CN104800100A - Mild and highly effective wash-free makeup removal cream and preparation method thereof - Google Patents
Mild and highly effective wash-free makeup removal cream and preparation method thereof Download PDFInfo
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- CN104800100A CN104800100A CN201510266286.2A CN201510266286A CN104800100A CN 104800100 A CN104800100 A CN 104800100A CN 201510266286 A CN201510266286 A CN 201510266286A CN 104800100 A CN104800100 A CN 104800100A
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Abstract
The invention relates to a mild and highly effective wash-free makeup removal cream. The mild and highly effective wash-free makeup removal cream is characterized in that the mild and highly effective wash-free makeup removal cream consists of the following components in percentage by weight: 2 to 10 percent of polyethylene, 2 to 20 percent of cetyl alcohol ethylhexoate, 2 to 20 percent of PEG-10 isostearate, 2 to 20 percent of PEG-20 glyceryl triisostearate, 0.2 to 1 percent of tocopheryl acetate, 2 to 10 percent of phenyl trimethicone, 0.2 to 3.0 percent of dextrin palmitate and the balance of caprylic/capric triglyceride. The makeup removal cream disclosed by the invention has the advantages of high makeup removal capability, mild properties, high safety and convenience and easiness in carrying.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of make-up remover, and the preparation method of this make-up remover.
Background technology
Increasing ladies' choice for use is not de-adornment product lastingly, the anti-antiperspirant eye-liner of such as waterproof, eyeliner etc.In order to reach the effect of the anti-antiperspirant of better waterproof, needing in formula to add a large amount of film former, being therefore difficult to removal.The object of makeup removing is not only remove residual adornment, also has sweat, sebum secretion thing and is attached to the dirt in the air on skin.Be difficult to thoroughly remove with cleansing milk or makeup removing liquid etc. simply, cause the nutritional labeling in the skin care item of follow-up use can not to be absorbed well by skin, even produce acne, cause the problem such as clogging of pores, acne.
Commercially available makeup remover is extensively liked by consumer due to its salubrious skinfeel, but adornment product is mainly oil-soluble at the bottom of most of color make-up product and persistency, therefore water preparation class or Hydrogels makeup removal products cannot thoroughly removal be clean, need to be wiped by makeup removing cotton rub, could the dressing of comparatively effective removal face; Portioned product is in order to reach effect of removing ornaments and formal dress preferably in addition, with the addition of the surfactant that zest is stronger, therefore should not be used for a lip.By contrast, although makeup remover has good molten adornment ability, its greasy feeling is comparatively strong, and flushing capacity is poor, and residual quantity is comparatively large, needs to use cleansing milk to clean further after unsnatching adornment.In addition, makeup remover and makeup remover are liquid dosage form, there is long-distance travel and carry inconvenience, easily leakage and can not be with shortcomings such as boarding a plane.
Summary of the invention
An object of the present invention is the technical problem for solving above, provide that a kind of makeup removing ability is good, character is gentle, safely, facilitate portative disposable make-up remover.
Another object of the present invention is to provide the preparation method of above-mentioned make-up remover.
For reaching above object, the invention provides following technical scheme:
A kind of gentle efficient disposable make-up remover, is characterized in that being made up of the component of following percentage by weight:
Polyethylene 2% ~ 10%, spermol ethylhexoate 2% ~ 20%, PEG-10 isostearate 2% ~ 20%, PEG-20 glyceryl triisostearate 2% ~ 20%, tocopherol acetas 0.2% ~ 1%, phenyl trimethicone 2% ~ 10%, dextrin cetylate 0.2% ~ 3.0%, surplus is caprylic/capric triglyceride.
Preferably, make-up remover of the present invention is made up of the component of following percentage by weight:
Polyethylene 2% ~ 6%, spermol ethylhexoate 2% ~ 8%, PEG-10 isostearate 2% ~ 5%, PEG-20 glyceryl triisostearate 10% ~ 20%, tocopherol acetas 0.2% ~ 0.5%, phenyl trimethicone 5% ~ 10%, dextrin cetylate 1% ~ 3%, surplus is caprylic/capric triglyceride.
