CN104815009B - Whole strain saline cistanche habitat processing method - Google Patents
Whole strain saline cistanche habitat processing method Download PDFInfo
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Abstract
The present invention relates to a kind of whole strain saline cistanche habitat processing method, the drying means of the saline cistanche includes：Whole strain saline cistanche is steamed into 20-30 minutes with vapor under normal pressure；Whole strain saline cistanche after steaming is dried.The whole strain saline cistanche habitat processing method of the present invention steams the activity for effectively inhibiting enzyme and microorganism by high temperature, reduce going mouldy for fresh whole strain saline cistanche, not only substantially reduce the drying time of medicinal material, also the exterior quality and intrinsic activity component content of saline cistanche are improved on the whole, easily operated and the method for the invention is simple and easy, cost is cheap, the production application after a large amount of fresh herba cistanches are excavated in medicinal material original producton location is especially suitable for, while is also convenient for the transport and storage of medicinal material.
Description
Technical field
The present invention relates to a kind of processing method of Chinese medicine, more particularly to one kind improve whole strain saline cistanche exterior quality with
The habitat processing method of intrinsic activity component content.
Background technology
Saline cistanche Cistanche deserticola Y.C.Ma are Orobanchaceae (Orobanchaceae) Cistanche deserticola
(Cistanche Hoffing.et Link) perennial parasitic herbaceous plant, is used as medicine with dry zone scale leaf fleshy stem, can kidney tonifying
Sun, benefiting essence-blood, moisturize logical intestines.Modern medicine study shows that it has anti-aging, antifatigue and raising immunity and other effects.Therefore
No matter in Market of Chinese Materia Medica or in health-product market, saline cistanche is all in occupation of important position.
Modern pharmacological research confirms benzyl carbinol glycosides and polysaccharide is the main active of saline cistanche performance drug effect.Wherein, it is loose
Fruit chrysanthemum glycosides and acteoside are the main actives of benzyl carbinol glycosides, and《Pharmacopoeia of People's Republic of China》In versions in 2010
The index composition of saline cistanche.The primary product form of saline cistanche is dry whole strain fleshy stem, not only can directly pack and sell
Sell, can also be by running through, cutting into slices, being dried to obtain saline cistanche piece.
The habitat processing method of saline cistanche is mainly the research to saline cistanche fresh slices at present：(the patent applications such as Guo Yuhai
Publication No. CN102526212A) and Jiang Yong etc. (patent application publication CN104138420A) report new technology and apply to first
Saline cistanche piece dries processing；Tu Pengfei etc. (license notification number CN1284556C) is killed using hot-water soak to saline cistanche piece
Enzyme is so as to improving echinacoside content；(the patent application publications such as (patent application publication CN1823914A), Lei Li such as stifled year life
Number CN101485731A) and Geng Zongcheng etc. (patent application publication CN104127506A) investigated standing time, section comprehensively
Thickness, kill the influence of enzyme mode and drying mode to benzyl carbinol glycoside content.But because saline cistanche picking time is shorter, section adds
Work occupied ground is big, time-consuming to take a lot of work, and therefore, after a large amount of fresh herba cistanches are excavated in medicinal material original producton location, it is still main that whole strain, which is dried,
Form processing.In whole strain drying process, Individual Size, if suppression enzyme, drying mode etc. can influence the activity of saline cistanche into
Divide content and exterior quality, so as to influence the medicinal effects of saline cistanche.Fresh herba cistanches fleshy stem volume is big, and water content is high
(70%-85%), sugar content height (27%-46%), therefore the drying means slow-drying dried using traditional natural (is typically needed
Take 2-4 months), enzyme digestion reaction and mouldy easily occurs during drying, the exterior quality and active component for reducing saline cistanche contain
Amount, it saline cistanche is all rotted, cause wastage of material and serious financial consequences.It can be seen that whole strain Habitat producing is located at meat
The source link of desert cistanche quality of medicinal material control, directly decide the quality of saline cistanche medicinal material.
The research report of the whole strain processing method of saline cistanche is had not yet to see, is more had no about whole strain drying and chip drying
The comparative study report that mode influences on saline cistanche quality.The extensive application in actual production is processed for whole strain at present, urgently
A kind of reasonable processing technology for being adapted to whole strain saline cistanche need to be studied, is contained with improving the appearance character of saline cistanche and intrinsic activity composition
Amount.
