Background technology:
Skin surface antibacterial is indispensable requisites in society life every day.Skin surface antibacterial comprises liquid detergent, handwashing liquid, 84 disinfectant solution, epoxy acetic acid disinfectant solution etc.At present, the effective ingredient of this series products synthesizes master with chemical industry, providing Personal hygiene and kill harmful microorganism simultaneously, can cause serious secondary pollution.Because the harm of this pollution is not obvious at short notice, therefore, often out in the cold.But micropollution continues to enter in body, take care of the pence and can cause serious consequence, cause the various pathological changes of human body.
The Bamboo vinegar collected in the process of bamboo wood pyrolysis bamboo charcoal, liquid is the smoke of bluish yellow color or yellowish-brown, tool uniqueness.Bamboo vinegar, primarily of material compositions such as water, organic acid, phenols, ketone, alcohols, has broad spectrum antibacterial.But because it has highly acid and multiple harmful substances, can not human body surface be directly applied to, limit its application on daily cleaning health field, can only feed lot be used at present, the clean deodorization of house pet.And Bamboo vinegar is obtained the plain composition of bamboo jade-like stone by rectification purification by the present invention, again with Chinese crude drug with pharmaceutic adjuvant is auxiliary joins, the product obtained has broad spectrum antibacterial, zest is little, to humans and animals safety, be applicable to the units such as kindergarten, school, office, hospital for skin and tool face antibacterial, for daily epidemic preventing working provides new means.
Summary of the invention:
It is raw material with Bamboo vinegar that object of the present invention provides a kind of, be aided with Chinese crude drug and the pharmaceutic adjuvants such as Rhizoma Coptidis, Cortex Magnoliae Officinalis, Radix Sophorae Flavescentis, Fructus Cnidii, prepare and have broad spectrum antibacterial, antibacterial ability is strong, zest is little, to lustrous and transparent plain skin surface antibacterial of the bamboo of humans and animals safety and preparation method thereof.
Technical scheme of the present invention is:
The plain skin surface antibacterial of a kind of bamboo jade-like stone, it is characterized in that, this antibacterial comprises following component and parts by weight: the plain 10-15 part of bamboo jade-like stone, Chinese medicinal material extract 5-10 part, aqueous thickener solution 5-10 part, adds to 100 parts by purified water.
The plain skin surface antibacterial of above-described bamboo jade-like stone is made up of following component and parts by weight: bamboo jade-like stone element 12 parts, Chinese medicinal material extract 8 parts, aqueous thickener solution 8 parts, adds to 100 parts by purified water.
A preparation method for the plain skin surface antibacterial of bamboo jade-like stone, comprise the preparation of bamboo jade-like stone element, Chinese medicinal material extract preparation, thickening agent preparation and the plain skin surface anti-infective drugs of bamboo jade-like stone, its technological operation is:
(1) bamboo jade-like stone element preparation: bamboo-vinegar 100 parts is added in reactor, adds calcium carbonate 5-10 part mix homogeneously under stirring, then use alkali adjust ph 5-6, cross leaching supernatant, add active carbon 5-10 part, stir 5-10 minute, filter, obtain bamboo jade-like stone element for subsequent use;
(2) Chinese medicinal material extract preparation: by Chinese crude drug 100 parts, purified water steaming and decocting is added three times according to 5,5,4 times amount, the heating of steaming and decocting is micro-boils, backflow lixiviate, three times extraction time is respectively 1hr, 1hr, 0.5hr, merging filtrate, drops into evacuation rotary evaporation and is concentrated into 200ml, obtain Chinese medicinal material extract for subsequent use by filtrate;
(3) thickening agent preparation: in purified water 100 parts, add thickening agent raw material 5-10 part, hold over night, then be heated to while stirring be greater than 90 DEG C, continues to stir until dissolve completely, obtains thickening agent for subsequent use;
(4) the plain skin surface anti-infective drugs of bamboo jade-like stone: in the plain 10-15 part of bamboo jade-like stone, be heated to 50-60 DEG C while stirring, add Chinese medicinal material extract 5-10 part and aqueous thickener solution 5-10 part, 100 parts are added to by purified water, cooling, packaging, obtains the plain skin surface antibacterial of bamboo jade-like stone.
Its raw material of above-described thickening agent can select in pharmaceutical grade adjuvant carbomer, pharmagel, polyvinylpyrrolidone any one.
Above-described alkali is any one in sodium bicarbonate, sodium hydroxide and potassium hydroxide.
Above-described Chinese crude drug is Rhizoma Coptidis, Cortex Magnoliae Officinalis, Radix Sophorae Flavescentis, Fructus Cnidii each 25 parts or Rhizoma Coptidis, each 50 parts of Cortex Magnoliae Officinalis.
Advantage of the present invention and beneficial effect:
Bamboo vinegar is obtained the plain composition of bamboo jade-like stone by rectification purification by the present invention, again with Rhizoma Coptidis, Cortex Magnoliae Officinalis, Radix Sophorae Flavescentis, Fructus Cnidii Chinese crude drug with pharmaceutic adjuvant is auxiliary joins, the product obtained has broad spectrum antibacterial, antibacterial ability is strong, zest is little, to humans and animals safety bamboo jade-like stone plain skin surface antibacterial, be applicable to the units such as kindergarten, school, office, hospital for skin and tool face antibacterial, for daily epidemic preventing working provides new skin antibacterial surface agent product, there is good economic benefit and social benefit.
