CN104770489A - Composition having anti-oxidation function and preparation method thereof - Google Patents
Composition having anti-oxidation function and preparation method thereof Download PDFInfo
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- CN104770489A CN104770489A CN201410015102.0A CN201410015102A CN104770489A CN 104770489 A CN104770489 A CN 104770489A CN 201410015102 A CN201410015102 A CN 201410015102A CN 104770489 A CN104770489 A CN 104770489A
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Abstract
The invention relates to a composition having an anti-oxidation function and a preparation method thereof. The composition is composed of jujube, hawthorn, wolfberry, green tea or extracts thereof. Experiments confirm that the composition can significantly reduce the content of lipid peroxide of old-aging rats, D-galactose peroxidation damage model rats and bromobenzene model mice, improves the activity of antioxidase, reduces the content of lipid peroxide of test-meal human bodies, improves the content of superoxide dismutase and glutathion peroxidase of the test-meal human bodies, and has the antioxidation activity.
Description
Technical field
The present invention relates to a kind of composition and method of making the same with anti-oxidation function.
Background technology
Free radical refers to atom, molecule or group containing unpaired electronics, owing to containing unpaired electron in free radical, has the tendency of pairing, and situation is unstable, has the activity of height.Free radical is paired to the stable electronics of oneself that must make to contiguous atom or molecule abstracts electronics, but also therefore makes electronics be become new free radical by that atom of taking by force or molecule, causes chain reaction.This process is exactly " oxidation ".
Under normal circumstances, the free radical in human body is among the continuous dynamic equilibrium produced and remove.Free radical produces too much or removed slow, will attack life macromolecule material and various cell, cause body in the various damages of molecular level, cellular level and histoorgan level, accelerate the senescence process of body and bring out various disease.Research confirms, has at least the disease of more than 70 kinds relevant with free radical.If tumour is because free radical attacks DNA, caused by the transformation causing cytogenetics information; Cardiovascular and cerebrovascular disease is because free radical can make lipid peroxidation, causes artery sclerosis; Hypoimmunity is because free radical can destroy eucaryotic cell structure, affects the normal immunologic function of cells play; Cataract is that free radical attacks crystalline lens generation; Senile dementia is that free radical is invaded caused by brain cell and nerve.Can say, free radical is " sources of ten thousand diseases ".
Polyphenoils can be act directly on free radical, or indirectly consumes the material easily generating free radical, prevents further reaction.Human body while inevitably producing free radical, also naturally producing the polyphenoils resisting free radical, offsetting the oxidative attacks of radical pair human body cell.Research proves, the antioxidant system of human body be one can comparable with immune system, have and improve and the system of complicated function, the oxidation resistant ability of body is stronger, more healthy, and life is also longer.
After people a to dating, in body, the quantity of spontaneous polyphenoils will reduce year by year, at this moment just there will be significantly old and feeble and unhealthy status.And the polyphenoils produced in person in middle and old age's human body is obviously not enough especially, so need to supplement.Along with the raising of Levels of Social Economic Development and the enhancing of people ' s health consciousness, people recognize the anti-oxidant importance to health more and more, and oxidation resistant product also receives the concern of people more and more.In recent years, from natural animal-plant, from the Chinese herbal medicine with long history, especially find efficient free radical scavenger has become a kind of trend, therefore develops the product with anti-oxidation function and has wide market prospects.
Date is rich in the nutritional labelings such as carbohydrate, cellulose, vitamin, amino acid, protein, mineral matter, particularly containing polysaccharide, rutin, CAMP isoreactivity composition, is the health food of integration of drinking and medicinal herbs, has very high nutritive value.Theory of traditional Chinese medical science is thought, date has effect such as qi-restoratives benefit gas, nourishing blood and tranquilization, strengthening the spleen and stomach etc., is the good health nutrient of the patients such as weakness of the spleen and the stomach, insufficiency of vital energy and blood, lassitude, insomnia and dreamful sleep.Modern study shows, date polysaccharide all has antioxidation to the various active oxygens in human body, is even better than alpha-tocopherol.Experiment proves, date polysaccharide to have a certain impact effect to rat blood serum free radical.