The content of the invention
It is an object of the present invention to provide a kind of whole strain saline cistanche habitat processing method, effectively overcomes the whole strain saline cistanche of prior art
Slow-drying, easily mouldy, the reduction technological deficiency such as exterior quality and intrinsic activity composition during natural drying.
To achieve the above object, the invention provides a kind of drying means of saline cistanche, including：
Whole strain saline cistanche is steamed into 20-30 minutes with vapor under normal pressure；
Whole strain saline cistanche after steaming is dried.
Preferably, the whole strain saline cistanche includes whole strain saline cistanche carrying out classification step before steaming step.
It is described that whole strain saline cistanche is steamed into 20-30 minutes step specially by I grade of whole strain meat desert with vapor under normal pressure
Rong is steamed 30 minutes with vapor under normal pressure, or II grade of whole strain saline cistanche is steamed 20 minutes with vapor under normal pressure, or
III grade of whole strain saline cistanche is steamed 20 minutes with vapor under normal pressure.
Specifically, the water content of whole strain saline cistanche is 0-10% after the drying step.
To achieve the above object, present invention also offers a kind of processing method of saline cistanche, including：
Whole strain saline cistanche is pre-processed；
Pretreated whole strain saline cistanche is steamed into 20-30 minutes with vapor under normal pressure；
Whole strain saline cistanche after steaming is dried.
Further, the pretreatment includes cleaning and/or removing inflorescence.
Preferably, include whole strain saline cistanche carrying out classification step before the pretreated whole strain saline cistanche steams step
Suddenly.
It is described that pretreated whole strain saline cistanche is steamed to 20-30 minutes step specially general with vapor under normal pressure
Pretreated I grade of whole strain saline cistanche is steamed 30 minutes with vapor under normal pressure, or by pretreated II grade whole strain meat desert
Rong is steamed 20 minutes with vapor under normal pressure, or pretreated III grade whole strain saline cistanche is steamed under normal pressure with vapor
20 minutes.
Specifically, the water content of whole strain saline cistanche is 0-10% after the drying step.
Preferably, whole strain saline cistanche after drying is included after the drying step and carries out packaging step.
The invention provides a kind of whole strain saline cistanche habitat processing method, there is advantages below：
1st, drying time is shortened.Whole strain saline cistanche generally requires 2-4 months during natural drying, and the whole strain of the present invention
Moisture declines 14%-22.6% immediately after saline cistanche habitat processing method steams 20-30 minutes with vapor, it is only necessary to dries
Saline cistanche water content can be made to be reduced to less than 10% within 25-40 days, substantially reduce the processing of crude drugs cycle, improve productivity,
It is also convenient for transporting and stores simultaneously.
2nd, economic loss is reduced.The whole strain saline cistanche habitat processing method of the present invention is steamed by vapor effectively inhibits enzyme
With the activity of microorganism, reduce going mouldy for fresh whole strain saline cistanche, while save drying process energy expenditure, natural ring
Protect.
3rd, intrinsic activity component content is improved.The whole strain saline cistanche habitat processing method of the present invention can make Echinacea purpurea in saline cistanche
Glycosides (also known as echinacosid, Echinacea glycosides, Echinacea glycosides) and acteoside (also known as acteoside, Syring vulgaris phenolic glycoside, Verbena officinalis
Glycosides, Verbascoside, acteoside) total content averagely improve 174%, polyoses content averagely improves 14%, improves on the whole
The medical value of saline cistanche.
4th, exterior quality is lifted.The whole strain saline cistanche outward appearance obtained through the whole strain saline cistanche habitat processing method of the present invention is more
Pitch-dark shinny, soft texture, bar shaped is straight, and its exterior quality is closer to the top grade " oily desert cistanche " in saline cistanche, economic benefit
Significantly.
5th, the whole strain saline cistanche habitat processing method of the present invention is simple and easy, and easily operated, cost is cheap, is especially suitable for a large amount of
Production application of the fresh herba cistanches after the excavation of medicinal material original producton location.
Below by drawings and examples, technical scheme is described in further detail.
Brief description of the drawings
Fig. 1 is the drying means flow chart of saline cistanche of the present invention；
Fig. 2 is the processing method flow chart of saline cistanche of the present invention.