Preferably, make-up remover of the present invention is made up of the component of following percentage by weight:
Polyethylene 6% ~ 10%, spermol ethylhexoate 2% ~ 20%, PEG-10 isostearate 2% ~ 20%, PEG-20 glyceryl triisostearate 2% ~ 20%, tocopherol acetas 0.5% ~ 1%, phenyl trimethicone 2% ~ 10%, dextrin cetylate 0.2% ~ 1%, surplus is caprylic/capric triglyceride.
Present invention also offers the preparation method of described make-up remover, its step is as follows:
(1) polyethylene, dextrin cetylate, caprylic/capric triglyceride, PEG-10 isostearate, PEG-20 glyceryl triisostearate, spermol ethylhexoate are added, stir;
(2) be warming up to 84 DEG C ~ 88 DEG C, be incubated 10 minutes, mixing speed remains on 300 revs/min, evacuation, homogenizing 5 minutes;
(3) phenyl trimethicone, tocopherol acetas are added successively, open and stir, mix homogeneously, cooling;
(4) when being down to 70 DEG C ~ 75 DEG C, discharging.
Beneficial effect of the present invention is:
1, there is very high makeup removing ability, in formula, add the salubrious oils and fats fully dissolving not de-adornment composition, and the nonionic surfactant of the noble and unsullied resulting net force of higher proportion, facial color make-up can be removed comparatively all sidedly.
2, product property is gentle especially, formula all components is gentle all especially, be applicable to various skin type, especially selected PEG type non-ionic surface active agent gentle especially, all show than anions and canons type surfactant to mucocutaneous or oculomucous zest low.
3, designed by optimization of C/C composites, make-up remover of the present invention has good flushing capacity, can meet water emulsification, does not need just can reach very salubrious effect with cleansing milk or other clean product again after makeup removing, has " disposable " performance.
4, novel appearance, be translucent paste, and namely tentacle is changed, and is easy to sprawl, is easy to carry about with one, and have the effect of Wet-dry.
5, the present invention has the safety of height, can be applied to eye and lip widely, safely.
Compared with prior art, the efficient disposable make-up remover of gentleness of the present invention overcomes the various shortcoming of traditional makeup removal products, adopt all oil system, the non-ionic surface active agent having selected safety high is as emulsifying agent, select polyethylene and dextrin cetylate as thick stabilization system simultaneously, utilize similar mixing and the coefficient principle of emulsifying, have efficient makeup removing, mildness high, disposable, not containing excellent properties such as antiseptic.
Accompanying drawing explanation
Fig. 1 is the cleaning capacity test result of make-up remover of the present invention.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme of the present invention is described in further detail, but protection scope of the present invention is not limited in following examples.
Weigh each component according to following mass percent, following component is all bought by commercial channel and is obtained.
The preparation method of make-up remover described in embodiment 1 ~ 3, its step is as follows:
(1) polyethylene in said components, dextrin cetylate, caprylic/capric triglyceride, PEG-10 isostearate, PEG-20 glyceryl triisostearate, spermol ethylhexoate are joined in emulsifying pot, open and stir;
(2) be warming up to 84 DEG C ~ 88 DEG C, be incubated 10 minutes, mixing speed remains on 300 revs/min, evacuation, homogenizing 5 minutes;
(3) phenyl trimethicone, tocopherol acetas are added in emulsifying pot successively, open and stir, mix homogeneously, cooling;
(4) when being down to 70 DEG C ~ 75 DEG C, discharging;
(5) be up to the standards, add hot filling.
Makeup removing merit rating:
The make-up remover of embodiment 1 ~ 3 is measured respectively to the cleaning capacity of BB frost, eyeliner by following program.
Respectively 50mg BB frost and 50mg eyeliner being applied in area on microscope slide is equably within the scope of 7.2cmx2.6cm, smear altogether five groups, be respectively blank group, reference examples, embodiment 1 embodiment 2 and embodiment 3, often group smeared the microscope slide of BB frost and eyeliner respectively by two pieces, totally 10 pieces of microscope slides, and weigh and record weight M
1.10 pieces of microscope slides are placed in 40 DEG C of biochemical cultivation cases to take out after air-dry one day.With the clean beautiful clean skin liquid complete wetting makeup removing cotton (about 1g) of Bei Dema (Bioderma), apply respectively on microscope slide, to scribble BB frost and eyeliner region in, the make-up remover of embodiment 1 ~ 3 respectively gets about 0.5g on makeup removing cotton in addition, and uniform fold is in the region scribbling BB frost and eyeliner, wait for after 3 minutes, rub back and forth after 10 times with makeup removing cotton and use tap water, all microscope slides are placed in 40 DEG C of biochemical cultivation cases air-dry 15 minutes after flushing, finally claim microscope slide weight M once again
2, and keep a record.Clean rate is calculated by following equation
[5].
