CN104784061A - Spraying cream with lecithin emulsifying thickener system - Google Patents

Spraying cream with lecithin emulsifying thickener system Download PDF

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Publication number
CN104784061A
CN104784061A CN201510193731.7A CN201510193731A CN104784061A CN 104784061 A CN104784061 A CN 104784061A CN 201510193731 A CN201510193731 A CN 201510193731A CN 104784061 A CN104784061 A CN 104784061A
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lecithin
emulsifying
cream frost
thickened systems
emulsifier
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CN201510193731.7A
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CN104784061B (en
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张向阳
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Guangdong Simei Fanghua Biotechnology Co.,Ltd.
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FOSHAN SAM JANE DAILY CHEMICAL Co Ltd
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Abstract

The invention discloses a spraying cream with a lecithin emulsifying thickener system. The spraying cream comprises the following components in mass percent: 0.3-3% of a lecithin emulsifier, 1.0-2.5% of a thixotropic thickener and the balance of a functional additive component, wherein the lecithin emulsifier is natural plant lecithin or a lecithin-containing mixture; the functional additive component is chemically synthesized grease or active component with functional effects or plant refined grease or active component. The spraying cream with the lecithin emulsifying thickener system is high in system stability and high in moisture retention, and is particularly capable of improving the storage manner and using manner of the cream and decreasing the secondary pollution of the skin-protection cream.