Embodiment
Fig. 1 is the drying means flow chart of saline cistanche of the present invention, is specially：
Step A1, whole strain saline cistanche is steamed into 20-30 minutes with vapor under normal pressure；
Step A2, the whole strain saline cistanche after steaming is dried.
In the above-mentioned technical solutions, can also include before step A1：Whole strain saline cistanche is classified.The water steams
Temperature degree can be 90-100 DEG C, and the normal pressure pressure can be 100-115KPa.
The technical scheme of the drying means of saline cistanche of the present invention is further illustrated below by specific embodiment.
The drying means first embodiment of saline cistanche of the present invention
Step A101, whole strain saline cistanche is steamed 20 minutes with vapor under normal pressure；
Step A102, the whole strain saline cistanche after steaming is dried, and its water content is down to less than 10%.
The drying means second embodiment of saline cistanche of the present invention
Step A201, whole strain saline cistanche is steamed 25 minutes with vapor under normal pressure；
Step A202, the whole strain saline cistanche after steaming is dried, and its water content is down to less than 10%.
The drying means 3rd embodiment of saline cistanche of the present invention
Step A301, whole strain saline cistanche is steamed 30 minutes with vapor under normal pressure；
Step A302, the whole strain saline cistanche after steaming is dried, and its water content is down to less than 10%.
Saline cistanche of the present invention drying means first embodiment into 3rd embodiment, the steam temperature can be
90-100 DEG C, the normal pressure pressure can be 100-115KPa.
The drying means fourth embodiment of saline cistanche of the present invention
Step A401, fresh whole strain saline cistanche is classified, I grade of saline cistanche fleshy stem is spread in a single layer in there is hole stainless
On steel material disc, steamed with 100 DEG C of vapor of temperature under normal pressure 30 minutes；
Step A402, I grade of saline cistanche fleshy stem after steaming is spread rapidly on bamboo mat is dried, and is put into airing field solarization
It is dry, its water content is down to less than 10%.
In the present embodiment, compared with directly shining drying method, Echinacea purpurea in I grade of saline cistanche medicinal material after being dried using the present invention
Glycosides and acteoside total content can improve 150.26%, and polyoses content can improve 33.73%, and whole strain saline cistanche outward appearance is more black
Dark hair is bright, soft texture, and bar shaped is straight.
The embodiment of drying means the 5th of saline cistanche of the present invention
Step A501, fresh whole strain saline cistanche is classified, II grade of saline cistanche fleshy stem is spread in a single layer Yu Youkong not
Become rusty on steel material disc, steamed with 100 DEG C of vapor of temperature under normal pressure 20 minutes；
Step A502, II grade of saline cistanche fleshy stem after steaming is spread rapidly on bamboo mat is dried, and is put into airing field solarization
It is dry, its water content is down to less than 10%.
In the present embodiment, compared with directly shining drying method, pine nut in II grade of saline cistanche medicinal material after being dried using the present invention
Chrysanthemum glycosides and acteoside total content can improve 328.66%, and polyoses content can improve 0.26%, and whole strain saline cistanche outward appearance is more
Pitch-dark shinny, soft texture, bar shaped is straight.
The drying means sixth embodiment of saline cistanche of the present invention
Step A601, fresh whole strain saline cistanche is classified, III grade of saline cistanche fleshy stem is spread in a single layer Yu Youkong not
Become rusty on steel material disc, steamed with 100 DEG C of vapor of temperature under normal pressure 20 minutes；
Step A602, III grade of saline cistanche fleshy stem after steaming is spread rapidly on bamboo mat is dried, and is put into airing field solarization
It is dry, its water content is down to less than 10%.
In the present embodiment, compared with directly shining drying method, pine nut in III grade of saline cistanche medicinal material after being dried using the present invention
Chrysanthemum glycosides and acteoside total content can improve 44.38%, and polyoses content can improve 8.19%, and whole strain saline cistanche outward appearance is more black
Dark hair is bright, soft texture, and bar shaped is straight.
