CN104622755B - Natural volatile oil microcapsule talcum powder and preparation method thereof - Google Patents
Natural volatile oil microcapsule talcum powder and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of natural volatile oil microcapsule talcum powder and preparation method thereof, the talcum powder is counted composed of the following components by weight：70 85 parts of cornstarch, 4 10 parts of superfine silica gel powder, 48 parts of magnesium stearate, 15 parts of ascorbic acid, 2 10 parts of volatile honeysuckle oil microcapsules, 2 10 parts of Forsythia volatile oil microcapsules, 3 10 parts of Herba Houttuyniae volatile oil microcapsules, 48 parts of Radix Saposhnikoviae volatile oil microcapsules, 38 parts of Cortex Cinnamomi volatile oil microcapsules, 4 10 parts of volatile argyi leaf oil microcapsules, 38 parts of Radix Astragali volatile oil microcapsule.Because of the addition of a variety of essential oil microcapsules, make talcum powder of the present invention that not only there is health-care efficacy, also play a part for the treatment of to a certain extent, be especially suitable for the use of some special populations, such as old group or arthritic.
Description
Technical field
The present invention relates to a kind of talcum powder, more particularly to a kind of natural volatile oil microcapsule talcum powder and preparation method thereof.
Background technology
Talcum powder is the amenities commonly used in summer and daily life, after summer takes a shower or after haircut, is flutterred with being dispersed in
Or on head, can not only lubricate the skin and muscle, sweat is absorbed, more there is the pleasant heart spleen of aromatic odor, enjoys comfortable refrigerant in hot summer
Sensation.
Talcum powder species at present on the market is various, and its composition, ratio are roughly the same, and majority is in lubrication, mobility, prevented
Improvement is made in terms of rotten and odor type, but still is come with some shortcomings, such as most talcum powder is using talcum powder as main
Absorbing sweat composition, but contain lead in talcum powder, the harm to body is very big；Also some talcum powders are increased using magnesium sulfate
Frictional force, so that talcum powder is well attached in skin surface, if but magnesium sulfate powder enters respiratory tract accidentally, a variety of exhale can be induced
Inhale tract disease.Importantly, existing talcum powder component and effect on the market is limited, some can not be especially better adapted to special
The demand of crowd, such as elderly population.
The content of the invention
In view of this, it is an object of the invention to provide a kind of natural volatile oil microcapsule talcum powder, the talcum powder due to
Traditional Chinese medicine ingredients are with the addition of, make talcum powder that not only there is the effect of common talcum powder, also with certain health care and therapeutic action, especially
It is adapted to the use of some special populations；Present invention also offers the preparation method of talcum powder.
The technical scheme that the present invention takes is as follows：
1st, natural volatile oil microcapsule talcum powder, is counted composed of the following components by weight：70-85 parts of cornstarch,
4-10 parts of superfine silica gel powder, 4-8 parts of magnesium stearate, 1-5 parts of ascorbic acid, 2-10 parts of volatile honeysuckle oil microcapsules, capsule of weeping forsythia volatilization
2-10 parts of oil microcapsule, 3-10 parts of Herba Houttuyniae volatile oil microcapsules, 4-8 parts of Radix Saposhnikoviae volatile oil microcapsules, the micro- glue of Cortex Cinnamomi volatile oil
3-8 parts of capsule, 4-10 parts of volatile argyi leaf oil microcapsules, 3-8 parts of Radix Astragali volatile oil microcapsule.
It is preferred that, count by weight composed of the following components：70 parts of cornstarch, 4 parts of superfine silica gel powder, magnesium stearate 4
Part, 1 part of ascorbic acid, 2 parts of volatile honeysuckle oil microcapsules, 2 parts of Forsythia volatile oil microcapsules, Herba Houttuyniae volatile oil microcapsules 3
Part, 4 parts of Radix Saposhnikoviae volatile oil microcapsules, 3 parts of Cortex Cinnamomi volatile oil microcapsules, 4 parts of volatile argyi leaf oil microcapsules, the micro- glue of Radix Astragali volatile oil
3 parts of capsule.
It is preferred that, count by weight composed of the following components：80 parts of cornstarch, 7 parts of superfine silica gel powder, magnesium stearate 6
Part, 3 parts of ascorbic acid, 6 parts of volatile honeysuckle oil microcapsules, 6 parts of Forsythia volatile oil microcapsules, Herba Houttuyniae volatile oil microcapsules 7
Part, 6 parts of Radix Saposhnikoviae volatile oil microcapsules, 5 parts of Cortex Cinnamomi volatile oil microcapsules, 6 parts of volatile argyi leaf oil microcapsules, the micro- glue of Radix Astragali volatile oil
5 parts of capsule.