Description

A kind of sprayable cream frost with lecithin emulsifying thickened systems
Technical field
The present invention relates to nursing cream frost technical field, particularly relate to a kind of sprayable cream frost with lecithin emulsifying thickened systems.
Background technology
Cream frost, as a conventional category of skin care item, along with the development of age and science and technology, has developed and has derived diversified emulsification system.But be not a lot of at this emulsification system of the cream frost that can spray, or the mastic atomization of ejection is not obvious, major part is all spray with a kind of form of ray always.Conventional cream frost system, because the limitation of emulsification system and thickened systems, mastic is generally all contained in open-top receptacle, and when using, major part is all directly taken out by mastic with hands, like this, not only open-top receptacle increases the directly exposed area of mastic and the external world, increase the risk of mastic secondary pollution, and, directly go to take with hands, direct especially exist secondary pollution to mastic, is unfavorable for the control of product sanitary index.
In addition, traditional emulsifier power is low, and generally all need two kinds of emulsifying agents or coordinate co-emulsifier to use together, and microgranule after emulsifying is larger, do not reach requirement that is nanometer emulsified or microemulsified, the form being unfavorable for equally spraying is taken.In addition, along with people's level of consumption improves, safety, health perception constantly strengthens, the source of emulsifying agent is also recently brought the category considered into when recipe design, the emulsifying agent of some poly(ethylene oxide) types is constantly being abandoned, and the external surfactant also limiting this type in consideration by legislation comes for detention type skin care item.
Summary of the invention
The object of the invention is to propose a kind of sprayable cream frost with lecithin emulsifying thickened systems, system stability is high, and moisture retention is high, and can improve the storing mode of cream frost and take mode, reduces the secondary pollution of cold cream cream body.
For reaching this object, the present invention by the following technical solutions:
A kind of sprayable cream frost with lecithin emulsifying thickened systems, the mass percent of each composition is: 0.3%-3% lecithin emulsifier, 1%-2.5% composition silicate thickening agent, and surplus is functional addO-on therapy;
Described lecithin emulsifier is natural plants lecithin or containing the mixture of lecithin, and described functional addO-on therapy is the oils and fats that refines of the oils and fats of the chemosynthesis with function affect or component or plant or active component.
Preferably, described composition silicate thickening agent is one or more the mixture in Magnesiumaluminumsilicate, lithium magnesium silicate or sodium magnesium silicate.
Preferably, the content of described lecithin emulsifier is 0.5%-2.5%.
Preferably, described functional addO-on therapy is have one or more the mixed function in whitening, defying age, anti-acne, sun-proof, moisturizing or antiallergic component.
Preferably, described functional addO-on therapy contains antiseptic.
The above-mentioned preparation method with the sprayable cream frost of lecithin emulsifying thickened systems, comprises following operation:
A, weighing: according to the dissolution characteristics of material, press oil phase by all materials or aqueous phase classification weighs, and wherein lecithin emulsifier joins oil phase, and thickening agent joins aqueous phase, and antiseptic and essence independently weigh;
B, dissolving, heating: oil phase material is dissolved in oils and fats, being added water by aqueous phase material is heated to more than 80 DEG C and carries out heating hydration;
C, emulsifying: the aqueous phase that hydration is good in step B is pumped in emulsifying pot, in emulsifying pot, 80 DEG C of insulations, start stirring, homogenizing, oil phase component are pumped in emulsifying pot, homogenizing 3-5 minute, stir cooling, are cooled to add antiseptic when 60 DEG C until mastic;
D, discharging, obtain the sprayable cream frost with lecithin emulsifying thickened systems.
Beneficial effect of the present invention: 1, use lecithin and composition silicate thickening agent as emulsifying thickened systems, stable system, mobility is moderate, makes cream frost realize spray atomization under vacuum extruding state, can Direct spraying in skin, easy to use; 2, adopt natural plants lecithin or the mixture containing lecithin as emulsifying agent, not only reach emulsifying effectiveness, also increase the moisture retention of product and the nursing role to skin simultaneously; 3, osculum or approximate airtight receptacle can be contained in, adopt when taking and pump or ejection form, the area reducing mastic and extraneous contact and the chance of following hands to contact; 4, mastic is reduced because of contamination and deterioration and the risk causing skin infection because mastic pollutes.
Detailed description of the invention
Technical scheme of the present invention is further illustrated below by detailed description of the invention.
The selection of emulsification system of the present invention is the key realizing spraying cream frost recipe design, and emulsification system determines the characteristic of mastic.The position that general cream frost system exists by oil water phase, can be divided into Water-In-Oil (W/O) type, or oil-in-water (O/W) type.With surfactant (emulsifying agent) for medium, oil phase at internal layer, is called Water-In-Oil (W/O) type at outer water phase, and aqueous phase at internal layer, is called oil-in-water (W/O) type at outer oil phase.Water-in-oil type mastic is generally by the high molecular surfactant of lipophilic, aqueous phase is coated, and therefore, general water-in-oil type mastic, viscosity is comparatively large, and emulsified particles particle diameter is comparatively large, is unfavorable for spraying.So involved in the present invention can not consider water-in-oil emulsion system by aerosol type emulsification system.
In oil-in-water emulsification system, the surfactant as emulsifying agent generally selects nonionic or anionic, and cationic surfactant or amphoteric surfactant are generally because zest is comparatively strong or foaming characteristic does not better adopt in this field of emulsifying.But traditional emulsifier power is low, generally all need two kinds of emulsifying agents or coordinate co-emulsifier to use together, and microgranule after emulsifying is larger, do not reach requirement that is nanometer emulsified or microemulsified, the form being unfavorable for equally spraying is taken.Emulsifying agent of the present invention using adopt natural origin vegetable lecithin or containing the mixture of lecithin as emulsifying agent, not only reach emulsifying effectiveness, be conducive to taking of Sprayable, the moisture retention of product and the nursing role to skin can also be increased simultaneously.