Hawthorn contains the number of chemical compositions such as flavonoids, flavane and polymer class thereof, triterpenes and organic acid, as medicine-food two-purpose good merchantable brand, except clinical, is also widely used in each fields such as food, beverage, health products.Flavone of hawthorn fruit is a compounds of generally acknowledged most antioxidation potential, has remove and generate inhibitory action hydroxy radical and superoxide anion.
Matrimony vine is rich in own polysaccharide, several amino acids, trace element, vitamin, taurine, alkaloid, volatile oil, and be exactly the excellent tonic product of medicine-food two-purpose since ancient times, Shennong's Herbal is classified as top grade, call it ": take hard muscles and bones for a long time, make light of one's life by commiting suicide old, resistance to cold and heat." modern study shows; LBP-X can improve D-galactolipin institute Aging mice body glutathion inside peroxidase and superoxide dismutase activity; thus excessive free radical can be removed, and reduce MDA and lipofuscin content, have the ability of stronger elimination oxygen radical.Show the research of Lycium barbarum polysaccharides antioxidation activity, Lycium barbarum polysaccharides is better to the elimination effect of hydroxyl radical free radical, and its clearance rate is higher than vitamin C.
Green tea is one of large teas of China six, belongs to azymic tea, the more natural materials remained in fresh leaf.Wherein Tea Polyphenols, caffeine retain more than 85% of fresh leaf, and chlorophyll retains about 50%, and vitamin loss is also less.The traditional Chinese medical science is thought, can refresh oneself on tealeaves, in can promoting digestion to eliminate stagnation, lower can diuresis, be natural health beverages.Shennong's Herbal is recorded: " shennong went into the mountains collecting, tasting and testing different kinds of herbs to be used as medicine, meets 72 poison day, obtain tea and separate it ".Green tea is mainly containing Tea Polyphenols, and caffeine, carbohydrate, the compounds such as flavonoids, have anti-oxidant, antitumor, anti-inflammatory, hypotensive, blood fat and blood sugar, reduce the effects such as cardiovascular and cerebrovascular disease risk factor.Modern study shows, Tea Polyphenols can remove the reactive oxygen species of human body surplus, has extremely strong antioxidation, and its oxidation resistance is 18 times of vitamin E, is ascorbic 3 ~ 10 times.
Therefore, the effective scavenging free radicals of working substance mass-energy that date, matrimony vine, green tea propose is utilized.
Summary of the invention
The object of the invention is to provide a kind of composition and method of making the same with anti-oxidation function.
Hawthorn digestingization is stagnant, blood circulation promoting competent silt; Date tonifying spleen and stomach, nourishing qi and blood promotes the production of body fluid, removing toxic substances.Hawthorn, date are harmonious, and invigorate blood circulation and just do not hinder, not stagnant blood of enriching blood.Matrimony vine filling liver kidney improving eyesight.Green tea refresh oneself, relieving thirst and restlessness, eliminates indigestion and phlegm, and diuresis is detoxified.Matrimony vine and green tea share, and liver kidney must be mended, and the head obtains clearly.There is the effect of good refresh oneself.Hawthorn and green tea phase 5, the power of relieving dyspepsia brings out the best in each other.Date and green tea all can detoxify, and green tea also can restrict the warm nature of date simultaneously.Full side's compatibility is rationally precise and appropriate, mild in medicine property and, be the good recipe prolonged life.
In this composition, each raw material all has scavenging free radicals, oxidation resistant effect, what date in side, hawthorn, the fruit of Chinese wolfberry were that the Ministry of Public Health announces is food and the article list of medicine, one of beverage that Cha Shi world today consumption figure is maximum, it and coffee, cocoa claim the world three large non-alcoholic drink, all have long edible history, and this composition has no side effect through safety evaluatio, can eat for a long time.
Experiment confirms, this composition significantly can reduce old rats, D-galactolipin peroxide injury rat model and bromobenzene model mice LPO and improve antioxidase activity; Reduce the LPO of test-meal human body, improve test-meal human body superoxide dismutase and glutathione peroxidase content, there is antioxidation activity.