Fig. 1 display is when using the cotton friction of makeup removing 10 times, and the make-up remover of embodiment 1 ~ 3 all reaches more than 50% to two kinds of long wear cosmetic clean rates respectively, especially reaches 92% to the makeup removing rate of eyeliner, exceeds 66% than makeup remover clean rate.Because the film former methyl that eyeliner contains silicones class gathers trimethicone or macromolecular colloid acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer, solvent normally ring five polydimethylsiloxane of these products, therefore make-up remover of the present invention is removed because unloading preferably containing the phenyl trimethicone composition good with its intermiscibility, the cleaning capacity only containing the relatively simple makeup remover of the composition such as common surfactant and polyhydric alcohol is then poor.
In addition, the display of picture under microscope, there is more large stretch of wax crystallization commercially available prod, and the make-up remover of the embodiment of the present invention 1 ~ 3 does not have large stretch of wax crystallization, solves this phenomenon well, makes the stability of product and smear sense more excellent.
Product mildness and safety evaluation (human skin patch result)
Evaluation methodology:
1) tested material: the make-up remover of embodiment 1 ~ 3.
2) negative control: blank.
3) experimenter: totally 40 people, male 15 people, female 25 people, at 18 ~ 30 years old age, meets experimenter and volunteers inclusion criteria.
4) speckle method for testing: select qualified speckle examination device, with closed patch test method, tested material being about 0.02ml ~ 0.025ml is applied in speckle examination device, external special adhesive tape sticks in the bent side of experimenter's forearm, tested material is removed after 24 hours, 30min after removal tested material speckle examination device, observes dermoreaction, by its result of dermoreaction grade scale record in " cosmetics health specification " (version in 2007) after impression disappears.
5) evaluation of result: according to the form below (skin adverse reaction grade scale) records reaction result.
6) result of the test is as shown in the table:
Cosmetics human skin patch result
Table 2
Human skin patch result shows: in the make-up remover of embodiment 1 ~ 3, and 40 subjects skin are all negative reaction (grading system: 0 grade).According to " cosmetics health specification " (version in 2007) human body skin class paste test criterion, sample to human body without skin adverse reaction.And in reference examples (commercially available internationally renowned brand make-up remover), have 2 experimenters to occur 1 order reaction.Visible, make-up remover mildness of the present invention is high, and safety is good.
Product stability is assessed
1. temperature stability test
(1) 48 DEG C of stability test:
Test sample: the make-up remover of embodiment 1 ~ 3
Testing time: 4 weeks
Method of testing: product (content) is loaded in the PET bottle of 30mL, labelled, indicate name of product, formula number, the information such as test condition, testDate, be placed in the heat-resistant stability of the biochemical cultivation case test products of 48 DEG C, 24 hours, 1 week, 2 weeks, 4 weeks time, (returning to room temperature) observes the change of the outward appearance of product, abnormal smells from the patient, pH, viscosity respectively, and by the change of day part, be recorded in report.
(2) 40 DEG C of stability tests:
Test sample: the make-up remover of embodiment 1 ~ 3
Testing time: 12 weeks
Method of testing: product (content) is loaded in the PET bottle of 30mL, labelled, indicate name of product, formula number, the information such as test condition, testDate, be placed in the heat-resistant stability of the biochemical cultivation case test products of 40 DEG C, when 24 hours, 1 week, 2 weeks, 4 weeks, 8 weeks and 12 weeks, (returning to room temperature) observed the change of the outward appearance of product, abnormal smells from the patient, pH, viscosity respectively, and by the change of day part, be recorded in report.
(3) room temperature (Ambient) stability test:
Test sample: the make-up remover of embodiment 1 ~ 3
Testing time: 12 weeks
Method of testing: product (content) is loaded in the PET bottle of 30mL, labelled, indicate name of product, formula number, the information such as test condition, testDate, be placed in sample cabinet, respectively 24 hours (survey pH value, viscosimetric), 1 week, 2 weeks, 4 weeks, 8 weeks and 12 weeks (survey pH value) time the outward appearance of observation product, abnormal smells from the patient, pH, viscosity change, and by the change of day part, be recorded in report.
