CN104629434A - Formula for preparing blue-green wheat straw dye and production method thereof - Google Patents

Formula for preparing blue-green wheat straw dye and production method thereof Download PDF

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Publication number
CN104629434A
CN104629434A CN201310550610.4A CN201310550610A CN104629434A CN 104629434 A CN104629434 A CN 104629434A CN 201310550610 A CN201310550610 A CN 201310550610A CN 104629434 A CN104629434 A CN 104629434A
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CN
China
Prior art keywords
wheat straw
solution
blue
raw material
dye
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201310550610.4A
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Chinese (zh)
Inventor
马文侠
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Harbin Arts and Crafts Co Ltd
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Harbin Arts and Crafts Co Ltd
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Filing date
Publication date
Application filed by Harbin Arts and Crafts Co Ltd filed Critical Harbin Arts and Crafts Co Ltd
Priority to CN201310550610.4A priority Critical patent/CN104629434A/en
Publication of CN104629434A publication Critical patent/CN104629434A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/02Staining or dyeing wood; Bleaching wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • B27K9/007Straw
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Coloring (AREA)

Abstract

The invention discloses a formula for preparing blue-green wheat straw dye and a production method thereof. The dye is mainly composed of blue grass, an antimony ion solution, nettle, alum, an iron ion compound solution, and mineral water. The main procedure of dyed wheat straw production comprises the following steps: material choosing, material cutting, drying, soaking, boiling, mixing, precipitating, dyeing, and finishing. The dye is prepared from pure natural plants, is natural, pollution-free, green, and environment-friendly, and does not have any side or toxic effect to human body.

Description

A kind of formula and production method preparing blue-greenish colour wheat straw dye
technical field:
the present invention relates to a kind of vegetable dye, particularly relates to a kind of formula and the production method of preparing blue-greenish colour wheat straw dye
background technology:
in prior art, the main raw material Wheat Straw making straw patchwork is dyed glaucous method to be had a variety of, but most dyestuff is chemical dye, the blue-greenish colour dyed is impure, easily fade, not only not environmentally, some dyes even can produce toxic gas in the process of dye system, threatens the health of human body.
thus, make field at straw patchwork and lack a kind of vegetable dye Wheat Straw being dyed different colours, particularly Wheat Straw is dyed glaucous natural plant dyestuff, not only color is pure for the blue-greenish colour Wheat Straw that it dyes, and the straw patchwork made with its material is bright and new beautiful, not easily fades, and environmental protection, works give out plant fragrance for a long time, have the physical and mental health of easy people, and what degree was different solves other poisonous and harmful chemical dye in dye process processed to the prestige evil that people's health causes.
summary of the invention:
the object of the present invention is to provide a kind of pure natural, pollution-free, environmental protection, a kind of formula and the production method preparing blue-greenish colour wheat straw dye be mixed with natural plant that the person is had no side effect.
the object of the present invention is achieved like this.It is that the raw material of being joined by following weight is made, bluegrass 10-30 part, antimony ion solution 10-30 part, nettle 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
the formula optimization weight proportion scope preparing blue-greenish colour wheat straw dye of the present invention is, wherein the weight proportion of various raw material is bluegrass 10-25 part, antimony ion solution 10-25 part, nettle 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
the optimum weight ratio range preparing blue-greenish colour wheat straw dye of the present invention is that wherein the weight proportion of various raw material is: bluegrass 15 parts, antimony ion solution 8 parts, nettle 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of blue-greenish colour wheat straw dye of the present invention, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the bluegrass, antimony ion solution, nettle, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, the raw material bluegrass selected, nettle are cut into bulk; C, oven dry, the bluegrass of the shape that is cut into small pieces, nettle raw material are placed in stoving oven mummification, temperature controls at 100-120 DEG C, 30 minutes time, makes raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, add antimony ion solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure blue-greenish colour cellulose solution; H, dyeing, the temperature of 100 liters of pure blue-greenish colour cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb blue-greenish colour cellulose solution, level dyeing; I, finished product, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to blue-greenish colour Wheat Straw finished product at room temperature.
production method advantage of the present invention is: 1, select raw material, scientific formulation, color is pure; 2, do not add sanitas in product, industrial chemicals, pure natural, to human body without any injury, the straw patchwork works made with its raw material not only distribute Scent, and anticorrosive; 3 raw material sources are extensive, add process line short, the easy processing and manufacturing of product.
Embodiment
below in conjunction with specific embodiment, the present invention is further illustrated:
embodiment 1:
the formulation weight ratio range preparing blue-greenish colour wheat straw dye of the present invention is: bluegrass 10-30 part, antimony ion solution 10-30 part, nettle 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
embodiment 2:
the formula optimization weight proportion scope preparing blue-greenish colour wheat straw dye of the present invention is: bluegrass 10-25 part, antimony ion solution 10-25 part, nettle 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
embodiment 3:
the formula optimum weight ratio range preparing blue-greenish colour wheat straw dye of the present invention is: wherein the weight proportion of various raw material is, bluegrass 15 parts, antimony ion solution 15 parts, nettle 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
above-mentioned each component is made the production method of blue-greenish colour wheat straw dye of the present invention, technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the bluegrass, antimony ion solution, nettle, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, the raw material bluegrass selected, nettle are cut into bulk; C, oven dry, the bluegrass of the shape that is cut into small pieces, nettle raw material are placed in stoving oven mummification, temperature controls at 100-120 DEG C, 30 minutes time, makes raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, add antimony ion solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure blue-greenish colour cellulose solution; H, dyeing, the temperature of 100 liters of pure blue-greenish colour cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb blue-greenish colour cellulose solution, level dyeing; I, finished product, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to blue-greenish colour Wheat Straw finished product at room temperature.

