CN104726215A - Preparation method of sphorus laundry powder - Google Patents
Preparation method of sphorus laundry powder Download PDFInfo
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- CN104726215A CN104726215A CN201510144547.3A CN201510144547A CN104726215A CN 104726215 A CN104726215 A CN 104726215A CN 201510144547 A CN201510144547 A CN 201510144547A CN 104726215 A CN104726215 A CN 104726215A
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Abstract
The invention discloses a preparation method of phosphorus-free laundry powder, which comprises the following steps: putting sodium bicarbonate and hydroxymethyl cellulose into a mixer to uniformly mix; adding sodium dodecyl benzene sulfonate, sodium silicate and sodium perborate, and stirring for 10-30 minutes; adding a fatty acid, and 12 hours later, adding shikakai powder, essences and a fluorescent whitening agent, so that phosphorus-free laundry powder is obtained. The phosphorus-free laundry powder is prepare from the following materials in parts by weight: 3-8 parts of sodium bicarbonate, 1-5 parts of hydroxymethyl cellulose, 16-26 parts of sodium dodecyl benzene sulfonate, 1-6 parts of sodium silicate, 1-4 parts of sodium perborate, 5-10 parts of a fatty acid, 5-10 parts of shikakai powder, 0.1-2 parts of essences, and 0.05-0.5 part of a fluorescent whitening agent. The method disclosed by the invention is wide in raw material source, simple in process, less in production procedure, and simple in production equipment, and prepared laundry powder does not contain phosphorous, produces less foams, and has strong dirt removing power.
Description
Technical field
The invention belongs to household chemicals field, be specifically related to a kind of preparation method of non-phosphide detergent.
Background technology
Washing powder is when washing clothes, and adds to be dissolved in water and cleans, and makes the meal that clothes is more easily cleaned.The composition of washing powder is generally main comprises tensio-active agent, water-softening chemicals, alkaline agent, SYNTHETIC OPTICAL WHITNER etc.Also to add some auxiliary agents and auxiliary during preparation washing powder, make the performance of washing powder more perfect.The general auxiliary agent of washing powder is divided into inorganic salt and the large class of organic salt two, by washing powder whether containing phosphorus, is divided into again Powdered Detergent Containing Phosphate and non-phosphide detergent.With the addition of tripoly phosphate sodium STPP mostly in Powdered Detergent Containing Phosphate, to improve the clean effect of washing powder.But tripoly phosphate sodium STPP has strong impulse effect to skin, and phosphorus very easily brings the ecological damage phenomenons such as water eutrophication, need to eliminate in time to use.
Summary of the invention
Technical problem to be solved by this invention is to provide the preparation method of the non-phosphide detergent that a kind of composition is simple, clean effect is good.
For solving the problem, the present invention will by the following technical solutions:
The preparation method of non-phosphide detergent, step is as follows:
Sodium bicarbonate and Walocel MT 20.000PV are placed in after mixing tank mixes, add Sodium dodecylbenzene sulfonate, water glass and Sodium peroxoborate again, stir 10 ~ 30 minutes, be then mixed into lipid acid, add spaonin powder, essence and white dyes after 12 hours, can non-phosphide detergent be obtained.
The weight part of each material is as follows:
Sodium bicarbonate 3 ~ 8 parts, carboxymethyl cellulose 1 ~ 5 part, Witco 1298 Soft Acid 16 ~ 26 parts, water glass 1 ~ 6 part, Sodium peroxoborate 1 ~ 4 part, 5 ~ 10 parts, lipid acid, spaonin powder 5 ~ 10 parts, 0.1 ~ 2 part, essence, white dyes 0.05 ~ 0.5 part.
Preferred weight part of described each material is:
Sodium bicarbonate 4 ~ 7 parts, carboxymethyl cellulose 2 ~ 4 parts, Witco 1298 Soft Acid 19 ~ 22 parts, water glass 2 ~ 4 parts, Sodium peroxoborate 1 ~ 3 part, 6 ~ 8 parts, lipid acid, spaonin powder 7 ~ 9 parts, 0.5 ~ 1.5 part, essence, white dyes 0.1 ~ 0.3 part.
