CN102250512B - Screen printing ink for polypropylene material - Google Patents
Screen printing ink for polypropylene material Download PDFInfo
- Publication number
- CN102250512B CN102250512B CN 201110021807 CN201110021807A CN102250512B CN 102250512 B CN102250512 B CN 102250512B CN 201110021807 CN201110021807 CN 201110021807 CN 201110021807 A CN201110021807 A CN 201110021807A CN 102250512 B CN102250512 B CN 102250512B
- Authority
- CN
- China
- Prior art keywords
- printing ink
- screen printing
- polypropylene material
- polyolefin resin
- chlorinated polyolefin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 239000000463 material Substances 0.000 title claims abstract description 47
- 239000004743 Polypropylene Substances 0.000 title claims abstract description 38
- 229920001155 polypropylene Polymers 0.000 title claims abstract description 37
- 238000007650 screen-printing Methods 0.000 title claims abstract description 37
- -1 polypropylene Polymers 0.000 title claims abstract description 27
- 229920005672 polyolefin resin Polymers 0.000 claims abstract description 18
- 125000005575 polycyclic aromatic hydrocarbon group Chemical group 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 25
- 239000013530 defoamer Substances 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 13
- 239000000853 adhesive Substances 0.000 claims description 11
- 239000003795 chemical substances by application Substances 0.000 claims description 11
- 230000008719 thickening Effects 0.000 claims description 11
- 239000002270 dispersing agent Substances 0.000 claims description 8
- 238000009736 wetting Methods 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 7
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Polymers C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 6
- 150000002148 esters Chemical group 0.000 claims description 5
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Polymers COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical class O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 3
- 239000000975 dye Substances 0.000 claims description 3
- 239000000049 pigment Substances 0.000 claims description 3
- 229920001296 polysiloxane Polymers 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 239000003921 oil Substances 0.000 abstract description 3
- 229920001225 polyester resin Polymers 0.000 abstract 2
- 239000004645 polyester resin Substances 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000002932 luster Substances 0.000 abstract 1
- 235000019198 oils Nutrition 0.000 abstract 1
- 235000015112 vegetable and seed oil Nutrition 0.000 abstract 1
- 239000008158 vegetable oil Substances 0.000 abstract 1
- 238000007639 printing Methods 0.000 description 7
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000006185 dispersion Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- IBMRTYCHDPMBFN-UHFFFAOYSA-N Mono-Me ester-Pentanedioic acid Natural products COC(=O)CCCC(O)=O IBMRTYCHDPMBFN-UHFFFAOYSA-N 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 2
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 150000002170 ethers Chemical class 0.000 description 2
- 235000019439 ethyl acetate Nutrition 0.000 description 2
- 238000009775 high-speed stirring Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- YNPNZTXNASCQKK-UHFFFAOYSA-N phenanthrene Chemical compound C1=CC=C2C3=CC=CC=C3C=CC2=C1 YNPNZTXNASCQKK-UHFFFAOYSA-N 0.000 description 2
- BBEAQIROQSPTKN-UHFFFAOYSA-N pyrene Chemical compound C1=CC=C2C=CC3=CC=CC4=CC=C1C2=C43 BBEAQIROQSPTKN-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 208000005623 Carcinogenesis Diseases 0.000 description 1
- MUXOBHXGJLMRAB-UHFFFAOYSA-N Dimethyl succinate Chemical compound COC(=O)CCC(=O)OC MUXOBHXGJLMRAB-UHFFFAOYSA-N 0.000 description 1
- 239000011717 all-trans-retinol Substances 0.000 description 1
- 235000019169 all-trans-retinol Nutrition 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000036952 cancer formation Effects 0.000 description 1
- 231100000504 carcinogenesis Toxicity 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- GVEPBJHOBDJJJI-UHFFFAOYSA-N fluoranthrene Natural products C1=CC(C2=CC=CC=C22)=C3C2=CC=CC3=C1 GVEPBJHOBDJJJI-UHFFFAOYSA-N 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
Images
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- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a screen printing ink for a polypropylene material. The screen printing ink does not contain polycyclic aromatic hydrocarbons and comprises the following components in percentage by weight: 40-80% of chlorinated polyolefin resin solution and 6-30% of polyester resin solution. The screen printing ink prepared from the chlorinated polyolefin resin solution and polyester resin solution which have good adhesion to the polypropylene material and are used as main materials, not only does not contain PAHS (polycyclic aromatic hydrocarbons), but also has the advantages of good screenability, excellent leveling property, bright luster and good adhesion to treated and partially untreated surfaces of the PP (polypropylene) materials; and the ink film has excellent resistance to alcohol, vegetable oil and white oil.