It is preferred that, count by weight composed of the following components：85 parts of cornstarch, 10 parts of superfine silica gel powder, magnesium stearate 8
Part, 5 parts of ascorbic acid, 10 parts of volatile honeysuckle oil microcapsules, 10 parts of Forsythia volatile oil microcapsules, Herba Houttuyniae volatile oil microcapsules
10 parts, 8 parts of Radix Saposhnikoviae volatile oil microcapsules, 8 parts of Cortex Cinnamomi volatile oil microcapsules, 10 parts of volatile argyi leaf oil microcapsules, Radix Astragali volatile oil
8 parts of microcapsules.
2nd, the preparation method of natural volatile oil microcapsule talcum powder, comprises the following steps：
A. the preparation of the volatile oil microcapsule containing component A：It is 7~8 by cyclodextrin and the mass volume ratio of component A：1 ratio
Example weighs cyclodextrin and component A；Component A ethanol is dissolved, the ethanol solution of component A is obtained, cyclodextrin is configured to saturation with water
Solution；The ethanol solution of component A is added dropwise into cyclodextrin saturated solution, component A-cyclodextrin mixed solution is made；It will mix molten
60~70 DEG C of 2~3h of water-bath of liquid, then 24h is placed under the conditions of 5~10 DEG C, then stir and filter, obtain trapped substance；It will cut
Stay thing to be dried under conditions of not higher than 30 DEG C, produce the volatile oil microcapsule containing component A；
The component A is cinnamon essential oil or windproof essential oil；
B. the preparation of the volatile oil microcapsule containing B component：It is 10~12 by cyclodextrin and the mass volume ratio of B component:1
Ratio weighs cyclodextrin and B component；Mixed after B component ethanol is dissolved with cyclodextrin, obtain mixture；Mixture is ground
Mill, adds water in grinding, untill B component smell disappears and cyclodextrin surface no longer membranoid substance occurs；Filter mixture
After obtain trapped substance, by trapped substance under conditions of not higher than 30 DEG C dry, produce the volatile oil microcapsule containing B component；
The B component is cordate houttuynia essential oil, honeysuckle essential oil, Radix Astragali essential oil, Forsythia suspense essential oil or P-Cymene；
C. by Radix Saposhnikoviae volatile oil microcapsules, Cortex Cinnamomi volatile oil microcapsules, volatile honeysuckle oil made from step a and step b
Microcapsules, Forsythia volatile oil microcapsules, Herba Houttuyniae volatile oil microcapsules, volatile argyi leaf oil microcapsules and the micro- glue of Radix Astragali volatile oil
Capsule, and cornstarch, superfine silica gel powder, magnesium stearate and ascorbic acid are ground, 80~100 mesh sieves are crossed, by proportioning respectively
Talcum powder is produced after amount mixing.
It is preferred that, the preparation process of cyclodextrin saturated solution is as follows described in the step a：It is 1 by mass volume ratio:10
Ratio cyclodextrin is dissolved in after water, be placed in 60 DEG C of water-baths and heat while stirring, treat that cyclodextrin is completely dissolved and produce.
It is preferred that, component A-cyclodextrin mixed solution described in the step a is in 60 DEG C of water-bath 2h, then under the conditions of 5 DEG C
Place 24h.
It is preferred that, 100 mesh sieves are crossed after talcum powder each component is ground respectively in the step c.
Microcapsules are a kind of new drug carriers, and microcapsules technology is used as capsule by the use of natural or synthesis high polymer material
Material prepares cyst membrane, then wraps up medicine, and Microcapsules Size belongs to micron order between 1-250 μm, and feature is as follows：
1) bad smell, such as Herba Houttuyniae volatile oil are covered；
2) improving the stability of volatile oil slows down its evaporation rate, is easy to apply and storage；
3) there is sustained and controlled release, rate of release and the release position of volatile oil is controlled；
4) using cyclodextrin as capsule material, because cyclodextrin has hygroscopicity in itself, effect can be strengthened by coordinating with cornstarch；
5) volatile oil is become into dry powder, is easy to use by different proportion compatibility.