Optimum weight part of described each material is:
Sodium bicarbonate 5.5 parts, carboxymethyl cellulose 3 parts, Witco 1298 Soft Acid 21.2 parts, water glass 3 parts, Sodium peroxoborate 2.7 parts, 7 parts, lipid acid, spaonin powder 8 parts, 1.2 parts, essence, white dyes 0.25 part.
Beneficial effect of the present invention is:
Raw material sources of the present invention are extensive, technique is simple, production stage is few, production unit is simple, and obtained washing powder is not phosphorous, foam is few, soil removability is strong, are suitable for washing machine and use.
Embodiment
Be further described with specific embodiment below, but the present invention is not limited to these embodiments.
Embodiment 1
The preparation method of non-phosphide detergent, step is as follows:
Sodium bicarbonate and Walocel MT 20.000PV are placed in after mixing tank mixes, add Sodium dodecylbenzene sulfonate, water glass and Sodium peroxoborate again, stir 20 minutes, be then mixed into lipid acid, add spaonin powder, essence and white dyes after 12 hours, can non-phosphide detergent be obtained;
The weight part of each material is as follows: sodium bicarbonate 5.5 parts, carboxymethyl cellulose 3 parts, Witco 1298 Soft Acid 21.2 parts, water glass 3 parts, Sodium peroxoborate 2.7 parts, 7 parts, lipid acid, spaonin powder 8 parts, 1.2 parts, essence, white dyes 0.25 part.
Embodiment 2
The preparation method of non-phosphide detergent, step is as follows:
Sodium bicarbonate and Walocel MT 20.000PV are placed in after mixing tank mixes, add Sodium dodecylbenzene sulfonate, water glass and Sodium peroxoborate again, stir 10 minutes, be then mixed into lipid acid, add spaonin powder, essence and white dyes after 12 hours, can non-phosphide detergent be obtained;
The weight part of each material is as follows: sodium bicarbonate 6 parts, carboxymethyl cellulose 5 parts, Witco 1298 Soft Acid 16 parts, water glass 3 parts, Sodium peroxoborate 4 parts, 5 parts, lipid acid, spaonin powder 8 parts, 2 parts, essence, white dyes 0.05 part.
Embodiment 3
The preparation method of non-phosphide detergent, step is as follows:
Sodium bicarbonate and Walocel MT 20.000PV are placed in after mixing tank mixes, add Sodium dodecylbenzene sulfonate, water glass and Sodium peroxoborate again, stir 20 minutes, be then mixed into lipid acid, add spaonin powder, essence and white dyes after 12 hours, can non-phosphide detergent be obtained;
The weight part of each material is as follows: sodium bicarbonate 8 parts, carboxymethyl cellulose 1 part, Witco 1298 Soft Acid 22 parts, water glass 6 parts, Sodium peroxoborate 1 part, 8 parts, lipid acid, spaonin powder 10 parts, 0.1 part, essence, white dyes 0.15 part.
Embodiment 4
The preparation method of non-phosphide detergent, step is as follows:
Sodium bicarbonate and Walocel MT 20.000PV are placed in after mixing tank mixes, add Sodium dodecylbenzene sulfonate, water glass and Sodium peroxoborate again, stir 30 minutes, be then mixed into lipid acid, add spaonin powder, essence and white dyes after 12 hours, can non-phosphide detergent be obtained;
The weight part of each material is as follows: sodium bicarbonate 3 parts, carboxymethyl cellulose 3 parts, Witco 1298 Soft Acid 26 parts, water glass 1 part, Sodium peroxoborate 3 parts, 10 parts, lipid acid, spaonin powder 5 parts, 0.8 part, essence, white dyes 0.5 part
Result of use
The silk fabrics scribbling ballpoint pen person's handwriting of random selecting 4 pieces of 2cm*2cm, respectively with in embodiment 1 ~ 4 non-phosphide detergent cleaning, cleaning process hand is non-stimulated, red and swollen, and observe after dry, silk fabrics is totally vivid, without ballpoint pen person's handwriting, with fragrant.