Description
Technical field
The present invention relates to screen printing ink, relate in particular to a kind of PAHS(polycyclic aromatic hydrocarbons that do not contain) the polypropylene material screen printing ink.
Background technology
PAHS is the abbreviation of polynuclear aromatics, refers to contain in the molecule hydrocarbon polymer of 2 above phenyl ring, comprises kind of compound surplus naphthalene, anthracene, phenanthrene, the pyrene etc. 150, and human body is had carcinogenesis.At ink area, PAHS extensively is present in the aromatic series kind solvent and some toners that uses in the printing ink, and HUMAN HEALTH and environment are all had bigger harm.
Along with the raising of social development and human environmental consciousness, PAHS is by the countries in the world wide limits, is made in January, 2007 as technical equipment and consumer's goods board of management (ATAV) to add PAHS in the product G S verification process and test this Compulsory Feature.From on April 1st, 2008, the GS certificate of issuing required compulsory implement polynuclear aromatics file ZEK01-08.Existing polypropylene (PP) class printing ink, because of containing PAHS, its application progressively is restricted more.
Therefore, prior art awaits improving and development.
Summary of the invention
Problem to be solved by this invention is to provide a kind of PAHS(polycyclic aromatic hydrocarbons that do not contain) the polypropylene material screen printing ink.
In order to solve the problems of the technologies described above, technical scheme of the present invention is as follows:
A kind of polypropylene material screen printing ink does not contain polycyclic aromatic hydrocarbons in its component, comprise the component that weight percent is following:
Chlorinated polyolefin resin liquid 40-80;
Vibrin liquid 6-30.
Described polypropylene material screen printing ink further comprises the component that weight percent is following:
Wetting dispersing agent 0.1-5;
Toner 4-50.
Described polypropylene material screen printing ink, the solids content of described chlorinated polyolefin resin liquid are more than or equal to 40%, and solvent is an esters solvent; The solids content of described vibrin liquid is more than or equal to 30%, and solvent is an esters solvent.
Described polypropylene material screen printing ink, described wetting dispersing agent are the polyurethane-modified acrylic acid multipolymer; Described toner is inorganic or pigment dyestuff.
Described polypropylene material screen printing ink further comprises the component that weight percent is following:
Thickening material 0.5-10;
Adhesive agent 1-10;
Defoamer 0.1-3;
Flow agent 0.1-3.
Described polypropylene material screen printing ink, described thickening material are the aerosil class.
Described polypropylene material screen printing ink, described defoamer are silicon defoamer.
Described polypropylene material screen printing ink, described adhesive agent are the lower molecular weight chlorinated polyolefin resin.
Described polypropylene material screen printing ink, described flow agent are silicone based.
Described polypropylene material screen printing ink, described screen printing ink are under 20 ℃ of room temperatures, and its viscosity is 5000-30000CPS.
Adopt such scheme, the present invention is the screen printing ink that major ingredient makes polypropylene material is adhered to good chlorinated polyolefin resin liquid and vibrin liquid, not only do not contain PAHS, and it is good to cross net, the levelling property excellence, gloss is brighter, at the treated and untreated PP material surface of part good sticking power is arranged, and ink film ethanol-tolerant, anti-vegetables oil, white spirit excellent property.
Description of drawings
Fig. 1 does not have effect and the physical and chemical index state table of PAHS screen printing ink on treated PP material for embodiment of the invention gained.
Embodiment
Below, preferred embodiment of the present invention is described in further detail.
The invention provides a kind of PP material with no PAHS screen printing ink, its consisting of by weight percentage:
Chlorinated polyolefin resin liquid 50-80;
Vibrin liquid 10-30;
Thickening material 0.5-10;
Adhesive agent 1-10;
Defoamer 0.1-3;
Flow agent 0.1-3.
This PP material with the percentage composition of no PAHS screen printing ink optimum weight is:
Chlorinated polyolefin resin liquid 65;
Vibrin liquid 20;
Thickening material 2;
Adhesive agent 10;
Defoamer 1.5;
Flow agent 1.5.