The present invention is implemented by the following technical programs.
Said composition can be made up of the raw material of following weight portion:
Date 2-15 part, hawthorn 3-12 part, fruit of Chinese wolfberry 2-12 part, green tea 2-12 part.
The raw material of above-mentioned weight portion can be preferably:
Date 2-5 part, hawthorn 3-6 part, fruit of Chinese wolfberry 2-5 part, green tea 2-5 part.
The raw material of above-mentioned weight portion can be preferably:
3 parts, date, hawthorn 4 parts, the fruit of Chinese wolfberry 3 parts, green tea 3 parts.
The equal Disodium EDTA of date, hawthorn, the fruit of Chinese wolfberry and green tea.The present composition uses with above-mentioned material combination, can Synergistic.
Detailed description of the invention
The present invention is described further by embodiment.
Embodiment 1
The preparation of present composition tea in bag (with 1 people 1000 days with gauge):
Take 3kg date and 4kg hawthorn, the 3kg fruit of Chinese wolfberry, the mixing of 3kg green tea, make tea in bag.
Embodiment 2
The preparation of present composition tea in bag (with 1 people 1000 days with gauge):
Take 5kg date and 6kg hawthorn, the 5kg fruit of Chinese wolfberry, the mixing of 5kg green tea, make tea in bag.
Embodiment 3
The preparation of present composition tea in bag (with 1 people 1000 days with gauge):
Take 2kg date and the section of 3kg hawthorn, mix with the 2kg fruit of Chinese wolfberry and 2kg green tea, make tea in bag.
Embodiment 4
The preparation of present composition tea in bag (with 1 people 1000 days with gauge):
Take 3kg date and the section of 4kg hawthorn, mix with the 3kg fruit of Chinese wolfberry and 3kg green tea, make tea in bag
Embodiment 5
The preparation of present composition tea in bag (with 1 people 1000 days with gauge):
Take 15kg date and the section of 12kg hawthorn, mix with the 12kg fruit of Chinese wolfberry and 12kg green tea, make tea in bag.
Embodiment 6
The preparation of present composition tea in bag (with 1 people 1000 days with gauge):
Take 3kg date, 4kg hawthorn, the 3kg fruit of Chinese wolfberry, 3kg green tea, pulverize, mixing, granulate, make tea in bag.
Embodiment 7
The preparation of present composition tea in bag (with 1 people 1000 days with gauge):
Take 5kg date, 6kg hawthorn, the 5kg fruit of Chinese wolfberry and 5kg green tea, pulverize, mixing, granulate, make tea in bag.
Embodiment 8
The preparation of present composition capsule (with 1 people 1000 days with gauge):
Take 2kg date, the 2kg fruit of Chinese wolfberry adds 60% alcohol extract 3 times, each 0.5 hour, filter, merging filtrate, reclaim ethanol; Take 3kg hawthorn, 2kg green tea extracting in water 3 times, each 1 hour, filter, merging filtrate, merges with said extracted liquid, concentrated, dry, pulverize, and add dextrin mixing, adding PVPK30 ethanolic solution is wetting agent, granulates, and dry, filled capsules, makes capsule.
Embodiment 9
The preparation of present composition tablet (with 1 people 1000 days with gauge):
Take 5kg date, 5kg fruit of Chinese wolfberry extracting in water 2 times, each 1.5 hours, filter, merging filtrate; Take 6kg hawthorn and 5kg green tea adds 20% alcohol extract 2 times, each 1.5 hours, filter, merging filtrate, decompression recycling ethanol, merges with said extracted liquid, concentrated, dry, pulverize, add dextrin and Hydroxypropyl methylcellulose mixing, with PVPK30 ethanolic solution for wetting agent, granulation, drying, add dolomol mixing, compressing tablet, dressing, makes tablet.