(4)-18 DEG C of stability tests:
Test sample: the make-up remover of embodiment 1 ~ 3
Testing time: 12 weeks
Method of testing: product (content) is loaded in the PET bottle of 30mL, labelled, indicate name of product, formula number, the information such as test condition, testDate, be placed in the cold-resistant stability of-18 DEG C of refrigerator test products, when 24 hours, 1 week, 2 weeks, 4 weeks, 8 weeks and 12 weeks, (returning to room temperature) observed the change of the outward appearance of product, abnormal smells from the patient, pH, viscosity respectively, and by the change of day part, be recorded in report.
(5) 48 DEG C and-18 DEG C of cyclical stability tests
Test sample: 1 or more
Testing time: continuous three loop tests (first place in 48 DEG C of biochemical cultivation cases after 24 hours, place 24 hours at room temperature, be then placed on-18 DEG C of refrigerators 24 hours, and then return to room temperature be a circulation and observed result).
Method of testing: product (content) is loaded in the PET bottle of 30mL, labelled, indicate name of product, formula number, the information such as test condition, testDate, be placed in the biochemical cultivation case 24 hours of 48 DEG C, return to room temperature and place 24 hours, then be placed in-18 DEG C of refrigerators 24 hours, and then return to room temperature.Observe the change of product outward appearance, abnormal smells from the patient, pH, viscosity etc. of product when cold-resistant heat-resisting alternate cycles, and be recorded in report.
2. sunlight stability test
Test sample: the make-up remover of embodiment 1 ~ 3
Testing time: 4 weeks
Sunlight is tested, product (content) is loaded in the PET bottle of 30mL, labelled, indicate name of product, formula number, the information such as test condition, testDate, be placed on place near the window, west (label facing away from sunlight), 24 hours, 1 week, 2 weeks, 4 weeks time, (returning to room temperature) observes the outward appearance of product, the change of abnormal smells from the patient respectively, and by the change of day part, is recorded in report.
Result shows, and through the above stability test of 12 weeks, the stability of the make-up remover of embodiment 1 ~ 3 was better.
Claims (4)
1. the efficient disposable make-up remover of gentleness, is characterized in that being made up of the component of following percentage by weight:
Polyethylene 2% ~ 10%, spermol ethylhexoate 2% ~ 20%, PEG-10 isostearate 2% ~ 20%, PEG-20 glyceryl triisostearate 2% ~ 20%, tocopherol acetas 0.2% ~ 1%, phenyl trimethicone 2% ~ 10%, dextrin cetylate 0.2% ~ 3.0%, surplus is caprylic/capric triglyceride.
2. make-up remover according to claim 1, is characterized in that being made up of the component of following percentage by weight:
Polyethylene 2% ~ 6%, spermol ethylhexoate 2% ~ 8%, PEG-10 isostearate 2% ~ 5%, PEG-20 glyceryl triisostearate 10% ~ 20%, tocopherol acetas 0.2% ~ 0.5%, phenyl trimethicone 5% ~ 10%, dextrin cetylate 1% ~ 3%, surplus is caprylic/capric triglyceride.
3. make-up remover according to claim 1, is characterized in that being made up of the component of following percentage by weight:
Polyethylene 6% ~ 10%, spermol ethylhexoate 2% ~ 20%, PEG-10 isostearate 2% ~ 20%, PEG-20 glyceryl triisostearate 2% ~ 20%, tocopherol acetas 0.5% ~ 1%, phenyl trimethicone 2% ~ 10%, dextrin cetylate 0.2% ~ 1%, surplus is caprylic/capric triglyceride.
4. the preparation method of make-up remover described in any one of claims 1 to 3, is characterized in that, its step is as follows:
(1) polyethylene, dextrin cetylate, caprylic/capric triglyceride, PEG-10 isostearate, PEG-20 glyceryl triisostearate, spermol ethylhexoate are added, stir;
(2) be warming up to 84 DEG C ~ 88 DEG C, be incubated 10 minutes, mixing speed remains on 300 revs/min, evacuation, homogenizing 5 minutes;
(3) phenyl trimethicone, tocopherol acetas are added successively, open and stir, mix homogeneously, cooling;
(4) when being down to 70 DEG C ~ 75 DEG C, discharging.
