose buckwheat rhizome powder of seeds, EAT 160 degrees Celsius, the highest must not higher than 175 degrees Celsius, temperature of outgoing air is 85 ~ 90 degrees Celsius, material moisture≤5% after dry;
(7) the cymose buckwheat rhizome seed tea treasure after spraying dry packs, 2 grams every bag, can obtain the precious finished product of cymose buckwheat rhizome seed tea.
Embodiment 3: the efficacy test of cymose buckwheat rhizome seed tea treasure
(1) choosing the range of age is 20 ~ 65 years old 200 people, wherein respiratory tract infection, unsmooth breath, cough patients 100 example, high fat of blood, hyperpietic 100 example.
(2) crowd that tests respectively drinks the precious solution of one bag of 150ml cymose buckwheat rhizome seed tea 2 months every day sooner or later.
(3) crowd's 2 months Symptoms are tested as follows:
Table 1
Conclusion: known by testing above, the tea treasure drunk made by the present invention can effectively reduce inflammation, breathing problem and have effect of good angiocardiopathy preventing.
The example of more than setting forth further illustrates cymose buckwheat rhizome seed tea treasure and is not only and superior drinks good merchantable brand, has more good health-care efficacy.
Should be understood that, for those of ordinary skills, can be improved according to the above description or convert, and all these improve and convert the protection domain that all should belong to claims of the present invention.
Claims (1)
1. a cymose buckwheat rhizome seed tea treasure's preparation method, is characterized in that, described method, and step is as follows:
(1), select full seed, drying and not pulverizing containing the cymose buckwheat rhizome seed pulverizer of other impurity, the granularity of the cymose buckwheat rhizome seed after pulverizing is at 90 orders;
(2) food-grade ethanol of 80%, by weight 1: 5 is added, water bath with thermostatic control 40-60 degree Celsius of ultrasonic process, 60min, 250w;
(3) filtered by mixture in (2), filtrate is preserved;
(4) step (3) gained filter residue adds the food-grade ethanol of 80% by weight 1: 5, and water bath with thermostatic control is increased to 55-75 degree Celsius of ultrasonic process, 60min, 250w; Filter afterwards, filtrate is preserved;
(5) filtrate obtained twice merges, and carry out centrifugal treating, centrifugation time is 20min, and revolution is 3500r/min, obtains supernatant liquor;
(6) spraying dry is carried out, maltodextrin, beta-schardinger dextrin-is added in supernatant liquor, the beta-schardinger dextrin-of 0.3 gram of maltodextrin and 0.3 gram is added in the extract of every 100 grams of cymose buckwheat rhizome powder of seeds, EAT 160 degrees Celsius, the highest must not higher than 175 degrees Celsius, temperature of outgoing air is 85 ~ 90 degrees Celsius, material moisture≤5% after dry;
(7) the cymose buckwheat rhizome seed tea treasure after spraying dry packs, and can obtain the precious finished product of cymose buckwheat rhizome seed tea.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510278365.5A CN104872333A (en) | 2015-05-28 | 2015-05-28 | Manufacture method of cymose buckwheat rhizome seed tea powder |
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| CN201510278365.5A CN104872333A (en) | 2015-05-28 | 2015-05-28 | Manufacture method of cymose buckwheat rhizome seed tea powder |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105660936A (en) * | 2016-01-28 | 2016-06-15 | 吉林大学 | Method for preparing tea essence from Lycium ruthenicum leaves and Chinese red date peels |
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