For involved in the present invention to the emulsifying thickened systems that can spray, thickened systems be another need consider key technical problem.In common cream frost system, conventional thickened systems is all adopt water soluble polymer as thickening stabilizing agent, and these thickening agents not only make mastic thickening but also can make mastic thickening simultaneously, are unfavorable for that mastic sprays.The thickened systems that the present invention adopts is a kind of thixotropic thickened systems, and namely in the absence of external forces, it has certain denseness, after having certain external force, namely can be thinning because being subject to shearing force at once, what have this characteristic has lithium magnesium silicate, sodium magnesium silicate, Magnesiumaluminumsilicate etc.Be combined as emulsifying thickened systems, stable system by lecithin emulsifier and composition silicate thickening agent, mobility is moderate, realize cream frost sprayableization, easy to use, the secondary pollution used can be avoided, extend and use the shelf-life, lecithin emulsifier also has certain moisture-keeping function simultaneously.
Functional addO-on therapy mainly has the compositions such as whitening, anti-acne, defying age, moisturizing, sun-proof, antiallergic, it can be the functional components of chemosynthesis, can be the both effectiveness materials of water solublity such as vitamin C, vitamin B3, arbutin, Trenaxmine, Tai Gemeiting, lactobionic acid; Also can be the active component that plant is refined, can be methylhesperidin, tetrahydrocurcumin, naringenin, naringin two chalcone etc.; But consider the colloidization characteristic of thickened systems, functional addO-on therapy all necessarily requires to be the ionic not strong or ionic additive that addition is few.
The sprayable cream frost that the present invention produces may be used for the fields such as skin nursing products, hair care product, leatherware nursing or household care.
Component example one: the component of the basic sprayable cream frost of humidity-preserving type
Table 1
Component example two: the component of sprayable cream frost of taking care of hair
Table 2
Component example three: the component of the sprayable cream of skin-care type
Table 3
Component example four: the component of the sprayable cream of anti-ageing maintenance type
Table 4
Component example five: the component of sun-proof sprayable frost
Table 5
Below with functional addO-on therapy in component example one-basic sprayable frost of humidity-preserving type for constant concentration, test is carried out to the addition of lecithin emulsifier and thixotropic thickening agent and compares.
The addition impact of embodiment group 1-lecithin emulsifier
The addition of according to the form below 6 mesosilicic acid magnesium lithium weighs, dissolve heating mixing, by canned in spray bottle for the sprayable frost of humidity-preserving type obtained, and emulsification system stability experiment is carried out to spraying frost, mainly comprise viscosity adjustment test and high temperature, low tempertaure storage stability test.
Table 6
Can know from the result of the test of upper table 6, the interpolation of lecithin emulsifier is more, the mobility of mastic is larger, but the stability of product can increase with the interpolation of lecithin emulsifier and reduces, even can not pass through high temperature low tempertaure storage stability test smoothly, in storage, more easily there is the phenomenons such as layering, precipitation, oil impregnate, be unfavorable for storage.Lecithin emulsifier addition is the essential condition forming stability cream frost in 0.01%-4%, is especially applied in the product of cosmetic skin care product, and the stability influence of cream frost the satisfaction of user to cream frost usage degree.Repeat above-mentioned experiment, the interpolation preferable range value obtaining lecithin emulsifier is 0.3%-3%, and more preferably value range is 0.5%-2.5%, makes the emulsifying thickened systems of cream frost can be held in steady statue for a long time.
The addition impact of embodiment group 2-composition silicate thickening agent
According to the form below 7, the addition of composition silicate thickening agent weighs, dissolve heating mixing, by canned in spray bottle for the sprayable frost of humidity-preserving type obtained, and emulsification system stability experiment is carried out to spraying frost, mainly comprise viscosity adjustment test and high temperature, low tempertaure storage stability test.
Table 7
Can know from the result of the test of upper table 7, the interpolation of composition silicate thickening agent is more, the viscosity of mastic is larger, mobility is lower, but the stability of product and the effect that can realize atomization can increase with the interpolation of composition silicate thickening agent and reduce, even can not pass through high temperature low tempertaure storage stability test smoothly, in storage, more easily there is oil impregnate phenomenon, be unfavorable for storage and the too high smoothness that can affect spraying of viscosity.Composition silicate thickening agent addition is the essential condition forming stability cream frost in 1.5%-3%, is especially applied in the product of cosmetic skin care product.Repeat above-mentioned experiment, the interpolation preferable range value obtaining composition silicate thickening agent is 2%-2.5%, makes the emulsifying thickened systems of cream frost can be held in steady statue for a long time, and can keep the smoothness of ejection when being stored in spray bottle.Can obtain from embodiment 2-7 and 2-8, in same system, the interpolation of composition silicate thickening agent is more, if increase the content of lecithin, then can increase the viscosity of the system that these two kinds of materials are formed, good nebulization can not be played, therefore preferably, the lecithin emulsifier contained in spraying cream frost system is 0.3%-3%, and composition silicate thickening agent is 1%-2.5%.
Below know-why of the present invention is described in conjunction with specific embodiments.These describe just in order to explain principle of the present invention, and can not be interpreted as limiting the scope of the invention by any way.Based on explanation herein, those skilled in the art does not need to pay performing creative labour can associate other detailed description of the invention of the present invention, and these modes all will fall within protection scope of the present invention.