Embodiment 10
The preparation of present composition granule (with 1 people 1000 days with gauge):
Take 3kg date, 4kg hawthorn, the 3kg fruit of Chinese wolfberry, 3kg green tea extracting in water 3 times, each 1 hour, filter, filtrate merges, concentrated, dry, pulverize into fine powder, add lactose and dextrin mixing, with 90% ethanolic solution for wetting agent, granulation, drying, make granule.
Embodiment 11
The preparation of present composition granule (with 1 people 1000 days with gauge):
Take 5kg date, the 5kg fruit of Chinese wolfberry adds 50% alcohol extract 1 time, 2 hours, filter, reclaim ethanol; Take 6kg hawthorn, 5kg green tea extracting in water 1 time, 2 hours, filter, merge with said extracted liquid, concentrated, dry, pulverize into fine powder, add aspartame and dextrin mixing, with 70% ethanolic solution for wetting agent, granulation, drying, make granule.
Embodiment 12
The preparation of present composition soft capsule (with 1 people 1000 days with gauge):
Take 3kg date, 4kg hawthorn, the 3kg fruit of Chinese wolfberry, 3kg green tea adds 80% alcohol extract 2 times, each 1 hour, filter, merging filtrate, reclaim ethanol, concentrated, add corn oil, sorbitan mono-oleic acid ester, beeswax, make soft capsule.
Embodiment 13
The preparation of present composition oral liquid (with 1 people 1000 days with gauge):
Take 3kg date and 3kg fruit of Chinese wolfberry extracting in water 2 times, each 1 hour, filter, filtrate merges; Take 4kg hawthorn and add 70% alcohol extract 2 times, filter, decompression filtrate recycling ethanol; Take 3kg green tea and add 60% alcohol extract 2 times, each 1 hour, filter, filtrate merges, and reclaims ethanol, is diluted with water to 4ml/1g crude drug, cross polyamide column, use 50% ethanol elution with after water and 20% ethanol removal of impurities successively, collect eluent, decompression recycling ethanol, merge with said extracted liquid, concentrated, add sucrose and benzoic acid, make oral liquid.
Embodiment 14
The preparation of present composition syrup (with 1 people 1000 days with gauge):
Take 3kg date and 3kg fruit of Chinese wolfberry extracting in water 2 times, each 2 hours, filter, extract merges; Take 4kg hawthorn and 3kg green tea adds 20% alcohol extract 2 times, each 2 hours, filter, filtrate merges, and reclaims ethanol, merges, add sucrose and propionic acid, make syrup with said extracted liquid.
Embodiment 15
The preparation of present composition capsule (with 1 people 1000 days with gauge):
Take 3kg date, 4kg hawthorn, the 3kg fruit of Chinese wolfberry add 80% alcohol extract 1 time, 2 hours, filter, decompression filtrate recycling ethanol; Take 3kg green tea and add 60% ethanol, 75 DEG C of lixiviates 3 times, each 2 hours, filter, filtrate merges, reclaim ethanol, be diluted with water to 4ml/1g crude drug, cross large pore resin absorption column, use 70% ethanol elution with after water and 10% ethanol removal of impurities successively, collect eluent, decompression recycling ethanol; Merge with said extracted liquid, concentrated, dry, pulverize, add microcrystalline cellulose mixing, filled capsules, makes capsule.
Embodiment 16
The preparation of present composition tablet (with 1 people 1000 days with gauge):
Take 3kg date and 3kg fruit of Chinese wolfberry extracting in water 2 times, each 1 hour, filter, extract merges; Take 4kg hawthorn and add 60% alcohol extract 3 times, each 0.5 hour, filter, filtrate merges, decompression recycling ethanol; Take 3kg green tea and add 70% ethanol, 75 DEG C of lixiviates 2 times, each 3 hours, filter, filtrate merges, and reclaims ethanol, is diluted with water to 4ml/1g crude drug, crosses polyamide column, uses 80% ethanol elution successively with after water and 20% ethanol removal of impurities, collects eluent, reclaims ethanol; Merge with said extracted liquid, concentrated, dry, pulverize, add starch mixing, adding PVPK30 ethanolic solution is wetting agent, granulation, drying, and add dolomol mixing, compressing tablet, dressing, makes tablet.
