CN104799458A - Production method of permanent ultraviolet protecting, moisture absorbing and sweat removing fabric - Google Patents
Production method of permanent ultraviolet protecting, moisture absorbing and sweat removing fabric Download PDFInfo
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Abstract
The invention discloses a production method of a permanent ultraviolet protecting, moisture absorbing and sweat removing fabric. The method comprises the steps of blending and weaving; singeing; desizing-scouring-bleaching; mercerizing; sizing; dyeing; softening and tentering; pre-shrinking and arranging. The fabric manufactured by the production process is outstanding in permanent ultraviolet resisting function; the UPF is not less than 150; micro pores of CTATEX super-comfortable polyester fibers can be opened fully by the desizing-scouring-bleaching and mercerizing, holes in the fibers are smooth, the moisture absorbing and breathing performances of the fabric can be improved under the absorbing effect of hole cores, and the water drops can be absorbed within 3 seconds according to the test; the fuzzing and pilling resistance of the fabric is more than 4 grades; the advantages of wearing resistance, non-ironing, wrinkle preventing and quick drying of the polyester fibers are remained to the maximum; the fabric is particularly suitable for wearing when working and living outdoor in a hot season.
Description
Technical field
The present invention relates to textile technology field, especially relate to a kind of production technology adopting permanent antiultraviolet thread water absorben perspiring shell fabric.
Background technology
Along with the research that deepens continuously to weaving face fabric, fabric variety is also constantly weeded out the old and bring forth the new.People not only require more and more higher to wearability, but also require that fabric has pure color, economical and practical, environmental-friendly and comfortable and such as antiultraviolet, moisture absorbing and sweat releasing, the feature such as antibacterial.
In prior art, the fabric for the outdoor activities of hot season forms mainly with fibrous woven such as cotton, fiber crops or mulberry silks.There is the shortcomings such as powerful low, rub is poor, service life is short, quick-drying is poor in cotton work clothes, easily sweat tart flavour can be produced under long sweat effect, cause human body to produce clammy sense, and can electrostatic hazard be produced under the environment being less than 30% in relative humidity; Linen textile abrasion-proof corrosion-proof performance and heat conduction moisture pick-up properties are all better than wollen fabrics, and permeability is good, have unique cooling feeling, insensitive to acid-base reaction, antifungi, moisture-sensitive is not mouldy, and shortcoming is that feel is coarse, wear not smooth comfortable, crease easily, drapability is poor, and flaxen fiber steel is hard, cohesive force is poor, and blending producting process difficulty is large.In addition, a part of flaxen fiber in flax fabric is because of containing lignin, erose fiber cross section and linearly or the lumen of ellipse and have natural anti-ultraviolet property; Mulberry silk has preferably uvioresistant and moisture absorbing and sweat releasing performance equally, but because of its not easily arrange, easily hanging wire, fabric cost are high and cannot as outwork in summer wearing fabric.
The method of giving fabric anti-ultraviolet property in prior art mainly contains three kinds: the first, ultraviolet light screener nano material be mixed in fibrous material and make uvioresistant fiber; The second, in web surface coating ultraviolet resistant; Three, adopt the dressing liquid containing ultra-violet absorber and/or ultraviolet light screener to carry out Final finishing to fabric, make ultra-violet absorber and/or ultraviolet light screener scattered adsorption on fabric.Ultraviolet protection agent content in latter two method gained fabric can reduce because of the repeatedly cleaning of clothing, and anti-ultraviolet property is also corresponding to be weakened; And first method the wearability of fabric poor.Therefore, be necessary improve the fibrous and production technology of permanent antiultraviolet thread water absorben perspiring shell fabric of the prior art and optimize.
Summary of the invention
The object of the invention is to overcome the defect existed in prior art, provide a kind of production technology adopting permanent antiultraviolet thread water absorben perspiring shell fabric, this technique is simple to operation, and made fabric has permanent anti-ultraviolet function, and moisture absorption is ventilative, frivolous comfortable.
