CN1046886A - Means for leaf feeding of plants and preparation method thereof - Google Patents
Means for leaf feeding of plants and preparation method thereof Download PDFInfo
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- CN1046886A CN1046886A CN90105601A CN90105601A CN1046886A CN 1046886 A CN1046886 A CN 1046886A CN 90105601 A CN90105601 A CN 90105601A CN 90105601 A CN90105601 A CN 90105601A CN 1046886 A CN1046886 A CN 1046886A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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Abstract
Means for leaf feeding of plants, be a kind of mixing liquid fertilizer that contains macroelement and amino-acid trace element complex compound, its preparation method is: compositing acid solution is under the condition that is heated to about 70 ℃, with the trace element dissolving wherein, continue to be warming up to about 85 ℃, and maintain the temperature at 85 ℃ ± 5 ℃, and stir simultaneously, stop after 2-2.5 hour heating up, continue to stir about 1 hour, last naturally cooling makes the amino-acid trace element complex compound, and then this material is mixed with macroelement.
Description
The present invention relates to a kind of liquid plant leaf fertilizer and preparation method thereof.
Known means for leaf feeding of plants only contains macronutrient and micronutrient element usually, and the protein accumulation to plant when its shortcoming is that it is used does not produce direct effect.Chinese patent CN87100319A provides prescription of a kind of means for leaf feeding of plants and preparation method thereof, though wherein contain proteolysate, but because of its proteolysate (being amino acid) just simply mixes (although trace element is also by the lactose coupling in the whey) with trace element, therefore, comparatively speaking, trace element still is a less stable in this mixture, so influence the effective absorption of plant to trace element.
The method for preparing above-mentioned leaf fertilizer is that all the components with leaf fertilizer during heating is dissolved in the dispersion medium of dense whey and proteolysate solution, its shortcoming is that resulting mixture is a kind of suspension of tool microgranular texture after cooling, rather than solution state.Another shortcoming of this method is that the zymotechnique of a whey and the concentration process of lactic acid will be arranged in preparation process, in the component of prepared leaf fertilizer, still contains the deleterious sulfate radical of plant, carbonate and chlorine root etc. simultaneously, therefore, is unfavorable for long-term application.
The object of the present invention is to provide and a kind ofly be convenient to the leaf fertilizer that plant fully absorbs various nutritive ingredients, and the method for preparing this leaf fertilizer.
Utilize the means for leaf feeding of plants of amino-acid trace element complex compound and the composite gained of macroelement just can reach this purpose; The method for preparing above-mentioned means for leaf feeding of plants is at first compositing acid solution to be warming up to about 70 ℃, drop into required trace element subsequently, continue to be warming up to about 85 ℃, and maintain the temperature at 85 ℃ ± 5 ℃, stir simultaneously, stop heating after 2 hours-2.5 hours, continue to stir about 1 hour, last naturally cooling.Can obtain the amino-acid trace element complex compound thus, again that this complex compound and macroelement is composite.The means for leaf feeding of plants that makes like this, its amino acid is highly stable with the complexing degree of trace element, therefore helps the abundant absorption of plant.
Above-mentioned aminoacids complex can utilize discarded albumen to obtain by acid hydrolysis, and inserting of trace element is to be achieved by add the different salt of measuring in compositing acid solution, according to different requirements, select different types of salt for use, as: copper sulfate, ferrous sulfate, sal epsom, rose vitriol, calcium superphosphate, zinc sulfate, lucium, Sodium Tetraborate, silicon-dioxide, Selenium Sulphate, ammonium molybdate.The salt that is added can be a kind of, can also be the cooperation of several salt, to obtain needed amino-acid trace element complex compound.The above-mentioned vitriol of enumerating can also substitute with carbonate.
The advantage of leaf fertilizer provided by the present invention is, various nutritive ingredients are easily by plant absorbing, decomposition and conversion, have necessary amino acid of plant and various nutritive element, help the increase of plant biomass and the improvement of quality, and the fertile no burn into toxicological harmless of this leaf, do not pollute, not teratogenesis, unlikely change, noresidue.
