CN104788721A - 一种含氮丙啶交联剂的组合物及其制备方法 - Google Patents
一种含氮丙啶交联剂的组合物及其制备方法 Download PDFInfo
- Publication number
- CN104788721A CN104788721A CN201510156898.6A CN201510156898A CN104788721A CN 104788721 A CN104788721 A CN 104788721A CN 201510156898 A CN201510156898 A CN 201510156898A CN 104788721 A CN104788721 A CN 104788721A
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- weight
- aziridine crosslinker
- linking agent
- crosslinker
- organic amine
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000004971 Cross linker Substances 0.000 title claims abstract description 56
- 239000000203 mixture Substances 0.000 title claims abstract description 51
- NOWKCMXCCJGMRR-UHFFFAOYSA-N Aziridine Chemical compound C1CN1 NOWKCMXCCJGMRR-UHFFFAOYSA-N 0.000 title claims abstract description 48
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 32
- 150000001412 amines Chemical class 0.000 claims description 22
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 claims description 20
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 16
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- HQABUPZFAYXKJW-UHFFFAOYSA-N butan-1-amine Chemical compound CCCCN HQABUPZFAYXKJW-UHFFFAOYSA-N 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 229910021529 ammonia Inorganic materials 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 6
- 239000000243 solution Substances 0.000 claims description 5
- 239000003637 basic solution Substances 0.000 claims description 4
- 239000003381 stabilizer Substances 0.000 abstract 4
- 238000000576 coating method Methods 0.000 description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 239000011248 coating agent Substances 0.000 description 7
- 239000002904 solvent Substances 0.000 description 7
- OZDGMOYKSFPLSE-UHFFFAOYSA-N 2-Methylaziridine Chemical compound CC1CN1 OZDGMOYKSFPLSE-UHFFFAOYSA-N 0.000 description 6
- 239000007864 aqueous solution Substances 0.000 description 6
- 238000004821 distillation Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 2
- HXKKHQJGJAFBHI-UHFFFAOYSA-N 1-aminopropan-2-ol Chemical compound CC(O)CN HXKKHQJGJAFBHI-UHFFFAOYSA-N 0.000 description 2
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 239000002612 dispersion medium Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000012074 organic phase Substances 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 238000013517 stratification Methods 0.000 description 2
- 238000012795 verification Methods 0.000 description 2
- 150000001541 aziridines Chemical class 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 235000020354 squash Nutrition 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Paints Or Removers (AREA)
Abstract
Description
Claims (6)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810004852.6A CN108084771B (zh) | 2015-04-04 | 2015-04-04 | 一种交联剂组合物及其涂料 |
CN201510156898.6A CN104788721B (zh) | 2015-04-04 | 2015-04-04 | 一种含氮丙啶交联剂的组合物及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510156898.6A CN104788721B (zh) | 2015-04-04 | 2015-04-04 | 一种含氮丙啶交联剂的组合物及其制备方法 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201810004852.6A Division CN108084771B (zh) | 2015-04-04 | 2015-04-04 | 一种交联剂组合物及其涂料 |
Publications (2)
Publication Number | Publication Date |
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CN104788721A true CN104788721A (zh) | 2015-07-22 |
CN104788721B CN104788721B (zh) | 2017-12-12 |
Family
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Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
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CN201510156898.6A Expired - Fee Related CN104788721B (zh) | 2015-04-04 | 2015-04-04 | 一种含氮丙啶交联剂的组合物及其制备方法 |
CN201810004852.6A Active CN108084771B (zh) | 2015-04-04 | 2015-04-04 | 一种交联剂组合物及其涂料 |
Family Applications After (1)
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CN201810004852.6A Active CN108084771B (zh) | 2015-04-04 | 2015-04-04 | 一种交联剂组合物及其涂料 |
Country Status (1)
Country | Link |
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CN (2) | CN104788721B (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105646317A (zh) * | 2016-01-18 | 2016-06-08 | 上海华谊(集团)公司 | 三羟甲基丙烷三[3-(2-甲基氮丙啶基)丙酸酯]的制备方法 |
CN109678774A (zh) * | 2018-12-25 | 2019-04-26 | 西安近代化学研究所 | 一种氮丙环类化合物的存储方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101392108A (zh) * | 2008-11-06 | 2009-03-25 | 武汉市强龙化工新材料有限责任公司 | 氮丙啶类三官能团室温交联剂在水中稳定的稳定剂 |
CN102643452A (zh) * | 2011-02-16 | 2012-08-22 | 中国中化股份有限公司 | 一种改进氮丙啶交联剂稳定性的方法 |
CN103540217A (zh) * | 2013-10-08 | 2014-01-29 | 广东雅图化工有限公司 | 一种用氮丙啶交联的丙烯酸酯树脂双组份水性汽车涂料及其制备方法 |
-
2015
- 2015-04-04 CN CN201510156898.6A patent/CN104788721B/zh not_active Expired - Fee Related
- 2015-04-04 CN CN201810004852.6A patent/CN108084771B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101392108A (zh) * | 2008-11-06 | 2009-03-25 | 武汉市强龙化工新材料有限责任公司 | 氮丙啶类三官能团室温交联剂在水中稳定的稳定剂 |
CN102643452A (zh) * | 2011-02-16 | 2012-08-22 | 中国中化股份有限公司 | 一种改进氮丙啶交联剂稳定性的方法 |
CN103540217A (zh) * | 2013-10-08 | 2014-01-29 | 广东雅图化工有限公司 | 一种用氮丙啶交联的丙烯酸酯树脂双组份水性汽车涂料及其制备方法 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105646317A (zh) * | 2016-01-18 | 2016-06-08 | 上海华谊(集团)公司 | 三羟甲基丙烷三[3-(2-甲基氮丙啶基)丙酸酯]的制备方法 |
CN109678774A (zh) * | 2018-12-25 | 2019-04-26 | 西安近代化学研究所 | 一种氮丙环类化合物的存储方法 |
Also Published As
Publication number | Publication date |
---|---|
CN108084771A (zh) | 2018-05-29 |
CN108084771B (zh) | 2021-05-25 |
CN104788721B (zh) | 2017-12-12 |
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Effective date of registration: 20171107 Address after: Xi Mei Xinmei road Nanan city Fujian province 362300 Quanzhou City No. 272 building 4 Room 401 Applicant after: Chen Yuling Address before: The middle Tianfu Avenue in Chengdu city Sichuan province 610041 No. 1388 1 8 storey building No. 866 Applicant before: CHENGDU YUYA SCIENCE & TECHNOLOGY CO., LTD. |
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TA01 | Transfer of patent application right | ||
CB03 | Change of inventor or designer information | ||
CB03 | Change of inventor or designer information |
Inventor after: Zhao Xiaolei Inventor after: Bi Ning Inventor after: Li Huijun Inventor after: Cai Hongxin Inventor after: Xu Gaoyuan Inventor before: Xiang Hongxian |
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TA01 | Transfer of patent application right |
Effective date of registration: 20171115 Address after: No. 2001, Henan high tech Zone Century Road, Jiaozuo, Henan Applicant after: Henan Polytechnic University Address before: Xi Mei Xinmei road Nanan city Fujian province 362300 Quanzhou City No. 272 building 4 Room 401 Applicant before: Chen Yuling |
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CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171212 Termination date: 20200404 |