CN104774499A - Metal printing ink resistant to corrosion and preparation method thereof - Google Patents
Metal printing ink resistant to corrosion and preparation method thereof Download PDFInfo
- Publication number
- CN104774499A CN104774499A CN201510210906.0A CN201510210906A CN104774499A CN 104774499 A CN104774499 A CN 104774499A CN 201510210906 A CN201510210906 A CN 201510210906A CN 104774499 A CN104774499 A CN 104774499A
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- corrosion resistant
- metal ink
- resistant metal
- chitosan
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/108—Hydrocarbon resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Abstract
The invention belongs to the technical field of printing ink, and particularly relates to metal printing ink resistant to corrosion and a preparation method thereof. The metal printing ink comprises, by weight, 20-30 parts of waterborne polyurethane resin, 33-45 parts of chlorinated polypropylene resin, 25-35 parts of waterborne acrylic resin, 10-20 parts of glycerin monostearate, 10-25 parts of ethyl alcohol, 3-8 parts of chitosan and graphene composite materials, 3-8 parts of auxiliaries, 15-25 parts of metallic pigment, 3-8 parts of hollow glass beads and 1-2 parts of walnut shell flour. According to the metal printing ink resistant to corrosion and the preparation method thereof, all the raw materials achieve the purpose of mutual capacitance, and the corrosion resistance is good.
Description
Technical field
The present invention relates to technical field of ink, particularly relate to a kind of corrosion resistant metal ink and preparation method thereof.
Background technology
Metal ink refers to, with the ink of metallic pigment preparation, have the gloss of metal, and namely gold ink in general, silver-colored ink are this kind of ink.Pigment mainly bronze and the silver powder (copper powder and aluminium powder) of metal ink, also can add other pigment of people to produce the ink with particular color, be referred to as coloring metal ink.
Along with the continuous progress of people's living standard, require constantly to promote to the corrosion resistance nature of metal ink itself, therefore the corrosion-resistant performance need that waits of existing metal ink improves.
Summary of the invention
The object of the invention is the metal ink that a kind of corrosion resistance and good is provided for the deficiencies in the prior art.
Another object of the present invention is the preparation method providing a kind of corrosion resistant metal ink for the deficiencies in the prior art.
The present invention is achieved through the following technical solutions.
A kind of corrosion resistant metal ink, it comprises the raw material of following weight part: waterborne polyurethane resin 20-30 part, chlorinated polypropylene 33-45 part, water-borne acrylic resin 25-35 part, glyceryl monostearate 10-20 part, ethanol 10-25 part, chitosan-graphene composite material 3-8 part, auxiliary agent 3-8 part, metallic pigment 15-25 part, hollow glass micropearl 3-8 part, walnut shell flour 1-2 part.
Particularly, it comprises the raw material of following weight part: waterborne polyurethane resin 20-25 part, chlorinated polypropylene 39-45 part, water-borne acrylic resin 25-30 part, glyceryl monostearate 15-20 part, ethanol 10-18 part, chitosan-graphene composite material 3-5 part, auxiliary agent 6-8 part, metallic pigment 15-20 part, hollow glass micropearl 3-5 part, walnut shell flour 1-2 part.
Particularly, it comprises the raw material of following weight part: waterborne polyurethane resin 26-30 part, chlorinated polypropylene 33-38 part, water-borne acrylic resin 31-35 part, glyceryl monostearate 10-14 part, ethanol 19-25 part, chitosan-graphene composite material 6-8 part, auxiliary agent 3-5 part, metallic pigment 21-25 part, hollow glass micropearl 6-8 part, walnut shell flour 1-2 part.
Particularly, it comprises the raw material of following weight part: waterborne polyurethane resin 23-25 part, chlorinated polypropylene 38-42 part, water-borne acrylic resin 27-33 part, glyceryl monostearate 13-17 part, ethanol 14-19 part, chitosan-graphene composite material 5-7 part, auxiliary agent 5-6 part, metallic pigment 18-22 part, hollow glass micropearl 5-7 part, walnut shell flour 1-2 part.
Particularly, it also comprises nano aluminium oxide 3-5 weight part.
Particularly, auxiliary agent comprises defoamer, tensio-active agent, polyurethane thickener.Defoamer is silicone antifoam agent or natural fats and oils; Tensio-active agent is silicon system tensio-active agent or fluorine system tensio-active agent.