For achieving the above object, the technical solution used in the present invention is a kind of production technology of permanent antiultraviolet thread water absorben perspiring shell fabric, and it is characterized in that, described production technology comprises following production stage:
S1: hybrid woven, by percentage by weight be 65 ~ 70% CTATEX spy relax polyester fiber and 30 ~ 35% long-staple cotton through blending, be woven into combing grey cloth;
S2: singe, to singe process to the positive and negative of S1 gained combing grey cloth;
S3: move back and boil drift, adopts hydrogen peroxide-caustic soda destarch method to carry out one-bath DSB process to the grey cloth after singing;
S4: mercerising, carries out mercerization finish with sodium hydroxide solution to S3 gained fabric;
S5: sizing, adopts forming machine to carry out thermal finalization process to fabric;
S6: dyeing, adopts dispersion intellectual circle dyestuff to dye to fabric;
S7: soft tentering, is padded in the dressing liquid of moisture absorbing and sweat releasing auxiliary agent by fabric, again through stenter high temperature tentering after oven dry;
S8: shrunk finish, adopts sanforized method, first by fabric through spraying steam or spraying dewing, then impose warp-wise mechanical presses, then dry through loose formula, the obtained permanent antiultraviolet thread water absorben perspiring shell fabric of finished product;
Wherein, described concentration of moving back each component in the slurry boiling drift process employing is: NaOH 45 ~ 55g/L, hydrogen peroxide 10 ~ 14 g/L, micropore expansion auxiliary agent 8 ~ 12 g/L, hydrogen peroxide stabilizer 10 ~ 14 g/L, kiering temperature is 100 ~ 105 DEG C, and the kiering time is 25 ~ 35min, and described micropore expansion auxiliary agent is the mixture of chitin oligosaccharide non-ionic surface active agent and MES.
In order to optimize the composite effect of chitin oligosaccharide non-ionic surface active agent and MES anion surfactant further, preferred technical scheme is, in described micropore expansion auxiliary agent, the content of chitin oligosaccharide non-ionic surface active agent is 25 ~ 35%.
Moving back the slurry boiling drift process employing is strong basicity, larger sequestering in order to ensure that hydrogen peroxide stabilizer has metal ion in highly basic bath, improve the whiteness of white goods simultaneously as far as possible, preferred technical scheme is, described hydrogen peroxide stabilizer is polycarboxylate-type containing ehter bond or acrylic acid derivative hydrogen peroxide stabilizer.
Mercerising can improve the surface property of fabric further, increase the adsorption capacity to dyestuff, the easypro polyester fiber of the spy of the CTATEX in fabric and long-staple cotton fiber is made to have the gloss of silk, and sodium hydroxide solution can infiltrate in the micropore of the easypro polyester fiber of CTATEX spy, react with pore former further, the weight-loss ratio of fabric after mercerization finish and moisture permeability and anti-pilling property closely related, the too high meeting of naoh concentration causes fabric loss too much to affect the intensity of fabric, the too low improvement to moisture permeability and anti-pilling property of naoh concentration is not obvious, preferred weight-loss ratio is 18 ~ 22%, preferred technical scheme is, in the treatment fluid of mercerization finish, naoh concentration is 190 ~ 210 g/L.
Pre-setting temperature before dyeing can affect crystalline phase marshalling degree in the easypro polyester fiber of CTATEX spy, and then affect the dye-uptake of dyestuff, the too high cloth cover of temperature can turn to be yellow, cloth cover is endured with all one's will, in order to optimize Color, preferred technical scheme is, in S5, heat setting temperature is 185 ~ 195 DEG C, and the time is 30s.
The micropore of the easypro polyester fiber of CTATEX spy can give fabric certain anti-pilling property, in order to optimize the pilling property of fabric further, improve cloth cover gloss, this fabric Midlle-longstaple cotton and CTATEX spy relax polyester fiber due to material different, hot property differs, the too high meeting of the speed of a motor vehicle of singing causes burn-off phenomenon, after burning, fine hair is spherical, color dot is there will be during dyeing, can thermal contraction be there is in the too low fabric of the speed of a motor vehicle, comparatively the easypro polyester fiber thermal contraction of CTATEX spy is more obvious for cotton fiber in fabric, preferred technical scheme is, singe in S2 and be treated to two positive one and instead singe, the speed of a motor vehicle of singing is 105 ~ 115m/min, the distance of flame and cloth cover is 2cm.
Grease in fabric use procedure in sweat is inserted in micropore, affect uvioresistant and moisture permeability, need to carry out soft treatment to fabric, the washability of fabric can also be improved simultaneously, reduce decontamination difficulty, preferred technical scheme is, in S7, dressing liquid comprises: hydrophilic silicone finishing agent 30 ~ 35 g/L, shitosan 10 ~ 15 g/L, moisture absorbing and sweat releasing auxiliary agent 40 ~ 60g/L, and the pH value of described dressing liquid is 4 ~ 6.