Embodiment explanation with following ingredients:
Example one:
1, macroelement: nitrogen 10%, phosphorus 10%, potassium 5%
2, aminoacids complex: 12%
Comprise in the compositing acid solution:
Amino acid iron complex 0.5%
Amino acid copper complex 0.01%
Amino-acid zinc complex compound 1%
Amino acid molybdenum complex 0.01%
Amino acid cobalt complex 0.01%
Manganese amino acid complex compound 0.01%
Utilize the leaf fertilizer of said components, on wheat, barley and highland barley, paddy rice, vegetables, spray, tangible effect of increasing production is all arranged, further specify the effect of leaf fertilizer of the present invention with tabulating down:
Table 1, wheat yield (field experiment result)
| Different treatment | Jin/mu |
| 3.0 liang+3.0 liang of/mu tri-leaf period+period of seedling establishments of green fragrant prestige | 524 |
| Fertile 3.0 liang+3.0 liang of/mu tri-leaf period+period of seedling establishments of leaf of the present invention | 561 |
Above-mentioned data are the actual output of field experiment, unrepeated test
Table 2: wheat yield (plot experiment result)
| Different treatment | Jin/mu |
| Leaf of the present invention fertile 3 liang of/mu tri-leaf periods | 366.8 |
| Fertile 3 liang of/mu period of seedling establishments of leaf of the present invention | 433.5 |
| Fertile 3 liang of/mu filling stages of leaf of the present invention | 493.5 |
| Fertile 3 liang+3 liang of/mu tri-leaf period+period of seedling establishments of leaf of the present invention | 520.2 |
| Fertile 3 liang+3 liang+3 liang of/mu tri-leaf period+period of seedling establishment+filling stages of leaf of the present invention | 506.9 |
| Contrast | 333.5 |
Above-mentioned six kinds of processing are carried out three times and are repeated, each sub-district area is 0.025 mu of mean value that last output is three revision tests, all is converted into per mu yield, and test with wheat breed is: raise wheat No. five, base manure consumption: 50 jin/mu of ammonium hydrogencarbonates, 20 jin/mu of calcium superphosphate
Table 3: tomato yield (plot experiment result)
| Different treatment | Cell production: jin/16 strains |
| Contrast | 62.7 |
| Mid-term as a result in result early stage before the fertile 500ml+500ml+500ml/ mu of leaf of the present invention is bloomed | 66.5 |
Above-mentioned data are the mean value of three revision tests, and the test kind is: middle vegetables No. 4, base manure consumption: 60 jin/mu of calcium superphosphate, duck excrement 100 load/mus
Example two:
1, macroelement: nitrogen 10%, phosphorus 10%, potassium 5%
2, aminoacids complex: 12%
Comprise in the compositing acid solution:
Amino acid copper complex 5%
Amino-acid zinc complex compound 2%
Amino acid cobalt complex 1%
Amino acid iron complex 2%
Amino acid-magnesium chelate complex compound 0.5%
Utilize the leaf fertilizer of said components, can be used as sterilant and spray in plant, to the canker of fruit tree, three of capsicum (fallen leaves, fallen flowers, the shedding) disease that falls, the Powdery Mildew of wheat all has tangible prevention effect, further specifies the effect of leaf fertilizer of the present invention as sterilant with tabulating down:
Table 4: to the fall prevention effect of disease of capsicum three
| Different treatment | Sickness rate |
| Contrast | 100％ |
| Leaf fertilizer of the present invention | ＜25％ |
Table 5: the prevention effect of wheat powdery mildew
| Different treatment | Prevention effect |
| Tuzet | 41.89% |
| The Tobe bacterium | 18.72% |
| Derosal | 11.75% |
| Leaf fertilizer of the present invention | 76.62% |
Table 6: fruit tree putrefaction disease prevention effect
| Different varieties | Prevention effect |
| Apple apple pear apple too | 97.4% ＞95% ＞95% |
Table 7: rice bakanae disease prevention effect
| Different treatment | Prevention effect |
| 0.1％CuSO 4Invade 24 hours 0.1% leaf fertilizer of the present invention of kind and invaded kind 24 hours | 76.2% 83.3% |
The method for preparing above-mentioned leaf fertilizer is carried out in a kind of container, and technical process comprises following each step:
1, the preparation of amino-acid trace element complex compound;
2, sulfate radical;
3, the composite and precision work the finished product of macroelement and complex compound.