Saline cistanche of the present invention drying means fourth embodiment into sixth embodiment, the steam temperature can also
For 90,91,92,93,94,95,96,97,98 or 99 DEG C, the normal pressure pressure can be 100,101,102,103,104,105,
106th, 107,108,109,110,111,112,113,114 or 115KPa.Step A401, it is fresh in step A501 and step A601
Whole strain saline cistanche fleshy stem indication range as shown in table 1 is classified, and with fresh weight and the main index of a diameter of classification, length is than upper
Define the level by above-mentioned two indexs when stating the low one-level of two indexs, then press than above-mentioned two during lower than the above-mentioned two indexs two-stage of length
Index reduces one-level to define the level.(index parameter of table 1 derives from the 285 plants of fresh herba cistanches determined at random, is clustered using K
The result arrived, wherein I grade 68 plants, II grade 120 plants, III grade 97 plants)
The fresh whole strain saline cistanche graded index of table 1
Fig. 2 is the processing method flow chart of saline cistanche of the present invention, is specially：
Step B1, whole strain saline cistanche is pre-processed；
Step B2, pretreated whole strain saline cistanche is steamed into 20-30 minutes with vapor under normal pressure；
Step B3, the whole strain saline cistanche after steaming is dried.
In the above-mentioned technical solutions, can also include before step B1：Whole strain saline cistanche is classified；The pre- place
Reason is specially to clean and/or remove inflorescence.It can also include after step B3：Whole strain saline cistanche after drying is packed.
The steam temperature can be 90-100 DEG C, and the normal pressure pressure can be 100-115KPa.
The technical scheme of the processing method of saline cistanche of the present invention is further illustrated below by specific embodiment.
The processing method first embodiment of saline cistanche of the present invention
Step B101, whole strain saline cistanche is pre-processed；
Step B102, pretreated whole strain saline cistanche is steamed 20 minutes with vapor under normal pressure；
Step A103, the whole strain saline cistanche after steaming is dried, and its water content is down to less than 10%.
The processing method second embodiment of saline cistanche of the present invention
Step B201, whole strain saline cistanche is pre-processed；
Step B202, pretreated whole strain saline cistanche is steamed 25 minutes with vapor under normal pressure；
Step B203, the whole strain saline cistanche after steaming is dried, and its water content is down to less than 10%.
The processing method 3rd embodiment of saline cistanche of the present invention
Step B301, whole strain saline cistanche is pre-processed；
Step B302, pretreated whole strain saline cistanche is steamed 30 minutes with vapor under normal pressure；
Step B303, the whole strain saline cistanche after steaming is dried, and its water content is down to less than 10%.
Saline cistanche of the present invention processing method first embodiment into 3rd embodiment, the steam temperature can be
90-100 DEG C, the pressure of the normal pressure can be 100-115KPa.
The processing method fourth embodiment of saline cistanche of the present invention
Step B401, fresh whole strain saline cistanche is classified, chosen without obvious wound, no disease and pests harm, complete I grade of meat
Desert cistanche fleshy stem, water wash the silt for being attached to its surface, cut inflorescence head；
Step B402, the saline cistanche fleshy stem after above-mentioned steps are handled is spread in a single layer in having on the stainless steel material disc of hole,
Steamed with 100 DEG C of vapor of temperature under normal pressure 30 minutes；
Step B403, I grade of saline cistanche fleshy stem after steaming is spread rapidly on bamboo mat is dried, and is put into airing field solarization
It is dry, its water content is down to less than 10%；
Step B404, the whole strain bundling of saline cistanche or single vacuum fine packaging are sold after drying.
In the present embodiment, compared with directly shining drying method, Echinacea purpurea in the I grade of saline cistanche medicinal material processed using the present invention
Glycosides and acteoside total content can improve 150.26%, and polyoses content can improve 33.73%, and whole strain saline cistanche outward appearance is more black
Dark hair is bright, soft texture, and bar shaped is straight.
The embodiment of processing method the 5th of saline cistanche of the present invention
Step B501, fresh whole strain saline cistanche is classified, chosen without obvious wound, no disease and pests harm, complete II grade
Saline cistanche fleshy stem, water wash the silt for being attached to its surface, cut inflorescence head；
Step B502, the saline cistanche fleshy stem after above-mentioned steps are handled is spread in a single layer in having on the stainless steel material disc of hole,
Steamed with 100 DEG C of vapor of temperature under normal pressure 20 minutes；
Step B503, II grade of saline cistanche fleshy stem after steaming is spread rapidly on bamboo mat is dried, and is put into airing field solarization
It is dry, its water content is down to less than 10%；
Step B504, the whole strain bundling of saline cistanche or single vacuum fine packaging are sold after drying.