In another program of the present invention, the PP material is with no PAHS screen printing ink consisting of by weight percentage:
Chlorinated polyolefin resin liquid 40-70;
Vibrin liquid 6-30;
Wetting dispersing agent 0.1-5;
Toner 4-50;
Thickening material 0.5-10;
Adhesive agent 1-10;
Defoamer 0.1-3;
Flow agent 0.1-3.
This PP material with the percentage composition of no PAHS screen printing ink optimum weight is:
Chlorinated polyolefin resin liquid 65;
Vibrin liquid 18;
Wetting dispersing agent 1;
Toner 8;
Thickening material 1;
Adhesive agent 5;
Defoamer 1;
Flow agent 1.
Specifically, described chlorinated polyolefin resin liquid, vibrin liquid is the dispersion liquid of solid resin and solvent mechanical stirring gained, the liquid-solid body burden of described chlorinated polyolefin resin is equal to or greater than 40%, solvent is esters solvents such as pure ethers acetic ester, dimethyl succinate, Methyl glutarate, the liquid-solid body burden of vibrin is equal to or greater than 30%, and solvent is pure ethers acetic ester.
Described wetting dispersing agent is the polyurethane-modified acrylic acid multipolymer, and its effect is to help the dispersion of toner in system, improves mill efficiency, shortens milling time, and keeps the stable of ink system in storage process, prevents toner gathering flocculation.The adhesive agent main component is low-molecular-weight chlorinated polyolefin resin, and its effect is to increase the sticking power of coating on polypropylene material.Thickening material is the aerosil class, and effect is to adjust the printing ink state, improves printing performance, (occurring shrinkage cavity when for example preventing ink printing), the stability of raising ink system.Flow agent is silicone based, can improve levelling property, brushability, the film forming properties of printing ink.Defoamer is a silicon defoamer, and effect is to reduce the bubble that is produced in manufacturing and the use.Described toner is inorganic or pigment dyestuff.
This screen printing ink is under 20 ℃ of room temperatures, and its viscosity is 5000-30000CPS, detects by the ZEK01-08 file standard, and PAHS content is up to specification.
The present invention also provides the Application Areas of this screen printing ink, can be used for the PP material of industries such as plastic cement, packing, stationery.
Contribution of the present invention is, it has effectively overcome PAHS pollution problem common in the existing solvent-borne type screen printing ink, it is good that this printing ink is crossed net, the levelling property excellence, gloss is brighter, at the treated and untreated PP material surface of part good sticking power is arranged, and ink film ethanol-tolerant, anti-vegetables oil, white spirit excellent property.
Embodiment 1
Get 70 parts of chlorinated polyolefin resin liquid (weight), 14 parts of vibrin liquid (weight), 5 parts of adhesive agent (weight), 1.5 parts of thickening materials (weight) stir after the mixing, after three-roller grinds dispersion, add 1.5 parts of defoamers (weight), 1.5 parts of flow agents (weight), it is even to re-use the stirrer high-speed stirring, gets product.
Embodiment 2
Get 65 parts of chlorinated polyolefin resin liquid (weight), 18 parts of vibrin liquid (weight), 5 parts of adhesive agent (weight), 1 part of wetting dispersing agent (weight), stir, slowly add 8 parts of toners (weight) again, 1 part of thickening material (weight), stir, reach below the 10 ц m through the three-roller mesh-of-grind, add 1 part of defoamer again, 1 part of flow agent, high-speed stirring is even, gets product.
Above embodiment gained do not have the PAHS screen printing ink on treated PP material with 300 order screen paintings, test its effect and physical and chemical index state.Test result is seen shown in Figure 1.
Should be understood that, for those of ordinary skills, can be improved according to the above description or conversion, and all these improvement and conversion all should belong to the protection domain of claims of the present invention.
Claims (7)
1. a polypropylene material screen printing ink does not contain polycyclic aromatic hydrocarbons in its component, it is characterized in that, comprises the component that weight percent is following:
Chlorinated polyolefin resin liquid 40-80;
Vibrin liquid 6-30;
Wetting dispersing agent 0.1-5;
Toner 4-50;
Thickening material 0.5-10;
Adhesive agent 1-10;
Defoamer 0.1-3;
Flow agent 0.1-3;
The solids content of described chlorinated polyolefin resin liquid is more than or equal to 40%, and solvent is an esters solvent; The solids content of described vibrin liquid is more than or equal to 30%, and solvent is an esters solvent.
2. polypropylene material screen printing ink according to claim 1 is characterized in that, described wetting dispersing agent is the polyurethane-modified acrylic acid multipolymer; Described toner is inorganic or pigment dyestuff.