Claims (4)

1. prepare the formula of blue-greenish colour wheat straw dye for one kind, it is characterized in that: it is made up of the raw material of following weight proportioning, bluegrass 10-30 part, antimony ion solion solution 10-30 part, nettle 10-30 part, alum 5-15 part, ferric ion compounds solution 5-15 part, mineral water 30-80 part.
2. prepare the formula of blue-greenish colour wheat straw dye for one kind, it is characterized in that: wherein the weight proportion of various raw material is, bluegrass 10-25 part, antimony ion solution 10-25 part, nettle 10-25 part, alum 5-10 part, ferric ion compounds solution 5-10 part, mineral water 30-70 part.
3. prepare a formula for blue-greenish colour wheat straw dye, it is characterized in that: wherein the weight proportion of various raw material is, bluegrass 15 parts, antimony ion solution 15 parts, nettle 15 parts, alum 8 parts, ferric ion compounds solution 8 parts, mineral water 65 parts.
4. a kind of production method preparing blue-greenish colour wheat straw dye formula according to claim 1-3, it is characterized in that: technical process is: select materials, blank, oven dry, immersion, heat are boiled, mix, precipitate, dye, finished product, concrete operation method follows these steps to successively: A, select materials, by raw material weight proportioning, select the bluegrass, antimony ion solution, nettle, alum, ferric ion compounds solution, the mineral water that meet national health and quality standard for subsequent use; B, blank, the raw material bluegrass selected, nettle are cut into bulk; C, oven dry, the bluegrass of the shape that is cut into small pieces, nettle raw material are placed in stoving oven mummification, temperature controls at 100-120 DEG C, 30 minutes time, makes raw materials evaporate moisture content, sterilizing; D, immersion, the raw material after drying is placed in the storage tank that mineral water is housed and soaks, temperature is 20 DEG C, room, time 2-4 hour; E, heat are boiled, pulled out from water by the raw material steeped, and are put into pottery interior heat and boil, 6 hours time, cook pigment solution; F, mixing, invaded in 20% ferric ion compounds solution by pigment solution, add antimony ion solution, time 4-8 hour, makes mixing solutions; G, precipitation, by cool for mixing solutions to 20 DEG C, be settled out pure blue-greenish colour cellulose solution; H, dyeing, the temperature of 100 liters of pure blue-greenish colour cellulose solutions is raised to more than 80 DEG C gradually, soaked wherein by Wheat Straw after sterilization, desulfurization, boiling process, constant temperature leaves standstill 12-14 hour, and Wheat Straw stirs by period up and down, Wheat Straw is made fully to absorb blue-greenish colour cellulose solution, level dyeing; I, finished product, the Wheat Straw after dyeing is put into the solution adding alum powder, soak 3-6 hour, pull out after making the abundant fixation of Wheat Straw, drench dry, be slowly dried to blue-greenish colour Wheat Straw finished product at room temperature.
CN201310550610.4A 2013-11-08 2013-11-08 Formula for preparing blue-green wheat straw dye and production method thereof Pending CN104629434A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310550610.4A CN104629434A (en) 2013-11-08 2013-11-08 Formula for preparing blue-green wheat straw dye and production method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310550610.4A CN104629434A (en) 2013-11-08 2013-11-08 Formula for preparing blue-green wheat straw dye and production method thereof

Publications (1)

Publication Number Publication Date
CN104629434A true CN104629434A (en) 2015-05-20

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Application Number Title Priority Date Filing Date
CN201310550610.4A Pending CN104629434A (en) 2013-11-08 2013-11-08 Formula for preparing blue-green wheat straw dye and production method thereof

Country Status (1)

Country Link
CN (1) CN104629434A (en)

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Application publication date: 20150520

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