In the present embodiment, compared with directly shining drying method, pine nut in the II grade of saline cistanche medicinal material processed using the present invention
Chrysanthemum glycosides and acteoside total content can improve 328.66%, and polyoses content can improve 0.26%, and whole strain saline cistanche outward appearance is more
Pitch-dark shinny, soft texture, bar shaped is straight.
The processing method sixth embodiment of saline cistanche of the present invention
Step B601, fresh whole strain saline cistanche is classified, chosen without obvious wound, no disease and pests harm, complete III grade
Saline cistanche fleshy stem, water wash the silt for being attached to its surface, cut inflorescence head；
Step B602, the saline cistanche fleshy stem after above-mentioned steps are handled is spread in a single layer in having on the stainless steel material disc of hole,
Steamed with 100 DEG C of vapor of temperature under normal pressure 20 minutes；
Step B603, III grade of saline cistanche fleshy stem after steaming is spread rapidly on bamboo mat is dried, and is put into airing field solarization
It is dry, its water content is down to less than 10%；
Step B604, the whole strain bundling of saline cistanche or single vacuum fine packaging are sold after drying.
In the present embodiment, compared with directly shining drying method, pine nut in the III grade of saline cistanche medicinal material processed using the present invention
Chrysanthemum glycosides and acteoside total content can improve 44.38%, and polyoses content can improve 8.19%, and whole strain saline cistanche outward appearance is more black
Dark hair is bright, soft texture, and bar shaped is straight.
Saline cistanche of the present invention processing method fourth embodiment into sixth embodiment, the steam temperature can also
For 90,91,92,93,94,95,96,97,98 or 99 DEG C, the normal pressure pressure can be 100,101,102,103,104,105,
106th, 107,108,109,110,111,112,113,114 or 115KPa.Step B401, it is fresh in step B501 and step B601
Whole strain saline cistanche fleshy stem indication range as shown in table 1 is classified, and with fresh weight and the main index of a diameter of classification, length is than upper
Define the level by above-mentioned two indexs when stating the low one-level of two indexs, then press than above-mentioned two during lower than the above-mentioned two indexs two-stage of length
Index reduces one-level to define the level.
Technique effect of the method for the invention to the whole strain saline cistanche quality of raising is evaluated below by specific experiment.
1 assay method
1.1 benzyl carbinol glycoside assays
It is prepared by reference substance solution：Accurately weighed echinacoside reference substance 5.08mg, acteoside reference substance 4.14mg and
2 '-acetyl group acteoside reference substance 5.12mg is in 5mL volumetric flasks, cistanoside A reference substance 5.17mg and different verbascose
Glycosides reference substance 5.36mg is in 10mL volumetric flasks, and 60% methanol of addition, which shakes up, is settled to scale, as reference substance storing solution.Essence respectively
It is close to measure echinacoside 2mL, acteoside 2.5mL, 2 '-acetyl group acteoside 2mL, boschnaloside 1mL, different feltwort
Glucosides 1mL adds 60% methanol constant volume to 10mL in 10mL volumetric flasks, obtains 5 composition mixed reference substance solutions.
Chromatographic condition：Chromatographic column：Merck Purospher STAR RP-C18 posts (250mm × 4.6mm, 5 μm), column temperature
30℃.Flow velocity 1mL/min.Mobile phase：The aqueous formic acid of methanol -0.1%, eluted by such as Gradient：0-10min, methanol-
0.1% aqueous formic acid (28:72, v/v)；10-30min, the aqueous formic acid of methanol-0.1% (28:72, v/v) linear change arrives
The aqueous formic acid of methanol -0.1% (38:62, v/v), 30-45min, the aqueous formic acid of methanol-0.1% (38:62, v/v).
It is prepared by need testing solution：Test sample powder (crossing No. four sieves) 0.5g is taken, it is accurately weighed, put in 50mL volumetric flasks, add
Enter 60% methanol 25mL, close plug, shake up, weighed weight, be ultrasonically treated 30min, let cool, then weighed weight, add 60% methanol
To supply the weight of less loss, shake up, stand, take supernatant, filter, take subsequent filtrate to cross 0.45 μm of miillpore filter, as test sample
Solution.