Detailed description of the invention:
Content described in embodiment is only basic explanation of the present invention below, and according to the equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.
Embodiment 1:
(1) component and parts by weight:
Bamboo jade-like stone element 15 parts, Chinese medicinal material extract 10 parts, aqueous thickener solution 10 parts, purified water 65 parts.
(2) the plain skin surface Antibacterial agent preparation method of bamboo jade-like stone:
Add in blender by bamboo jade-like stone element 15 parts, be heated to 50 DEG C while stirring, add Chinese medicinal material extract 10 parts and aqueous thickener solution 10 parts, purified water 65 parts, stirs, cooling, packaging, obtains the plain skin surface antibacterial of bamboo jade-like stone.
Embodiment 2:
(1) component and parts by weight:
Bamboo jade-like stone element 10 parts, Chinese medicinal material extract 5 parts, aqueous thickener solution 5 parts, purified water adds to 80 parts.
(2) the plain skin surface Antibacterial agent preparation method of bamboo jade-like stone:
Add in blender by bamboo jade-like stone element 10 parts, be heated to 55 DEG C while stirring, add Chinese medicinal material extract 5 parts and aqueous thickener solution 5 parts, purified water 80 parts, stirs, cooling, packaging, obtains the plain skin surface antibacterial of bamboo jade-like stone.
Embodiment 3:
(1) component and parts by weight:
Bamboo jade-like stone element 12 parts, Chinese medicinal material extract 8 parts, aqueous thickener solution 7 parts, purified water adds to 73 parts
(2) the plain skin surface Antibacterial agent preparation method of bamboo jade-like stone:
Add in blender by bamboo jade-like stone element 12 parts, be heated to 60 DEG C while stirring, add Chinese medicinal material extract 8 parts and aqueous thickener solution 7 parts, purified water 73 parts, stirs, cooling, packaging, obtains the plain skin surface antibacterial of bamboo jade-like stone.
Embodiment 4:
The preparation of bamboo jade-like stone element: add in reactor by bamboo-vinegar 100 parts, add calcium carbonate 5 parts of mix homogeneously, then use sodium bicarbonate adjust ph 5 under stirring, precipitation, cross leaching supernatant, add active carbon 5 parts, stir 10 minutes, filter, obtains bamboo jade-like stone element for subsequent use.
Embodiment 5:
The preparation of bamboo jade-like stone element: add in reactor by bamboo-vinegar 100 parts, add calcium carbonate 10 parts of mix homogeneously, then use sodium hydroxide adjust ph 6 under stirring, cross leaching supernatant, add active carbon 10 parts, stir 5 minutes, filter, obtains bamboo jade-like stone element for subsequent use.
Embodiment 6:
The preparation of Chinese medicinal material extract: Rhizoma Coptidis, Cortex Magnoliae Officinalis, Radix Sophorae Flavescentis, each 25 parts of Fructus Cnidii are added in reactor, purified water decocting in water is added three times according to 5,5,4 times amount, the heating of decocting in water is micro-boils, backflow lixiviate, the time of lixiviate is respectively 1hr, 1hr, 0.5hr, merges three filtrates, filtrate is added evacuation rotary evaporator, be concentrated into 200ml, obtain Chinese medicinal material extract for subsequent use.
Embodiment 7:
The preparation of Chinese medicinal material extract: Rhizoma Coptidis, each 50 parts of Cortex Magnoliae Officinalis are added in digester, purified water decocting in water is added three times according to 5,4,4 times amount, the heating of decocting in water is micro-boils, backflow lixiviate, the time of decocting in water is respectively 1hr, 1hr, 0.5hr, merges three filtrates, filtrate is added evacuation rotary evaporator, be concentrated into 200ml, obtain Chinese medicinal material extract for subsequent use.
Embodiment 8:
The preparation of aqueous thickener solution: add in digester purified water 100 parts, adds thickening agent raw material carbomer 5 parts, hold over night, then is heated to 90 DEG C while stirring, continues to stir until dissolve completely, obtains thickening agent for subsequent use.
Embodiment 9:
The preparation of aqueous thickener solution: add in digester purified water 100 parts, adds 10 parts, thickening agent raw material gelatin, hold over night, then is heated to 95 DEG C while stirring, continues to stir until dissolve completely, obtains thickening agent for subsequent use.
The mensuration of the plain antibacterial ability of bamboo jade-like stone:
Product of the present invention detects through the general notary of Disease Control and Prevention Center of Guilin City and Hong Kong, and testing result is in table 1 and table 2.
Table 1: Disease Control and Prevention Center of Guilin City testing result table
Table 2: Hong Kong SGS measurement result table
The antibacterial mensuration of table 2, with reference to American Pharmacopeia, international quality controls, US Patent No. P, 25,2002,51 chapters; Measurement result shows: bamboo jade-like stone element to above-mentionedly representing antibacterial, fungus has reliable killing action.