In fabric after dyeing, the partial pore of the easypro polyester fiber of CTATEX spy can be blocked by dyestuff, the uvioresistant performance of fabric and moisture permeability is caused to reduce, the ultrasonic dyestuff that can impel is discharged from micropore, fiber surface can also be etched further, increase the specific area of fiber, preferred technical scheme is, is ultrasonic bath for holding the stock tank of described dressing liquid.
Beneficial effect of the present invention is:
CTATEX spy relaxes the molecular structure of polyester fiber with terephthalic acid (TPA) diol ester for agent structure, procedure of fibre production needs to add specific pore former, pore former part is residual in the fibre, the moisture absorption of fabric can be had influence on, the style of anti-ultraviolet property and fabric, move back the object of boiling drift process to be to make alkali lye go deep into taking pore former out of in micropore, micro pore shape is fully presented, in general, chitin oligosaccharide non-ionic surface active agent can make the surface tension of water be down to below 30mN/m, by chitin oligosaccharide non-ionic surface active agent and MES anion surfactant used in combination in move back boil drift process adopt slurry in, compound system can be formed, additive synergism is realized in reduction surface tension and enhancing permeance property,
Fabric obtained by this production technology has excellent permanent anti-ultraviolet function, and UPF is not less than 150; Move back and boil drift and mercerization finish operation the relax micropore of polyester fiber of CTATEX spy is fully opened, fibrous inside cavity is unimpeded, the moisture permeability of hole core sucting action enhancing fabric, is less than 3 seconds through the experimental test soak time that drips; The anti-fluffing and anti-pilling performance of fabric reaches more than 4 grades; Farthest remain the advantage of wear-resisting, non-ironing, the wrinkle resistant and quick-drying of polyester fiber, dress when being specially adapted to outwork life hot season.
Detailed description of the invention
Below in conjunction with embodiment, the specific embodiment of the present invention is further described.Following examples only for technical scheme of the present invention is clearly described, and can not limit the scope of the invention with this.
Embodiment 1
The production technology of the permanent antiultraviolet thread water absorben perspiring shell fabric of embodiment 1 comprises following production stage:
S1: hybrid woven, by percentage by weight be 65% CTATEX spy relax polyester fiber and 35% long-staple cotton through blending, be woven into combing grey cloth;
S2: singe, to singe process to the positive and negative of S1 gained combing grey cloth;
S3: move back and boil drift, adopts hydrogen peroxide-caustic soda destarch method to carry out one-bath DSB process to the grey cloth after singing;
S4: mercerising, carries out mercerization finish with sodium hydroxide solution to S3 gained fabric;
S5: sizing, adopts forming machine to carry out thermal finalization process to fabric;
S6: dyeing, adopts dispersion intellectual circle dyestuff to dye to fabric;
S7: soft tentering, is padded in the ultrasonic wave stock tank of the dressing liquid that moisture absorbing and sweat releasing auxiliary agent is housed by fabric, again through stenter high temperature tentering after oven dry;
S8: shrunk finish, adopts sanforized method, first by fabric through spraying steam or spraying dewing, then impose warp-wise mechanical presses, then dry through loose formula, the obtained permanent antiultraviolet thread water absorben perspiring shell fabric of finished product;
Wherein, the concentration of moving back each component in the slurry boiling drift process employing is: NaOH 45g/L, hydrogen peroxide 14 g/L, micropore expansion auxiliary agent 8g/L, hydrogen peroxide stabilizer 14 g/L, kiering temperature is 100 ~ 105 DEG C, and the kiering time is 25min, and micropore expansion auxiliary agent is the mixture of chitin oligosaccharide non-ionic surface active agent and MES.
In the present embodiment, in micropore expansion auxiliary agent, the content of chitin oligosaccharide non-ionic surface active agent is 25%; Hydrogen peroxide stabilizer is polycarboxylate-type containing ehter bond or acrylic acid derivative hydrogen peroxide stabilizer; In the treatment fluid of mercerization finish, naoh concentration is 190 g/L; In S5, heat setting temperature is 185 ~ 190 DEG C, and the time is 30s; Singe in S2 and be treated to two positive one and instead singe, the speed of a motor vehicle of singing is 105m/min, and the distance of flame and cloth cover is 2cm; In S7, dressing liquid comprises: hydrophilic silicone finishing agent 30 g/L, shitosan 10 g/L, moisture absorbing and sweat releasing auxiliary agent 60g/L, and the pH value of dressing liquid is 4.