Solution content determines：Sample introduction test sample and each 10 μ l of reference substance solution respectively, liquid chromatograph is injected, in 330nm
Lower each component content of detection.
1.2 determination of polysaccharide
It is prepared by reference substance solution：Precision weighs glucose 10.44mg, adds distilled water and dissolves and be settled to 100mL browns
Volumetric flask.
It is prepared by need testing solution：Test sample powder 0.5g is taken, it is accurately weighed, put in conical flask, add 80% ethanol 25mL,
Close plug, shakes up, and is ultrasonically treated 30min, filters while hot, repeats extraction once.Filter residue volatilizees after dry ethanol, adds water 25mL, close plug,
Shake up, be ultrasonically treated 30min, filter while hot, repeat extraction once.Merging filtrate, and be settled in 50mL volumetric flasks, shake up,
Precision draws 5mL, adds water constant volume to be shaken up into 25mL volumetric flasks, to be measured.
Solution content determines：Precision draws reference substance and each 1mL of need testing solution, puts in dry test tube, adds water to respectively
2mL, 6% phenol reagent 1mL is added, is shaken up；Concentrated sulfuric acid 5mL is rapidly added, 5min is shaken, boiling water bath heating 15min, puts
It is cold, while a blank is done with distilled water, solution is existed in cuvette with ultraviolet-visible spectrophotometer after adding appropriate reaction
Absorbance is detected under 490nm.
1.3 powder determination of colority
Colorimeter, which is used for medicinal material color measuring, has the characteristics of objective, accurate, and according to bear cry of certain animals etc., (bear is chanted, Xiao Xiao, Yan Yong
It is red, wait effective ingredient of honeysuckle contents of the based on colorimetric analysis principle and color value correlation research [J] China traditional Chinese medicine and pharmacy
Periodical, 2013 (03):667-670.) assay method measure saline cistanche powder colourity.
2 technique effects
2.1 steam treatments influence on whole strain saline cistanche quality
Modern study shows that echinacoside and acteoside content are not only in Cistanche deserticola (saline cistanche not of the same race
C.deserticola, halophilous herbage C.salsa, Cistanche tubulosa C.tubulosa and husky desert cistanche C.sinensis) between it is poor
It is different notable, there is significant difference between different sources of the same race, growth year, collecting season and position.Therefore《The Chinese people
Republic's pharmacopeia》Version regulation saline cistanche in 2010 must not be less than 3g kg containing echinacoside and acteoside total amount-1, and pipe is spent
Saline cistanche must not be less than 15g kg containing echinacoside and acteoside total amount-1.Such as Wang Li nanmus etc. are to the same as a collection of saline cistanche medicine
Material research finds that echinacoside and acteoside total content are in medicinal material upper part on the premise of all treatment conditions are all consistent
Only 3.3g kg-1, and in medicinal material bottom up to 32.0g kg-1, both differ nearly 10 times.
In view of the inherent component content of saline cistanche individual is widely different, result is influenceed to exclude individual difference, by green meat
The uniform rip cutting of desert cistanche into two parts, directly dry by a part, and another part was according to the method for the invention steam treatment 30 minutes
After dry, respectively determine 2 parts of samples external and interior quality, experimental result is as shown in table 2 and table 3.Following technique effects are special
Not Shi Yongyu saline cistanche of the present invention drying means 3rd embodiment and fourth embodiment, the processing method of saline cistanche of the present invention
Three embodiments and fourth embodiment.Active component content (the g.kg in following technique effects-1)=active component percentage composition
(%) × 10.
The experimental result that the steam treatment of table 2 influences on saline cistanche exterior quality
The experimental result that the steam treatment of table 3 influences on saline cistanche active component content
The result of table 2 shows：Obtained saline cistanche is dried after being steamed by the method for the invention, its integral color is obvious
It is deeper than and directly dries obtained saline cistanche, powder color is also more bright.
The result of table 3 shows：Obtained saline cistanche is dried after being steamed by the method for the invention, its active component pine nut
Chrysanthemum glycosides, acteoside, different acteoside, 2'- acetyl group acteoside, polyoses content also significantly greater than directly dry institute
The saline cistanche of acquisition.