A kind of preparation method of corrosion resistant metal ink, preparation process is as follows: by above-mentioned weight part, first glyceryl monostearate is mixed with ethanol, add waterborne polyurethane resin, chlorinated polypropylene, water-borne acrylic resin under whipped state, after mixing, dispersion, grinding, add chitosan-graphene composite material, ultrasonic grinding 30-40 minute, add all the other raw materials, after stirring, obtain corrosion resistant metal ink.
the present invention has following beneficial effect:corrosion resistant metal ink of the present invention; have the following advantages: glycan-graphene composite material has larger specific surface area; there is between chitosan and Graphene the synergy of enhancing; chitosan-graphene composite material and the synergy such as walnut shell flour, hollow glass micropearl simultaneously; metal ink is made to have corrosion resistant self-shield coating; effectively inhibit the diffusion of corrosives in metal ink, there is good corrosion resistance nature.The each raw material of the present invention reaches the object of mutual tolerance, corrosion resistance and good.
Embodiment
Below in conjunction with embodiment, the present invention is described in detail.
embodiment 1.
A kind of corrosion resistant metal ink, it comprises the raw material of following weight part: waterborne polyurethane resin 20 parts, chlorinated polypropylene 39 parts, water-borne acrylic resin 30 parts, glyceryl monostearate 20 parts, ethanol 10 parts, chitosan-graphene composite material 5 parts, auxiliary agent 6 parts, metallic pigment 15 parts, hollow glass micropearl 5 parts, walnut shell flour 1 part.Metallic pigment are bronze, and auxiliary agent comprises defoamer 2 parts, 2 parts, tensio-active agent, polyurethane thickener 2 parts.Defoamer is silicone antifoam agent (as organic silicon modified by polyether) or natural fats and oils; Tensio-active agent is silicon system tensio-active agent or fluorine system tensio-active agent.
A kind of preparation method of corrosion resistant metal ink, preparation process is as follows: by above-mentioned weight part, first glyceryl monostearate is mixed with ethanol, add waterborne polyurethane resin, chlorinated polypropylene, water-borne acrylic resin under whipped state, after mixing, dispersion, grinding, add chitosan-graphene composite material, ultrasonic grinding 30 minutes, adds all the other raw materials, after stirring, obtain corrosion resistant metal ink.
embodiment 2.
The difference of the present embodiment and embodiment 1 is: a kind of corrosion resistant metal ink, and it comprises the raw material of following weight part: waterborne polyurethane resin 25 parts, chlorinated polypropylene 45 parts, water-borne acrylic resin 25 parts, glyceryl monostearate 15 parts, ethanol 18 parts, chitosan-graphene composite material 3 parts, auxiliary agent 8 parts, metallic pigment 20 parts, hollow glass micropearl 3 parts, walnut shell flour 2 parts.Metallic pigment are silver powder, and auxiliary agent comprises defoamer 2 parts, 3 parts, tensio-active agent, polyurethane thickener 3 parts.
A kind of preparation method of corrosion resistant metal ink, preparation process is as follows: by above-mentioned weight part, first glyceryl monostearate is mixed with ethanol, add waterborne polyurethane resin, chlorinated polypropylene, water-borne acrylic resin under whipped state, after mixing, dispersion, grinding, add chitosan-graphene composite material, ultrasonic grinding 33 minutes, adds all the other raw materials, after stirring, obtain corrosion resistant metal ink.
embodiment 3.
The difference of the present embodiment and embodiment 1 is: a kind of corrosion resistant metal ink, and it comprises the raw material of following weight part: waterborne polyurethane resin 26 parts, chlorinated polypropylene 38 parts, water-borne acrylic resin 31 parts, glyceryl monostearate 14 parts, ethanol 19 parts, chitosan-graphene composite material 8 parts, auxiliary agent 3 parts, metallic pigment 22 parts, hollow glass micropearl 8 parts, walnut shell flour 1 part.Metallic pigment are copper powder, and auxiliary agent comprises defoamer 1 part, 1.5 parts, tensio-active agent, polyurethane thickener 0.5 part.
A kind of preparation method of corrosion resistant metal ink, preparation process is as follows: by above-mentioned weight part, first glyceryl monostearate is mixed with ethanol, add waterborne polyurethane resin, chlorinated polypropylene, water-borne acrylic resin under whipped state, after mixing, dispersion, grinding, add chitosan-graphene composite material, ultrasonic grinding 35 minutes, adds all the other raw materials, after stirring, obtain corrosion resistant metal ink.
embodiment 4.
The difference of the present embodiment and embodiment 1 is: a kind of corrosion resistant metal ink, and it comprises the raw material of following weight part: waterborne polyurethane resin 30 parts, chlorinated polypropylene 33 parts, water-borne acrylic resin 35 parts, glyceryl monostearate 10 parts, ethanol 25 parts, chitosan-graphene composite material 6 parts, auxiliary agent 5 parts, metallic pigment 25 parts, hollow glass micropearl 6 parts, walnut shell flour 2 parts.Metallic pigment are the mixture of 15 parts, silver powder, aluminium powder 10 parts, and auxiliary agent comprises defoamer 1 part, 2 parts, tensio-active agent, polyurethane thickener 2 parts.
