CN104817462A - 三异丙醇胺的生产方法 - Google Patents
三异丙醇胺的生产方法 Download PDFInfo
- Publication number
- CN104817462A CN104817462A CN201510220328.9A CN201510220328A CN104817462A CN 104817462 A CN104817462 A CN 104817462A CN 201510220328 A CN201510220328 A CN 201510220328A CN 104817462 A CN104817462 A CN 104817462A
- Authority
- CN
- China
- Prior art keywords
- isopropanolamine
- tri
- ammonia
- reaction
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- SLINHMUFWFWBMU-UHFFFAOYSA-N Triisopropanolamine Chemical compound CC(O)CN(CC(C)O)CC(C)O SLINHMUFWFWBMU-UHFFFAOYSA-N 0.000 title claims abstract description 38
- 238000000034 method Methods 0.000 title abstract description 19
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 135
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 67
- 238000006243 chemical reaction Methods 0.000 claims abstract description 58
- 238000004519 manufacturing process Methods 0.000 claims abstract description 49
- 239000002904 solvent Substances 0.000 claims abstract description 32
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 30
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 claims abstract description 25
- 235000011114 ammonium hydroxide Nutrition 0.000 claims abstract description 24
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims abstract description 16
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 48
- LVTYICIALWPMFW-UHFFFAOYSA-N diisopropanolamine Chemical compound CC(O)CNCC(C)O LVTYICIALWPMFW-UHFFFAOYSA-N 0.000 claims description 22
- 229940043276 diisopropanolamine Drugs 0.000 claims description 22
- HXKKHQJGJAFBHI-UHFFFAOYSA-N 1-aminopropan-2-ol Chemical compound CC(O)CN HXKKHQJGJAFBHI-UHFFFAOYSA-N 0.000 claims description 19
- 239000007921 spray Substances 0.000 claims description 11
- 239000012535 impurity Substances 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000006227 byproduct Substances 0.000 abstract description 16
- 238000005265 energy consumption Methods 0.000 abstract description 11
- 239000000126 substance Substances 0.000 abstract description 4
- 239000004566 building material Substances 0.000 abstract description 2
- 230000003247 decreasing effect Effects 0.000 abstract 2
- 239000012295 chemical reaction liquid Substances 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 241000350481 Pterogyne nitens Species 0.000 description 48
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 21
- 239000000047 product Substances 0.000 description 18
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 12
- 239000007789 gas Substances 0.000 description 10
- 239000006096 absorbing agent Substances 0.000 description 9
- 239000004568 cement Substances 0.000 description 7
- 239000003245 coal Substances 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- 238000002485 combustion reaction Methods 0.000 description 6
- 239000000945 filler Substances 0.000 description 6
- 239000003546 flue gas Substances 0.000 description 6
- 230000035484 reaction time Effects 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 230000007613 environmental effect Effects 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 238000003912 environmental pollution Methods 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- -1 petrohol amine Chemical class 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000006837 decompression Effects 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 238000004807 desolvation Methods 0.000 description 2
- 229910001873 dinitrogen Inorganic materials 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000004567 concrete Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 239000011440 grout Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000012453 solvate Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510220328.9A CN104817462B (zh) | 2015-05-04 | 2015-05-04 | 三异丙醇胺的生产方法 |
Applications Claiming Priority (1)
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CN201510220328.9A CN104817462B (zh) | 2015-05-04 | 2015-05-04 | 三异丙醇胺的生产方法 |
Publications (2)
Publication Number | Publication Date |
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CN104817462A true CN104817462A (zh) | 2015-08-05 |
CN104817462B CN104817462B (zh) | 2016-07-06 |
Family