Embodiment 2
Different being of embodiment 2 and embodiment 1 technological parameter: in combing grey cloth, fibre furnish is: CTATEX spy is relaxed polyester fiber 70%, long-staple cotton 30%; The concentration of moving back each component in the slurry boiling drift process employing is: NaOH 55g/L, hydrogen peroxide 10 g/L, micropore expansion auxiliary agent 12 g/L, hydrogen peroxide stabilizer 10g/L, kiering temperature is 100 ~ 105 DEG C, the kiering time is 35min, and micropore expansion auxiliary agent is the mixture of chitin oligosaccharide non-ionic surface active agent and MES.
In the present embodiment, in micropore expansion auxiliary agent, the content of chitin oligosaccharide non-ionic surface active agent is 25 ~ 30%; Hydrogen peroxide stabilizer is polycarboxylate-type containing ehter bond or acrylic acid derivative hydrogen peroxide stabilizer; In the treatment fluid of mercerization finish, naoh concentration is 210 g/L; In S5, heat setting temperature is 190 ~ 195 DEG C, and the time is 30s; Singe in S2 and be treated to two positive one and instead singe, the speed of a motor vehicle of singing is 115m/min, and the distance of flame and cloth cover is 2cm; In S7, dressing liquid comprises: hydrophilic silicone finishing agent 35 g/L, shitosan 15 g/L, moisture absorbing and sweat releasing auxiliary agent 40g/L, and the pH value of dressing liquid is 4 ~ 6.
Embodiment 3
Different being of embodiment 3 and embodiment 1 technological parameter: in combing grey cloth, fibre furnish is: CTATEX spy is relaxed polyester fiber 68%, long-staple cotton 32%; The concentration of moving back each component in the slurry boiling drift process employing is: NaOH 50g/L, hydrogen peroxide 12g/L, micropore expansion auxiliary agent 10 g/L, hydrogen peroxide stabilizer 12 g/L, kiering temperature is 102 DEG C, the kiering time is 30min, and micropore expansion auxiliary agent is the mixture of chitin oligosaccharide non-ionic surface active agent and MES.
In the present embodiment, in micropore expansion auxiliary agent, the content of chitin oligosaccharide non-ionic surface active agent is 30%; Hydrogen peroxide stabilizer is polycarboxylate-type containing ehter bond or acrylic acid derivative hydrogen peroxide stabilizer; In the treatment fluid of mercerization finish, naoh concentration is 200 g/L; In S5, heat setting temperature is 190 ~ 195 DEG C, and the time is 30s; Singe in S2 and be treated to two positive one and instead singe, the speed of a motor vehicle of singing is 110m/min, and the distance of flame and cloth cover is 2cm; In S7, dressing liquid comprises: hydrophilic silicone finishing agent 32 g/L, shitosan 12 g/L, moisture absorbing and sweat releasing auxiliary agent 50g/L, and the pH value of dressing liquid is 4 ~ 6.
Embodiment 1,2,3 is weighed to sample after soft tentering process, and compared with combing embryo cloth weight, weight-loss ratio is respectively 18.3%, 21.7%, 20.4%; The water droplet of finished product fabric is respectively 2.9s, 1.6s, 2.1s diffusion time; Evaporation rate is 0.24g/h, 0.26g/h, 0.18g/h; Anti-fluffing and anti-pilling grade be respectively 4 grades, 4-5 level, 4-5 level.
The CTATEX spy polyester fiber that relaxes is developed by China Textile Academy, and molecular structure take ethylene glycol terephthalate as agent structure, the modified poly ester produced by carrying out chemical modification and physical modification to Macroscopic single crystal system.Have in this fiber similar natural formation, the micro pore shape of from outward appearance to inner essence lack of alignment, by using the sodium hydroxide solution of variable concentrations to process fiber or fabric under uniform temperature condition, realize the controlled of hole number and the degree of depth.
Chitin oligosaccharide non-ionic surface active agent specifically can select alkoxyl hydroxypropyl chitin oligosaccharide, synthetic method is: be adopt corresponding alcohol (phenol) and epoxychloropropane synthesis of alkyl glycidol ether in the presence of a phase transfer catalyst, then alkyl glycidyl ether and chitin oligosaccharide reacted and prepared corresponding alkoxyl hydroxypropyl chitin oligosaccharide.The monose number that in chitin oligosaccharide non-ionic surface active agent oligosaccharides molecule structure, glycosidic bond connects is 5-10.