A kind of preparation method of corrosion resistant metal ink, preparation process is as follows: by above-mentioned weight part, first glyceryl monostearate is mixed with ethanol, add waterborne polyurethane resin, chlorinated polypropylene, water-borne acrylic resin under whipped state, after mixing, dispersion, grinding, add chitosan-graphene composite material, ultrasonic grinding 38 minutes, adds all the other raw materials, after stirring, obtain corrosion resistant metal ink.
embodiment 5.
The difference of the present embodiment and embodiment 1 is: a kind of corrosion resistant metal ink, and it comprises the raw material of following weight part: waterborne polyurethane resin 23 parts, chlorinated polypropylene 42 parts, water-borne acrylic resin 27 parts, glyceryl monostearate 17 parts, ethanol 14 parts, chitosan-graphene composite material 7 parts, auxiliary agent 5 parts, metallic pigment 18 parts, hollow glass micropearl 7 parts, walnut shell flour 1 part.Metallic pigment are the mixture of bronze 8 parts, 10 parts, silver powder, and auxiliary agent comprises defoamer 2 parts, 1 part, tensio-active agent, polyurethane thickener 2 parts.
A kind of preparation method of corrosion resistant metal ink, preparation process is as follows: by above-mentioned weight part, first glyceryl monostearate is mixed with ethanol, add waterborne polyurethane resin, chlorinated polypropylene, water-borne acrylic resin under whipped state, after mixing, dispersion, grinding, add chitosan-graphene composite material, ultrasonic grinding 40 minutes, adds all the other raw materials, after stirring, obtain corrosion resistant metal ink.
Corrosion resistant metal ink prepared by Application Example 1-5 carries out performance measurement, as table 1.
Table 1
Finally should be noted that; above embodiment is only in order to illustrate technical scheme of the present invention; but not limiting the scope of the invention; although done to explain to the present invention with reference to preferred embodiment; those of ordinary skill in the art is to be understood that; can modify to technical scheme of the present invention or equivalent replacement, and not depart from essence and the scope of technical solution of the present invention.
Claims (7)
1. a corrosion resistant metal ink, it is characterized in that, it comprises the raw material of following weight part: waterborne polyurethane resin 20-30 part, chlorinated polypropylene 33-45 part, water-borne acrylic resin 25-35 part, glyceryl monostearate 10-20 part, ethanol 10-25 part, chitosan-graphene composite material 3-8 part, auxiliary agent 3-8 part, metallic pigment 15-25 part, hollow glass micropearl 3-8 part, walnut shell flour 1-2 part.
2. corrosion resistant metal ink according to claim 1, it is characterized in that, it comprises the raw material of following weight part: waterborne polyurethane resin 20-25 part, chlorinated polypropylene 39-45 part, water-borne acrylic resin 25-30 part, glyceryl monostearate 15-20 part, ethanol 10-18 part, chitosan-graphene composite material 3-5 part, auxiliary agent 6-8 part, metallic pigment 15-20 part, hollow glass micropearl 3-5 part, walnut shell flour 1-2 part.
3. corrosion resistant metal ink according to claim 1, it is characterized in that, it comprises the raw material of following weight part: waterborne polyurethane resin 26-30 part, chlorinated polypropylene 33-38 part, water-borne acrylic resin 31-35 part, glyceryl monostearate 10-14 part, ethanol 19-25 part, chitosan-graphene composite material 6-8 part, auxiliary agent 3-5 part, metallic pigment 21-25 part, hollow glass micropearl 6-8 part, walnut shell flour 1-2 part.
4. corrosion resistant metal ink according to claim 1, it is characterized in that, it comprises the raw material of following weight part: waterborne polyurethane resin 23-25 part, chlorinated polypropylene 38-42 part, water-borne acrylic resin 27-33 part, glyceryl monostearate 13-17 part, ethanol 14-19 part, chitosan-graphene composite material 5-7 part, auxiliary agent 5-6 part, metallic pigment 18-22 part, hollow glass micropearl 5-7 part, walnut shell flour 1-2 part.
5. corrosion resistant metal ink according to claim 1, is characterized in that, it also comprises nano aluminium oxide 3-5 weight part.
6. corrosion resistant metal ink according to claim 1, is characterized in that, auxiliary agent comprises defoamer, tensio-active agent, polyurethane thickener.