3. polypropylene material screen printing ink according to claim 1 is characterized in that, described thickening material is the aerosil class.
4. polypropylene material screen printing ink according to claim 1 is characterized in that, described defoamer is a silicon defoamer.
5. polypropylene material screen printing ink according to claim 1 is characterized in that, described adhesive agent are the lower molecular weight chlorinated polyolefin resin.
6. polypropylene material screen printing ink according to claim 1 is characterized in that, described flow agent is silicone based.
7. polypropylene material screen printing ink according to claim 1 is characterized in that, described screen printing ink is under 20 ℃ of room temperatures, and viscosity is 5000-30000CPS.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110021807 CN102250512B (en) | 2011-01-19 | 2011-01-19 | Screen printing ink for polypropylene material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110021807 CN102250512B (en) | 2011-01-19 | 2011-01-19 | Screen printing ink for polypropylene material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102250512A CN102250512A (en) | 2011-11-23 |
| CN102250512B true CN102250512B (en) | 2013-07-31 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110021807 Expired - Fee Related CN102250512B (en) | 2011-01-19 | 2011-01-19 | Screen printing ink for polypropylene material |
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| Country | Link |
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| CN (1) | CN102250512B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3281991A4 (en) * | 2015-04-06 | 2018-09-26 | Kao Corporation | Aqueous ink |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103351718B (en) * | 2013-07-23 | 2015-01-07 | 东莞市卓艺印刷制品有限公司 | 3D stereoscopic printing ink, and transfer film provided with 3D stereoscopic decorative layer and made by same |
| CN104804537A (en) * | 2015-04-22 | 2015-07-29 | 黎司华 | Low-temperature curing silk-screen printing ink for polypropylene materials |
| CN104774499A (en) * | 2015-04-29 | 2015-07-15 | 韦利束 | Metal printing ink resistant to corrosion and preparation method thereof |
| CN106280701A (en) * | 2016-08-08 | 2017-01-04 | 惠州市至上新材料有限公司 | A kind of aqueous, environmental protective sand streak gravure ink |
| WO2024029099A1 (en) * | 2022-08-04 | 2024-02-08 | Dic株式会社 | Laminate ink composition for flexible packaging |
| JP7355271B1 (en) * | 2022-08-04 | 2023-10-03 | Dic株式会社 | Laminating ink composition for flexible packaging |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1457351A (en) * | 2001-02-16 | 2003-11-19 | 日本制纸株式会社 | Resin composition for printing ink and process for producing the same |
| CN101415770A (en) * | 2006-04-05 | 2009-04-22 | 东洋化成工业株式会社 | Adhesive resin composition |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3988076B2 (en) * | 2002-06-21 | 2007-10-10 | ハリマ化成株式会社 | Method for producing resin varnish for printing ink |
-
2011
- 2011-01-19 CN CN 201110021807 patent/CN102250512B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1457351A (en) * | 2001-02-16 | 2003-11-19 | 日本制纸株式会社 | Resin composition for printing ink and process for producing the same |
| CN101415770A (en) * | 2006-04-05 | 2009-04-22 | 东洋化成工业株式会社 | Adhesive resin composition |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3281991A4 (en) * | 2015-04-06 | 2018-09-26 | Kao Corporation | Aqueous ink |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102250512A (en) | 2011-11-23 |
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Legal Events
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
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| ASS | Succession or assignment of patent right |
Owner name: SHENZHEN MEILIHUA INK + COATING CO., LTD. Free format text: FORMER OWNER: YIKE INKS + PAINTS (SHENGZHEN) CO., LTD. Effective date: 20120330 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20120330 Address after: 518103, Feng Tong Road 243, Fuyong Town, Shenzhen, Guangdong, Baoan District Applicant after: Shenzhen Meilihua Ink & Coating Co., Ltd. Address before: 518103 Guangdong city of Shenzhen province Baoan District Fuyong Whitehead industrial district Applicant before: Yike Inks & Paints (Shengzhen) Co., Ltd. |
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Address after: Shenzhen, Guangdong, Baoan District province Fuyong street, Feng Tong Avenue and Yonghe Road intersection Patentee after: Shenzhen beautiful Polytron Technologies Inc Address before: 518103, Feng Tong Road 243, Fuyong Town, Shenzhen, Guangdong, Baoan District Patentee before: Shenzhen Meilihua Ink & Coating Co., Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130731 Termination date: 20190119 |