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| CN105411993A (en) * | 2016-01-13 | 2016-03-23 | 广州丹奇日用化工厂有限公司 | Makeup removing cream and preparation method thereof |
| CN105411965A (en) * | 2016-01-13 | 2016-03-23 | 广州丹奇日用化工厂有限公司 | Safe makeup removing cream and preparation method thereof |
| CN105434291A (en) * | 2016-01-20 | 2016-03-30 | 广州丹奇日用化工厂有限公司 | Refreshing and non-greasy type makeup removing paste and preparation method thereof |
| CN105496825A (en) * | 2016-01-20 | 2016-04-20 | 广州丹奇日用化工厂有限公司 | Cleansing cream capable of repairing damaged hydrolipidic film and preparation method thereof |
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| CN105560131A (en) * | 2016-03-16 | 2016-05-11 | 广州丹奇日用化工厂有限公司 | Sensitive repairing type cleansing cream and preparation method thereof |
| CN105581915A (en) * | 2016-03-05 | 2016-05-18 | 广州丹奇日用化工厂有限公司 | Hydrolipidic film repairing type makeup removal paste with traditional Chinese medicine ingredients and preparation method of makeup removal paste |
| CN105581939A (en) * | 2015-12-10 | 2016-05-18 | 诺斯贝尔化妆品股份有限公司 | Massaging and makeup-removing cleansing paste |
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| CN106420456A (en) * | 2016-10-10 | 2017-02-22 | 珍尔姿（广州）化妆品有限公司 | Multiple-effect makeup-removing cleaning cream |
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| CN106913478A (en) * | 2017-05-04 | 2017-07-04 | 广州诺胜化妆品有限公司 | A kind of big red tangerine make-up remover and preparation method |
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| CN106580717B (en) * | 2017-02-24 | 2020-02-07 | 花安堂生物科技集团有限公司 | Suspension composition and application thereof in cosmetics |
| CN106913478A (en) * | 2017-05-04 | 2017-07-04 | 广州诺胜化妆品有限公司 | A kind of big red tangerine make-up remover and preparation method |
| CN109431878A (en) * | 2018-11-23 | 2019-03-08 | 广州市科能化妆品科研有限公司 | A kind of anhydrous disposable gold seaweed makeup remover |
| CN109431878B (en) * | 2018-11-23 | 2022-03-11 | 广州市科能化妆品科研有限公司 | Waterless washing-free gold seaweed cleansing oil |
| CN109288734A (en) * | 2018-11-30 | 2019-02-01 | 广州市科能化妆品科研有限公司 | Disposable algal oil make-up remover and preparation method thereof |
| CN109288734B (en) * | 2018-11-30 | 2021-09-03 | 广州市科能化妆品科研有限公司 | Washing-free seaweed oil makeup removing cream and preparation method thereof |
| CN111374895A (en) * | 2018-12-29 | 2020-07-07 | 伽蓝（集团）股份有限公司 | Skin care composition, preparation method and application thereof, and prepared skin care product |
| CN111374895B (en) * | 2018-12-29 | 2023-08-15 | 伽蓝（集团）股份有限公司 | Skin care composition, preparation method and application thereof and prepared skin care product |
| CN115154347A (en) * | 2022-07-27 | 2022-10-11 | 广州环亚化妆品科技股份有限公司 | Makeup removing cream and preparation method thereof |
| CN115154347B (en) * | 2022-07-27 | 2024-02-23 | 广州环亚化妆品科技股份有限公司 | Cleansing cream and preparation method thereof |
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Effective date of registration: 20190201 Address after: 528300 No. 3 Lianhua Road, Leliu Fuan industrial area, Shunde District, Foshan, Guangdong Patentee after: FOSHAN WIN COSMETIC CO., LTD. Address before: 510000 Room 18, 20 and 22, 22nd Floor, Dongcheng Square, No. 111-115, Youxin Road, Temple, Yuexiu District, Guangzhou City, Guangdong Province Patentee before: GUANGZHOU SHENCAI COSMETICS CO., LTD. |