Embodiment 17
The preparation of present composition granule (with 1 people 1000 days with gauge):
Take 3kg date and 3kg fruit of Chinese wolfberry extracting in water 3 times, each 0.5 hour, filter, filtrate merges; Take 4kg hawthorn and add 60% alcohol extract 3 times, each 0.5 hour, filter, filtrate merges, and reclaims ethanol; Take 3kg green tea and add 20% alcohol extract 3 times, each 0.5 hour, filter, filtrate merges, reclaim ethanol, be diluted with water to 4ml/1g crude drug, cross polyamide column, use 50% ethanol elution with after water and 10% ethanol removal of impurities successively, collect eluent, reclaim ethanol, merge with said extracted liquid, concentrated, dry, be ground into fine powder, add aspartame and starch, mixing, with 80% ethanolic solution for wetting agent, granulation, drying, make granule.
Embodiment 18
The preparation of present composition soft capsule (with 1 people 1000 days with gauge):
Take 3kg date and 3kg fruit of Chinese wolfberry extracting in water 2 times, each 1.5 hours, filter, extract merges; Take 4kg hawthorn 80% alcohol extract 2 times, each 1.5 hours, filter, decompression filtrate recycling ethanol; Take 3kg green tea and add 80% alcohol extract 2 times, each 1.5 hours, filter, decompression filtrate recycling ethanol, is diluted with water to 4ml/1g crude drug, crosses polyamide column, use 70% ethanol elution with after water and 30% ethanol removal of impurities successively, collect eluent, reclaim ethanol, merge with said extracted liquid, concentrated, dry, be ground into fine powder, add soybean oil, phosphatide, beeswax, makes soft capsule.
Embodiment 19
The preparation of present composition oral liquid (with 1 people 1000 days with gauge):
Take 3kg date, 4kg hawthorn, 3kg fruit of Chinese wolfberry extracting in water 2 times, each 1 hour, filter, filtrate merges, and takes 3kg green tea and adds 60% alcohol extract 2 times, each 1 hour, filter, decompression filtrate recycling ethanol, is diluted with water to 4ml/1g crude drug, cross large pore resin absorption column, use 70% ethanol elution with after water and 10% ethanol removal of impurities successively, collect eluent, reclaim ethanol, merge with said extracted liquid, concentrated, add lactose and sorbic acid again, make oral liquid.
Embodiment 20
The preparation of present composition syrup (with 1 people 1000 days with gauge):
Take 3kg date and 3kg fruit of Chinese wolfberry extracting in water 3 times, each half an hour, filter, extract merges; Take 4kg hawthorn and add 50% extraction 3 times, each 45 minutes, filter, filtrate merges, reclaim ethanol, take 3kg green tea and add 70% alcohol extract 2 times, each 2 hours, filter, filtrate merges, and reclaims ethanol, is diluted with water to 4ml/1g crude drug, excessive polyamide column, uses 80% ethanol elution with after water and 20% ethanol removal of impurities successively, collects eluent, reclaim ethanol, merge with said extracted liquid, concentrated, merge with said extracted liquid, add sucrose and benzoic acid, make syrup.
Claims (7)
1. have a composition for anti-oxidation function, it is characterized in that, said composition is made up of the raw material of following weight portion: date 2-15 part, hawthorn 3-12 part, fruit of Chinese wolfberry 2-12 part, green tea 2-12 part.
2. composition according to claim 1, is characterized in that, said composition is made up of the raw material of following weight portion: date 2-5 part, hawthorn 3-6 part, fruit of Chinese wolfberry 2-5 part, green tea 2-5 part.
3. composition according to claim 2 is characterized in that, said composition is made up of the raw material of following weight portion: 3 parts, date, hawthorn 4 parts, the fruit of Chinese wolfberry 3 parts, green tea 3 parts.
4. according to claim 1---the preparation method of the composition according to any one of 3, is characterized in that it comprises the following steps:
By the date of described weight proportion, hawthorn, the fruit of Chinese wolfberry, green tea mixing or pulverize, mixing, make tea in bag or the date of described weight proportion, hawthorn are cut into slices, mix with the fruit of Chinese wolfberry of described weight proportion and green tea, make tea in bag.