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Family Applications (1)
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CN201510220328.9A Active CN104817462B (zh) | 2015-05-04 | 2015-05-04 | 三异丙醇胺的生产方法 |
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CN (1) | CN104817462B (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105061226A (zh) * | 2015-08-04 | 2015-11-18 | 茂名云龙工业发展有限公司 | 一种无催化剂生产二乙醇单异丙醇胺的工业连续化生产方法 |
CN105130826A (zh) * | 2015-08-04 | 2015-12-09 | 茂名云龙工业发展有限公司 | 一种无催化剂的连续生产二乙醇单异丙醇胺的工业化生产方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1803762A (zh) * | 2006-01-01 | 2006-07-19 | 抚顺佳化聚氨酯有限公司 | 一种三异丙醇胺的合成装置及合成方法 |
SK932005A3 (sk) * | 2005-08-22 | 2007-03-01 | Novácke Chemické Závody, A. S. | Bezodpadový spôsob výroby triizoprapanolamínu |
-
2015
- 2015-05-04 CN CN201510220328.9A patent/CN104817462B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SK932005A3 (sk) * | 2005-08-22 | 2007-03-01 | Novácke Chemické Závody, A. S. | Bezodpadový spôsob výroby triizoprapanolamínu |
CN1803762A (zh) * | 2006-01-01 | 2006-07-19 | 抚顺佳化聚氨酯有限公司 | 一种三异丙醇胺的合成装置及合成方法 |
Non-Patent Citations (1)
Title |
---|
黄永春 等: "甲醇中用氨和环氧丙烷合成异丙醇胺", 《南京化工大学学报》 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105061226A (zh) * | 2015-08-04 | 2015-11-18 | 茂名云龙工业发展有限公司 | 一种无催化剂生产二乙醇单异丙醇胺的工业连续化生产方法 |
CN105130826A (zh) * | 2015-08-04 | 2015-12-09 | 茂名云龙工业发展有限公司 | 一种无催化剂的连续生产二乙醇单异丙醇胺的工业化生产方法 |
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Publication number | Publication date |
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CN104817462B (zh) | 2016-07-06 |
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Effective date of registration: 20160712 Address after: Meishan City, Sichuan Province town south 620460 Qingshen County Daxing village 2 groups Qingshen Xin building materials limited company command Patentee after: QINGSHEN XINTONGLING BUILDING MATERIAL Co.,Ltd. Address before: Xiangfan City, Hubei Province, Yicheng 441403 Helei Lei Yan Da Dao Xin Hubei and Vientiane Technology Co. Ltd. Patentee before: HUBEI XINTONGLING VIENTIANE TECHNOLOGY CO.,LTD. |
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Effective date of registration: 20170316 Address after: Xiangfan City, Hubei Province, Yicheng 441403 Helei Lei Yan Da Dao Xin Hubei and Vientiane Technology Co. Ltd. Patentee after: HUBEI XINTONGLING VIENTIANE TECHNOLOGY CO.,LTD. Address before: Meishan City, Sichuan Province town south 620460 Qingshen County Daxing village 2 groups Qingshen Xin building materials limited company command Patentee before: QINGSHEN XINTONGLING BUILDING MATERIAL Co.,Ltd. |
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Address after: 441400 Leihe Leiyan Avenue, Yicheng, Xiangyang City, Hubei Province Patentee after: Xiangyang conch New Material Technology Co.,Ltd. Address before: Xiangfan City, Hubei Province, Yicheng 441403 Helei Lei Yan Da Dao Xin Hubei and Vientiane Technology Co. Ltd. Patentee before: HUBEI XINTONGLING VIENTIANE TECHNOLOGY CO.,LTD. |
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Effective date of registration: 20201111 Address after: Room 208, building 1, No.9, Wanjiang Avenue, Jiangbei industrial concentration zone, Wuhu City, Anhui Province 241000 Patentee after: Anhui Conch New Materials Technology Co.,Ltd. Patentee after: Xiangyang conch New Material Technology Co.,Ltd. Address before: 441400 Leihe Leiyan Avenue, Yicheng, Xiangyang City, Hubei Province Patentee before: Xiangyang conch New Material Technology Co.,Ltd. |
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Address after: 241000 No. 1-301, Area G, Construction Headquarters, Jiangbei New Area, Wuhu City, 150 meters south of Tongjiang Avenue, Jiangbei New Area, Wanjiang New Industry Cluster (except the trusteeship area), Wuhu City Patentee after: Anhui Conch Material Technology Co.,Ltd. Patentee after: Xiangyang conch New Material Technology Co.,Ltd. Address before: Room 208, No. 1 Building, No. 9 Wanjiang Avenue, Jiangbei Industrial Concentration Area, Wuhu City, Anhui Province Patentee before: Anhui Conch New Materials Technology Co.,Ltd. Patentee before: Xiangyang conch New Material Technology Co.,Ltd. |
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