The preferred amplitude of ultrasonic wave stock tank is 15 ~ 25 microns, and the too high meeting of ultrasonic amplitude makes micropore excessive, thus reduces the intensity of fabric; Ultrasonic amplitude is crossed low-fiber specific area and is improved not obvious.
Moisture absorbing and sweat releasing auxiliary agent is the SCOTCHGARD moisture control agent that U.S.'s Hensel steps HSD moisture absorbing and sweat releasing auxiliary agent or 3M.
Move back boil drift and mercerising process also can use ultrasonic wave stock tank.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (8)
1. a production technology for permanent antiultraviolet thread water absorben perspiring shell fabric, is characterized in that, described production technology comprises following production stage:
S1: hybrid woven, by percentage by weight be 65 ~ 70% CTATEX spy relax polyester fiber and 30 ~ 35% long-staple cotton through blending, be woven into combing grey cloth;
S2: singe, to singe process to the positive and negative of S1 gained combing grey cloth;
S3: move back and boil drift, adopts hydrogen peroxide-caustic soda destarch method to carry out one-bath DSB process to the grey cloth after singing;
S4: mercerising, carries out mercerization finish with sodium hydroxide solution to S3 gained fabric;
S5: sizing, adopts forming machine to carry out thermal finalization process to fabric;
S6: dyeing, adopts dispersion intellectual circle dyestuff to dye to fabric;
S7: soft tentering, is padded in the dressing liquid of moisture absorbing and sweat releasing auxiliary agent by fabric, again through stenter high temperature tentering after oven dry;
S8: shrunk finish, adopts sanforized method, first by fabric through spraying steam or spraying dewing, then impose warp-wise mechanical presses, then dry through loose formula, the obtained permanent antiultraviolet thread water absorben perspiring shell fabric of finished product;
Wherein, described concentration of moving back each component in the slurry boiling drift process employing is: NaOH 45 ~ 55g/L, hydrogen peroxide 10 ~ 14 g/L, micropore expansion auxiliary agent 8 ~ 12 g/L, hydrogen peroxide stabilizer 10 ~ 14 g/L, kiering temperature is 100 ~ 105 DEG C, and the kiering time is 25 ~ 35min, and described micropore expansion auxiliary agent is the mixture of chitin oligosaccharide non-ionic surface active agent and MES.
2. the production technology of permanent antiultraviolet thread water absorben perspiring shell fabric according to claim 1, is characterized in that, in described micropore expansion auxiliary agent, the content of chitin oligosaccharide non-ionic surface active agent is 25 ~ 35%.
3. the production technology of permanent antiultraviolet thread water absorben perspiring shell fabric according to claim 1, is characterized in that, described hydrogen peroxide stabilizer is polycarboxylate-type containing ehter bond or acrylic acid derivative hydrogen peroxide stabilizer.
4. the production technology of permanent antiultraviolet thread water absorben perspiring shell fabric according to claim 1, is characterized in that, in the treatment fluid of mercerization finish, naoh concentration is 190 ~ 210 g/L.
5. the production technology of permanent antiultraviolet thread water absorben perspiring shell fabric according to claim 1, is characterized in that, in S5, heat setting temperature is 185 ~ 195 DEG C, and the time is 30s.
6. the production technology of permanent antiultraviolet thread water absorben perspiring shell fabric according to claim 1, is characterized in that, singes to be treated to two positive one and instead to singe in S2, and the speed of a motor vehicle of singing is 105 ~ 115m/min, and the distance of flame and cloth cover is 2cm.
7. the production technology of permanent antiultraviolet thread water absorben perspiring shell fabric according to claim 1, it is characterized in that, in S7, dressing liquid comprises: hydrophilic silicone finishing agent 30 ~ 35 g/L, shitosan 10 ~ 15 g/L, moisture absorbing and sweat releasing auxiliary agent 40 ~ 60g/L, and the pH value of described dressing liquid is 4 ~ 6.
8. the production technology of permanent antiultraviolet thread water absorben perspiring shell fabric according to claim 7, is characterized in that, is ultrasonic bath for holding the stock tank of described dressing liquid.
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