7. the preparation method of the corrosion resistant metal ink of claim 1 to 6 any one, it is characterized in that, preparation process is as follows: by above-mentioned weight part, first glyceryl monostearate is mixed with ethanol, waterborne polyurethane resin, chlorinated polypropylene, water-borne acrylic resin is added under whipped state, after mixing, dispersion, grinding, add chitosan-graphene composite material, ultrasonic grinding 30-40 minute, add all the other raw materials, after stirring, obtain corrosion resistant metal ink.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510210906.0A CN104774499A (en) | 2015-04-29 | 2015-04-29 | Metal printing ink resistant to corrosion and preparation method thereof |
| PCT/CN2015/094282 WO2016173237A1 (en) | 2015-04-29 | 2015-11-11 | Corrosion resistant metallic printing ink and preparation method therefor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510210906.0A CN104774499A (en) | 2015-04-29 | 2015-04-29 | Metal printing ink resistant to corrosion and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104774499A true CN104774499A (en) | 2015-07-15 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510210906.0A Pending CN104774499A (en) | 2015-04-29 | 2015-04-29 | Metal printing ink resistant to corrosion and preparation method thereof |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN104774499A (en) |
| WO (1) | WO2016173237A1 (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105482026A (en) * | 2016-01-06 | 2016-04-13 | 上海墨传新材料科技有限公司 | Water-soluble acrylic resin spherical particles and preparation method thereof |
| CN105860705A (en) * | 2016-04-26 | 2016-08-17 | 安徽康瑞鑫电子科技有限公司 | Antirust paint |
| WO2016173237A1 (en) * | 2015-04-29 | 2016-11-03 | 张双峰 | Corrosion resistant metallic printing ink and preparation method therefor |
| CN109233457A (en) * | 2018-10-09 | 2019-01-18 | 福建师范大学福清分校 | A kind of graphene-based water paint of anti-freezing type for deep-sea engineering |
| CN109969548A (en) * | 2017-12-28 | 2019-07-05 | 战马（北京）饮料有限公司 | A kind of more sense of touch regions tank body |
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| JPH0457866A (en) * | 1990-06-26 | 1992-02-25 | Sanei Kagaku Kk | Hole-filling ink for manufacturing copper through-hole printed wiring board |
| CN101717596A (en) * | 2009-12-08 | 2010-06-02 | 杭华油墨化学有限公司 | Water-based ink for package printing of high-adhesion film and manufacturing method thereof |
| CN102093781A (en) * | 2011-01-27 | 2011-06-15 | 广东天龙油墨集团股份有限公司 | Aqueous metal ink and preparation method thereof |
| CN102964917A (en) * | 2012-11-23 | 2013-03-13 | 东莞市佳烨化工科技有限公司 | Water-based offset print anti-forgery ink and method for preparing same |
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| JP2002226758A (en) * | 2001-02-01 | 2002-08-14 | Toyo Ink Mfg Co Ltd | Aqueous binder, water-base ink composition, and laminate using the same |
| CN101457052B (en) * | 2008-09-25 | 2011-01-26 | 黄山市新力油墨化工厂 | Gravure transparent ink and preparation method thereof |
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| CN102061113B (en) * | 2011-01-31 | 2013-06-26 | 郑州峰源油墨有限公司 | Alcohol soluble polyurethane gravure plastic ink and preparation method thereof |
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2015
- 2015-04-29 CN CN201510210906.0A patent/CN104774499A/en active Pending
- 2015-11-11 WO PCT/CN2015/094282 patent/WO2016173237A1/en active Application Filing
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPH0457866A (en) * | 1990-06-26 | 1992-02-25 | Sanei Kagaku Kk | Hole-filling ink for manufacturing copper through-hole printed wiring board |
| CN101717596A (en) * | 2009-12-08 | 2010-06-02 | 杭华油墨化学有限公司 | Water-based ink for package printing of high-adhesion film and manufacturing method thereof |
| CN102093781A (en) * | 2011-01-27 | 2011-06-15 | 广东天龙油墨集团股份有限公司 | Aqueous metal ink and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016173237A1 (en) * | 2015-04-29 | 2016-11-03 | 张双峰 | Corrosion resistant metallic printing ink and preparation method therefor |
| CN105482026A (en) * | 2016-01-06 | 2016-04-13 | 上海墨传新材料科技有限公司 | Water-soluble acrylic resin spherical particles and preparation method thereof |
| CN105860705A (en) * | 2016-04-26 | 2016-08-17 | 安徽康瑞鑫电子科技有限公司 | Antirust paint |
| CN109969548A (en) * | 2017-12-28 | 2019-07-05 | 战马（北京）饮料有限公司 | A kind of more sense of touch regions tank body |
| CN109233457A (en) * | 2018-10-09 | 2019-01-18 | 福建师范大学福清分校 | A kind of graphene-based water paint of anti-freezing type for deep-sea engineering |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2016173237A1 (en) | 2016-11-03 |
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