The first step in technological process, after compositing acid solution is contained in the container, be warming up to about 70 ℃, drop into container with trace element this moment, and continue to be warming up to about 85 ℃, and maintain the temperature at 80 ℃-90 ℃, stir simultaneously, after 2 hours-2.5 hours, stop to heat up, continue to stir about 1 hour, last naturally cooling, above-mentioned condition is necessary for the complexing of amino acid and trace element.
Second step in technological process slowly adds lime in the solution in the container, adds strong mixing, measures the pH value of solution in the container at any time, reaches the adding that stopped lime at 7 o'clock, last filter cleaner.This step process can omit, to simplify the preparation technology of leaf fertilizer.Certainly the advantage that increases this processing step is the sulfate radical that can remove in the defoliation fertilizer, helps the long-term application of leaf fertilizer, can not produce plant and poison phenomenon.
In the 3rd step of technological process, the composite of macroelement and above-mentioned solution also carries out in container, preferably earlier macroelement is dissolved in the water, and then composite with the amino-acid trace element complex compound, be beneficial to thorough mixing.
Below by specific embodiment the fertile preparation method of leaf who relates among the present invention is described in further detail:
At first 500 kg of water are put into specified container, 500 kilograms of the vitriol oils of back adding 98% begin to heat up after dilution finishes, and add 500 kilograms of fishes again, and temperature is raised to 110 ℃-120 ℃, start the clock, and agitation as appropriate.Cooling immediately after 8-10 hour, begin to drop into lime when temperature drops to 50 ℃ of left and right sides, lime should bit by bit add gradually, can be hurry up during beginning, when the pH value of solution in the container reaches 4, must be gradually slowly lime be added, in the whole N-process that adds lime, fully stir, and the pH value of test soln at any time, until pH value reaches at 8 o'clock, stop the adding of lime, reduce the temperature to subsequently below 50 ℃ and begin centrifuging.The amino acid solution that centrifuging obtains is contained into retort, be warmed up to 80 ℃, add trace element, the consumption of various trace elements is: respectively 0.648 kilogram of 2.604 kilograms in copper sulfate, 1.95 kilograms of rose vitriols, ferrous sulfate, zinc sulfate, ammonium molybdate, sal epsom, Repone K, borax, manganous sulfate.Add trace element and the time fully stir, and controlled temperature stops to heat after 2 hours 80 ℃-85 ℃ scope, and continued to stir 1-2 hour.Add lime again and neutralize, the pH value of stoste in the assaying reaction jar reaches at 7 o'clock and stops to add lime at any time, cools to subsequently about 50 ℃, and recentrifuge filters, and obtains the amino-acid trace element complex compound.Take by weighing 100 kilograms of monoammonium phosphates at last, be dissolved in earlier in 100 kg of water, this solution is mixed promptly getting means for leaf feeding of plants of the present invention then with 1000 kilograms of amino-acid trace element complex compounds.
Each component content (weight percent) of the finished product of being made by the foregoing description is as follows:
Nitrogen (in N) 〉=1.0%
Effectively Vanadium Pentoxide in FLAKES is (with P
2O
5Meter) 〉=1.0%
Water soluble oxidized potassium is (with K
2The O meter) 〉=0.05%
Manganese (in Mn) 〉=0.0017%
Zinc (in Zn) 〉=0.00045%
Iron (in Fe) 〉=0.0002%
Copper (in Cu) 〉=0.0023%
Boron (in B) 〉=0.0006%
Molybdenum (in Mo) 〉=0.0015%
Magnesium (in Mg) 〉=0.008%
Cobalt (in Co) 〉=0.01%
Calcium (in Ca) 〉=0.008%
Aminoacids complex 〉=10%
Claims (5)
1, means for leaf feeding of plants contains macroelement, it is characterized in that liquid phase is the amino-acid trace element complex compound.
2,, it is characterized in that one or more the cooperation in the following material of consisting of of said amino-acid trace element complex compound according to the means for leaf feeding of plants of claim 1 regulation:
(1) amino acid copper complex;
(2) amino acid iron complex;
(3) amino acid-magnesium chelate complex compound;
(4) amino acid calcium complex compound;
(5) amino-acid zinc complex compound;
(6) amino acid boron complex;
(7) amino acid silicon complex compound;
(8) amino acid seleno-complex;
(9) amino acid molybdenum complex;
(10) amino acid cobalt complex;
(11) amino-acid rare earth element complex.