Claims (3)
1. the preparation method of non-phosphide detergent, is characterized in that, step is as follows:
Sodium bicarbonate and Walocel MT 20.000PV are placed in after mixing tank mixes, add Sodium dodecylbenzene sulfonate, water glass and Sodium peroxoborate again, stir 10 ~ 30 minutes, be then mixed into lipid acid, add spaonin powder, essence and white dyes after 12 hours, can non-phosphide detergent be obtained;
The weight part of each material is as follows: sodium bicarbonate 3 ~ 8 parts, carboxymethyl cellulose 1 ~ 5 part, Witco 1298 Soft Acid 16 ~ 26 parts, water glass 1 ~ 6 part, Sodium peroxoborate 1 ~ 4 part, 5 ~ 10 parts, lipid acid, spaonin powder 5 ~ 10 parts, 0.1 ~ 2 part, essence, white dyes 0.05 ~ 0.5 part.
2. preparation method according to claim 1, is characterized in that, the weight part of described material is as follows:
Sodium bicarbonate 4 ~ 7 parts, carboxymethyl cellulose 2 ~ 4 parts, Witco 1298 Soft Acid 19 ~ 22 parts, water glass 2 ~ 4 parts, Sodium peroxoborate 1 ~ 3 part, 6 ~ 8 parts, lipid acid, spaonin powder 7 ~ 9 parts, 0.5 ~ 1.5 part, essence, white dyes 0.1 ~ 0.3 part.
3. preparation method according to claim 1, is characterized in that, the weight part of described material is as follows:
Sodium bicarbonate 5.5 parts, carboxymethyl cellulose 3 parts, Witco 1298 Soft Acid 21.2 parts, water glass 3 parts, Sodium peroxoborate 2.7 parts, 7 parts, lipid acid, spaonin powder 8 parts, 1.2 parts, essence, white dyes 0.25 part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510144547.3A CN104726215A (en) | 2015-03-31 | 2015-03-31 | Preparation method of sphorus laundry powder |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510144547.3A CN104726215A (en) | 2015-03-31 | 2015-03-31 | Preparation method of sphorus laundry powder |
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| CN104726215A true CN104726215A (en) | 2015-06-24 |
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| CN201510144547.3A Pending CN104726215A (en) | 2015-03-31 | 2015-03-31 | Preparation method of sphorus laundry powder |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106085608A (en) * | 2015-11-25 | 2016-11-09 | 西北农林科技大学 | A kind of portable wine stain cleanser and preparation method thereof |
| CN108060037A (en) * | 2017-12-25 | 2018-05-22 | 上海和黄白猫有限公司 | Sodium oleate soap compound powder and its manufacturing method |
| CN108531309A (en) * | 2018-05-21 | 2018-09-14 | 李均辉 | A kind of color protection eliminates the unusual smell liquid detergent and its preparation method and application |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102465059A (en) * | 2010-11-15 | 2012-05-23 | 高玉纯 | Cleaning powder |
| CN103122279A (en) * | 2011-11-18 | 2013-05-29 | 大连得达科技发展有限公司 | Non-phosphorus low-foaming washing powder preparation method |
-
2015
- 2015-03-31 CN CN201510144547.3A patent/CN104726215A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102465059A (en) * | 2010-11-15 | 2012-05-23 | 高玉纯 | Cleaning powder |
| CN103122279A (en) * | 2011-11-18 | 2013-05-29 | 大连得达科技发展有限公司 | Non-phosphorus low-foaming washing powder preparation method |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106085608A (en) * | 2015-11-25 | 2016-11-09 | 西北农林科技大学 | A kind of portable wine stain cleanser and preparation method thereof |
| CN108060037A (en) * | 2017-12-25 | 2018-05-22 | 上海和黄白猫有限公司 | Sodium oleate soap compound powder and its manufacturing method |
| CN108060037B (en) * | 2017-12-25 | 2020-09-04 | 上海和黄白猫有限公司 | Soap powder composition of sodium oleate and its preparation method |
| CN108531309A (en) * | 2018-05-21 | 2018-09-14 | 李均辉 | A kind of color protection eliminates the unusual smell liquid detergent and its preparation method and application |
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Application publication date: 20150624 |
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