Claims (6)

1. one kind has the sprayable cream frost of lecithin emulsifying thickened systems, and it is characterized in that: the mass percent of each composition is: 0.3%-3% lecithin emulsifier, 1%-2.5% composition silicate thickening agent, surplus is functional addO-on therapy;
Described lecithin emulsifier is natural plants lecithin or containing the mixture of lecithin, and described functional addO-on therapy is the oils and fats that refines of the oils and fats of the chemosynthesis with function affect or component or plant or active component.
2. a kind of sprayable cream frost with lecithin emulsifying thickened systems according to claim 1, is characterized in that: described composition silicate thickening agent is one or more the mixture in Magnesiumaluminumsilicate, lithium magnesium silicate or sodium magnesium silicate.
3. a kind of sprayable cream frost with lecithin emulsifying thickened systems according to claim 1, is characterized in that: the content of described lecithin emulsifier is 0.5%-2.5%.
4. a kind of sprayable cream frost with lecithin emulsifying thickened systems according to claim 1, is characterized in that: described functional addO-on therapy is have one or more the mixed function in whitening, defying age, anti-acne, sun-proof, moisturizing or antiallergic component.
5. a kind of sprayable cream frost with lecithin emulsifying thickened systems according to claim 1, is characterized in that: described functional addO-on therapy contains antiseptic.
6. a kind of preparation method with the sprayable cream frost of lecithin emulsifying thickened systems as described in claim 1-5 any one, is characterized in that: comprise following operation:
A, weighing: according to the dissolution characteristics of material, press oil phase by all materials or aqueous phase classification weighs, and wherein lecithin emulsifier joins oil phase, and thickening agent joins aqueous phase, and antiseptic and essence independently weigh;
B, dissolving, heating: oil phase material is dissolved in oils and fats, being added water by aqueous phase material is heated to more than 80 DEG C and carries out heating hydration;
C, emulsifying: the aqueous phase that hydration is good in step B is pumped in emulsifying pot, in emulsifying pot, 80 DEG C of insulations, start stirring, homogenizing, oil phase component are pumped in emulsifying pot, homogenizing 3-5 minute, stir cooling, are cooled to add antiseptic when 60 DEG C until mastic;
D, discharging, obtain the sprayable cream frost with lecithin emulsifying thickened systems.
CN201510193731.7A 2015-04-22 2015-04-22 Lecithin emulsification thickened systems are preparing the application in sprayable cream Active CN104784061B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109106609A (en) * 2018-11-06 2019-01-01 张家港市绮丽日用化学品有限公司 A kind of foot softening cream technique
CN113143797A (en) * 2021-04-20 2021-07-23 东晟源研究院(广州)有限公司 Moisturizing lotion containing composition for improving atomization effect and preparation method thereof
CN115813780A (en) * 2022-03-30 2023-03-21 广东格烯生物科技股份有限公司 Nano-scale yellow-dispelling composition containing tetrahydrocurcumin and preparation method thereof

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CN1883447A (en) * 2006-05-23 2006-12-27 天津郁美净集团有限公司 Quickly absorptive skin-care composition

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109106609A (en) * 2018-11-06 2019-01-01 张家港市绮丽日用化学品有限公司 A kind of foot softening cream technique
CN113143797A (en) * 2021-04-20 2021-07-23 东晟源研究院(广州)有限公司 Moisturizing lotion containing composition for improving atomization effect and preparation method thereof
CN115813780A (en) * 2022-03-30 2023-03-21 广东格烯生物科技股份有限公司 Nano-scale yellow-dispelling composition containing tetrahydrocurcumin and preparation method thereof

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Effective date of registration: 20210201

Address after: 528143 No.3 Xingtang Road, Datang Town, Sanshui District, Foshan City, Guangdong Province

Patentee after: Guangdong Simei Fanghua Biotechnology Co.,Ltd.

Address before: 2 / F and 3 / F, Chuangye North Road, Songgang Songxia Industrial Park, Shishan town, Nanhai District, Foshan City, Guangdong Province

Patentee before: FOSHAN SAM JANE DAILY CHEMICAL Co.,Ltd.

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