3, prepare the method for means for leaf feeding of plants, it is characterized in that:
A, in container, contain aminoacids complex, be warming up to subsequently about 70 ℃, again trace element is dropped into container, continue to be warming up to about 85 ℃, and maintain the temperature at 85 ℃ ± 5 ℃, stir simultaneously, stop after 2 hours-2.5 hours heating up, continue to stir about 1 hour, last naturally cooling.
B, with macroelement and the amino-acid trace element complex compound thorough mixing that obtains by a step.
According to the method for preparing means for leaf feeding of plants of claim 3 regulation, it is characterized in that 4, said trace element is one or more the cooperation in the following salt:
A, copper sulfate (or copper carbonate);
B, ferrous sulfate (or iron protocarbonate);
C, sal epsom (or magnesiumcarbonate);
D, calcium superphosphate;
E, zinc sulfate (or zinc carbonate);
F, lucium;
G, Sodium Tetraborate;
H, silicon-dioxide;
I, Selenium Sulphate (or carbonic acid selenium);
J, rose vitriol (or cobaltous carbonate);
R, ammonium molybdate.
5, the means for leaf feeding of plants of stipulating according to claim 2, when the composition (weight %) of its amino-acid trace element complex compound is: amino acid copper complex 1-5%, amino-acid zinc complex compound 1-2%, amino acid cobalt complex 0.5-1%, amino acid iron complex 1-2%, during amino acid-magnesium chelate complex compound 0.5-1%, it is characterized in that spraying in plant leaf surface as sterilant.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN90105601A CN1046886A (en) | 1990-01-09 | 1990-01-09 | Means for leaf feeding of plants and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN90105601A CN1046886A (en) | 1990-01-09 | 1990-01-09 | Means for leaf feeding of plants and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1046886A true CN1046886A (en) | 1990-11-14 |
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ID=4879411
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN90105601A Pending CN1046886A (en) | 1990-01-09 | 1990-01-09 | Means for leaf feeding of plants and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1046886A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5597400A (en) * | 1992-06-19 | 1997-01-28 | Nonomura; Arthur M. | Methods and compositions for enhancing carbon fixation in plants |
| US5846908A (en) * | 1992-06-19 | 1998-12-08 | Nonomura; Arthur M. | Methods and compositions for enhancing plant growth with p-amino- or p-nitro-benzoic acids |
| CN103288496A (en) * | 2013-05-13 | 2013-09-11 | 淮阴师范学院 | Quick-acting amino acid molybdenum fertilizer |
| CN103539499A (en) * | 2013-10-08 | 2014-01-29 | 界首市昊坤农作物种植专业合作社 | Special foliage fertilizer for wheat |
| CN108456032A (en) * | 2017-12-29 | 2018-08-28 | 杨玉岗 | A kind of synthetic method of foliar fertilizer |
| EP3181538B1 (en) * | 2015-12-15 | 2024-04-17 | Fertinagro Biotech, S.L. | Use of a fertiliser composition including copper, iron and manganese ions complexed with amino acids to improve the solubilization of phosphorus by the microorganisms present in the soil |
-
1990
- 1990-01-09 CN CN90105601A patent/CN1046886A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5597400A (en) * | 1992-06-19 | 1997-01-28 | Nonomura; Arthur M. | Methods and compositions for enhancing carbon fixation in plants |
| US5846908A (en) * | 1992-06-19 | 1998-12-08 | Nonomura; Arthur M. | Methods and compositions for enhancing plant growth with p-amino- or p-nitro-benzoic acids |
| US6121195A (en) * | 1992-06-19 | 2000-09-19 | Nonomura; Arthur M. | Methods and compositions for enhancing formyltetrahydropteroylpolyglutamate in plants |
| CN103288496A (en) * | 2013-05-13 | 2013-09-11 | 淮阴师范学院 | Quick-acting amino acid molybdenum fertilizer |
| CN103539499A (en) * | 2013-10-08 | 2014-01-29 | 界首市昊坤农作物种植专业合作社 | Special foliage fertilizer for wheat |
| EP3181538B1 (en) * | 2015-12-15 | 2024-04-17 | Fertinagro Biotech, S.L. | Use of a fertiliser composition including copper, iron and manganese ions complexed with amino acids to improve the solubilization of phosphorus by the microorganisms present in the soil |
| CN108456032A (en) * | 2017-12-29 | 2018-08-28 | 杨玉岗 | A kind of synthetic method of foliar fertilizer |
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