In summary, at source whole strain saline cistanche is carried out steam treatment can preferably ensure in it and exterior quality.
Influence of 2.2 steaming times to the whole strain saline cistanche of different brackets
According to the grade scale shown in table 1, choosing 2 factors of the whole strain saline cistanche progress of 3 grades, (saline cistanche grade, is steamed
Time) 3 horizontal (I grade/II grade/III grade, 10min/20min/30min) factorial experiments, determine the active component of whole strain saline cistanche
Content, experimental result is as shown in table 4, table 5 and table 6.Drying means of following technique effects especially suitable for saline cistanche of the present invention
First embodiment and sixth embodiment, the processing method first embodiment of saline cistanche of the present invention and sixth embodiment.
4 I grades of saline cistanches of table each content determinations of active component result in the case where steaming different time
5 II grades of saline cistanches of table each content determinations of active component result in the case where steaming different time
6 III grades of saline cistanches of table each content determinations of active component result in the case where steaming different time
See on the whole, each component content is significantly higher than respectively after 3 grade saline cistanches steam does not steam the equal of processing
Level saline cistanche.As shown in table 4, after I grade of saline cistanche steams 30 minutes, its echinacoside, cistanoside A, different acteoside and
The equal highest of polyoses content, therefore I grade of saline cistanche preferably steams 30 minutes.As shown in table 5, after II grade of saline cistanche steams 20 minutes,
Its echinacoside, acteoside, cistanoside A and the equal highest of 2'- acetyl group acteoside contents, and polyoses content is steaming
System highest after 10 minutes, but due to raw heart phenomenon after steaming 10 minutes be present, therefore II grade of saline cistanche preferably steams 20 minutes.Such as
Shown in table 6, after III grade of saline cistanche steams 20 minutes, its acteoside, different acteoside and 2'- acetyl group acteosides
Content highest；And echinacoside, cistanoside A and the polyoses content highest after steaming 30 minutes, but due to steaming 30 minutes
It is easily soft rotten afterwards, therefore III grade of saline cistanche preferably steams 20 minutes.
2.3 whole strains with section saline cistanche mass ratio compared with
Choose and used without wound, no disease and pests harm, complete II grade of whole strain saline cistanche, uniform rip cutting into 4 parts, 1/4 part
The processing method of saline cistanche of the present invention (after steaming 30 minutes under normal pressure with the vapor of 100 DEG C of temperature shine by whole strain saline cistanche
It is dry), 1/4 part is directly dried, and routinely production requirement is cut into 3mm pieces for 1/4 part, with the vapor of 100 DEG C of temperature in normal pressure
Under steam 5 minutes after dry, routinely production requirement is cut into 3mm pieces for 1/4 part, directly dries.
7 whole strain of table and the measurement result of section saline cistanche active component content
As shown in table 7, it is bright using ingredient content of phenylethanoid glycosides in the whole strain saline cistanche of the method for the invention processing
The aobvious saline cistanche higher than two groups of slicing treatments directly shines the whole strain saline cistanche of drying method processing with tradition；And tradition is used directly to shine
The saline cistanche that ingredient content of phenylethanoid glycosides is handled with direct slicing in the whole strain saline cistanche of drying method processing is not significantly different,
But polyoses content directly shines dry-cure in section and is obviously improved.
In summary, the whole strain saline cistanche habitat processing method of the present invention is steamed by high temperature effectively inhibits enzyme and microorganism
Activity, reduce going mouldy for whole strain saline cistanche, not only substantially reduce the medicinal material drying time, also improve meat desert on the whole
Rong's exterior quality and intrinsic activity component content, and the method for the invention is simple and easy, easily operated, cost is cheap, very
It is adapted to production and processing application of a large amount of fresh herba cistanches behind medicinal material original producton location and the excavation of artificial growth base, while is also convenient for medicine
The transport and storage of material.
It should be noted last that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although ginseng
The present invention is described in detail according to preferred embodiment, it will be understood by those within the art that, can be to the present invention
Technical scheme modify or equivalent substitution, without departing from the spirit and scope of technical solution of the present invention.