5. according to claim 1---the preparation method of the composition according to any one of 3, is characterized in that it comprises the following steps:
The date of described weight proportion, hawthorn, the fruit of Chinese wolfberry, green tea added water or 20-80% alcohol extract 1-3 time, each 0.5-2 hour, filters, merging filtrate, concentrated or concentrated after reclaiming ethanol, dry, pulverize, mix with proper auxiliary materials, be prepared into acceptable preparation in pharmacy.
6. according to claim 1---the preparation method of the composition according to any one of 3, is characterized in that it comprises the following steps:
The date of described weight proportion, the fruit of Chinese wolfberry, hawthorn added water or 20-80% alcohol extract 1-3 time, each 0.5-2 hour, filters, decompression recycling ethanol after filtrate merges or merges; Green tea adds 20-80% alcohol extract 1-3 time, each 0.5-3 hour, filters, filtrate merges, decompression recycling ethanol, crosses polyamide column or large pore resin absorption column, use 50%-80% ethanol elution with after water and the removal of impurities of 10%-30% ethanol successively, collect eluent, decompression recycling ethanol, merge with said extracted liquid, concentrated, dry, pulverize, mix with auxiliary material, be prepared into acceptable preparation in pharmacy.
7. the composition according to any one of claim 1-3, for anti-oxidant.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410015102.0A CN104770489A (en) | 2014-01-14 | 2014-01-14 | Composition having anti-oxidation function and preparation method thereof |
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| CN201410015102.0A CN104770489A (en) | 2014-01-14 | 2014-01-14 | Composition having anti-oxidation function and preparation method thereof |
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| CN104770489A true CN104770489A (en) | 2015-07-15 |
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| CN201410015102.0A Pending CN104770489A (en) | 2014-01-14 | 2014-01-14 | Composition having anti-oxidation function and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105124708A (en) * | 2015-09-01 | 2015-12-09 | 殷志杰 | Health care beverage having function of expelling toxins |
| CN105167048A (en) * | 2015-08-14 | 2015-12-23 | 沈凯 | Green tea health drink |
| CN112568352A (en) * | 2020-02-29 | 2021-03-30 | 河北康平健康产业有限责任公司 | Anti-oxidation beauty-maintaining and young-keeping mulberry and lycium ruthenicum solid beverage and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101643483A (en) * | 2009-05-26 | 2010-02-10 | 苏州派腾生物医药科技有限公司 | Process for preparing tea polyphenol |
| CN102499300A (en) * | 2011-11-22 | 2012-06-20 | 西安医学院 | Solid tea having antioxidation function and preparation method thereof |
| CN102696803A (en) * | 2012-05-31 | 2012-10-03 | 绵阳兴川梦想食品科技有限公司 | Jujube tea and method for preparing beverage of same |
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2014
- 2014-01-14 CN CN201410015102.0A patent/CN104770489A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101643483A (en) * | 2009-05-26 | 2010-02-10 | 苏州派腾生物医药科技有限公司 | Process for preparing tea polyphenol |
| CN102499300A (en) * | 2011-11-22 | 2012-06-20 | 西安医学院 | Solid tea having antioxidation function and preparation method thereof |
| CN102696803A (en) * | 2012-05-31 | 2012-10-03 | 绵阳兴川梦想食品科技有限公司 | Jujube tea and method for preparing beverage of same |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105167048A (en) * | 2015-08-14 | 2015-12-23 | 沈凯 | Green tea health drink |
| CN105124708A (en) * | 2015-09-01 | 2015-12-09 | 殷志杰 | Health care beverage having function of expelling toxins |
| CN112568352A (en) * | 2020-02-29 | 2021-03-30 | 河北康平健康产业有限责任公司 | Anti-oxidation beauty-maintaining and young-keeping mulberry and lycium ruthenicum solid beverage and preparation method thereof |
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Application publication date: 20150715 |
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