Claims (7)
- A kind of 1. drying means of saline cistanche, it is characterised in that including：Whole strain saline cistanche is classified；I grade of whole strain saline cistanche is steamed 30 minutes with vapor under normal pressure, or II grade or III grade whole strain saline cistanche is steamed with water Gas steams 20 minutes under normal pressure；Whole strain saline cistanche after steaming is dried；The fresh weight of I grade of whole strain saline cistanche is more than or equal to 928.80 grams, and length is more than or equal to 50.64 centimetres, and diameter More than or equal to 19.34 centimetres；The fresh weight of II grade of whole strain saline cistanche is more than or equal to 533.96 grams and less than 928.80 gram, Length is more than or equal to 46.82 centimetres and less than 50.64 centimetre, and diameter is more than or equal to 14.86 centimetres and less than 19.34 lis Rice；The fresh weight of III grade of whole strain saline cistanche is less than or equal to 533.96 grams, and length is less than or equal to 46.82 centimetres, and diameter Less than or equal to 14.86 centimetres.
- 2. the drying means of saline cistanche according to claim 1, it is characterised in that whole strain saline cistanche after the drying step Water content is 0-10%.
- A kind of 3. processing method of saline cistanche, it is characterised in that including：Whole strain saline cistanche is pre-processed；Pretreated whole strain saline cistanche is classified；Pretreated I grade whole strain saline cistanche is steamed 30 minutes with vapor under normal pressure, or by pretreated II grade or III grade of whole strain saline cistanche is steamed 20 minutes with vapor under normal pressure；Whole strain saline cistanche after steaming is dried；The fresh weight of I grade of whole strain saline cistanche is more than or equal to 928.80 grams, and length is more than or equal to 50.64 centimetres, and diameter More than or equal to 19.34 centimetres；The fresh weight of II grade of whole strain saline cistanche is more than or equal to 533.96 grams and less than 928.80 gram, Length is more than or equal to 46.82 centimetres and less than 50.64 centimetre, and diameter is more than or equal to 14.86 centimetres and less than 19.34 lis Rice；The fresh weight of III grade of whole strain saline cistanche is less than or equal to 533.96 grams, and length is less than or equal to 46.82 centimetres, and diameter Less than or equal to 14.86 centimetres.
- 4. the processing method of saline cistanche according to claim 3, it is characterised in that the pretreatment includes cleaning and/or going Except inflorescence.
- 5. according to the processing method of the saline cistanche of claim 3 or 4, it is characterised in that whole strain meat desert after the drying step The water content of Rong is 0-10%.
- 6. the processing method of saline cistanche according to claim 5, it is characterised in that include drying after the drying step Whole strain saline cistanche carries out packaging step afterwards.
- 7. according to the processing method of the saline cistanche of claim 3 or 4, it is characterised in that including after the drying step will Whole strain saline cistanche carries out packaging step after drying.
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| CN105663261A (en) * | 2016-03-18 | 2016-06-15 | 内蒙古王爷地苁蓉生物有限公司 | Fresh product cistanche salsa raw material processing method |
| CN105902620A (en) * | 2016-03-18 | 2016-08-31 | 内蒙古王爷地苁蓉生物有限公司 | Fresh cistanche decoction piece and preparation method thereof |
| CN108310065A (en) * | 2018-03-12 | 2018-07-24 | 内蒙古曼德拉沙产业开发有限公司 | A kind of Herba Cistanches fresh goods dry processing technique |
| CN109381522B (en) * | 2019-01-03 | 2024-05-10 | 建昌帮药业有限公司 | Cistanche deserticola processing method |
| CN115068522B (en) * | 2022-06-15 | 2023-09-12 | 内蒙古三口生物科技有限公司 | Cistanche deserticola water extract and preparation method and application thereof |
| CN115590903A (en) * | 2022-11-08 | 2023-01-13 | 福建杏林晓筑科技有限公司（Cn） | Fresh cistanche deserticola processing technology |
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| CN101485731A (en) * | 2008-01-16 | 2009-07-22 | 杏辉天力（杭州）药业有限公司 | Processing method for improving ingredient content of phenylethanoid glycosides in fresh Chinese medicine desertliving cistanche |
-
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Non-Patent Citations (1)
| Title |
|---|
| 肉从蓉炮制对微量元素含量及对动物体内DNA合成率的影响;余南才等，;《中国中药杂志》;19900630;第15卷(第6期);第22-24页 * |
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