The beneficial effects of the present invention are：Talcum powder is replaced with cornstarch, cornstarch not only has stronger hygroscopicity,
Also contain lysine, it is safe and harmless with the effect for suppressing tumour growth；Magnesium sulfate is replaced with superfine silica gel powder, due to micro mist silicon
Glue relative surface area is big, not only with lubrication, it is anti-stick, help stream to act on, also have stronger hygroscopicity and anti-skidding effect；Add each
Kind of natural essential oil microcapsules, on the one hand make talcum powder be suitable to special population, especially elderly population, on the other hand, due to by essence
Oil makes the form of microcapsules, the effect with protection and controlled release so that the effect of talcum powder and aromatic odor are more lasting；Together
When, because of the addition of a variety of essential oil microcapsules, make talcum powder that not only there is health-care efficacy, the work for the treatment of is also played to a certain extent
With such as, adding after Radix Astragali volatile oil microcapsule, there is detumescence to treat the effect of sore, and suitable prolonged illness, which does not rise, is easy to the old group for giving birth to sore
Body；Cortex Cinnamomi volatile oil microcapsules are added, in addition to corrosion-resistant effect, the also effect of anti-inflammatory is adapted to arthritic；Separately
Outside, corrosion-resistant purpose is can reach using the natural volatile oil such as cloves, dried orange peel, and applies ascorbic acid anti-oxidant, then make product
Safer health；Furthermore, essence is substituted with the natural flavor of traditional medicine volatile oil such as volatile honeysuckle oil, traditional talcum powder is changed
Choke the fragrance of nose middle part, it is easier to allow people to receive.
Embodiment
The preferred embodiments of the present invention are described in detail below.The experiment side of unreceipted actual conditions in embodiment
Method, generally according to normal condition or according to the condition proposed by manufacturer.
Embodiment 1
Natural volatile oil microcapsule talcum powder, is counted composed of the following components by weight：70 parts of cornstarch, micro mist silicon
4 parts of glue, 4 parts of magnesium stearate, 1 part of ascorbic acid, 2 parts of volatile honeysuckle oil microcapsules, 2 parts of Forsythia volatile oil microcapsules, fish raw meat
Careless 3 parts of volatile oil microcapsule, 4 parts of Radix Saposhnikoviae volatile oil microcapsules, 3 parts of Cortex Cinnamomi volatile oil microcapsules, volatile argyi leaf oil microcapsules 4
Part, 3 parts of Radix Astragali volatile oil microcapsule.
The effect of various composition is as follows in above-mentioned formula：Cornstarch --- dilution, absorbing sweat, moisture absorption；Superfine silica gel powder --- help
Stream, lubrication, water suction；Magnesium stearate --- lubricate, help stream, anti-freezing；Ascorbic acid --- it is anti-oxidant；The micro- glue of volatile honeysuckle oil
It is capsule --- antibacterial, anti-inflammatory, antipyretic；Forsythia volatile oil microcapsules --- clearing heat and detoxicating, dispersing swelling and dissipating binds；The micro- glue of Herba Houttuyniae volatile oil
Capsule --- sore is treated in clearing heat and detoxicating, detumescence；Radix Saposhnikoviae volatile oil microcapsules --- expel pathogenic wind from the body surface；Cortex Cinnamomi volatile oil microcapsules --- anti-corrosion, control
Treat arthritis；Volatile argyi leaf oil microcapsules --- mosquito repellent, antibacterial；Radix Astragali volatile oil microcapsule --- inducing diuresis for removing edema, treatment sore.
This is formulated health care and the therapeutic efficiency that talcum powder is realized by adding various microcapsules.The 7 kinds of natural essential oils added
Mutual compatibility can play more preferable effect, wherein Forsythia volatile oil microcapsules, Herba Houttuyniae volatile oil microcapsules, Radix Astragali volatile oil
All there is microcapsules detumescence to treat sore effect, relatively be adapted to the elderly, therefore consumption is relatively more；Volatile honeysuckle oil microcapsules and
It is that people are general that volatile argyi leaf oil microcapsules, which play the role of the natural Chinese medicinal herbs such as antibacterial, anti-inflammatory, and cordate houttuynia and honeysuckle,
All over well known good medicine, it is easier to received by user.
The preparation method of above-mentioned natural volatile oil microcapsule talcum powder is as follows：
Natural volatile oil microcapsule is prepared first, and the preparation of microcapsules there are two methods：Saturated water solution method and polishing.
The present embodiment prepares Chinese cassia tree and windproof microcapsules with saturated water solution method, and cordate houttuynia, honeysuckle, the Radix Astragali, company are prepared with polishing
Stick up and folium artemisiae argyi microcapsules.
The concrete technology flow process of saturated water solution method and polishing is described respectively by taking Chinese cassia tree and cordate houttuynia as an example below：
(1) saturated water solution method prepares Cortex Cinnamomi volatile oil microcapsules：
Cinnamon essential oil 2mL is measured with 2mL pipette to be placed in clean small beaker, then is 1 by volume:20 ratio
40mL absolute ethyl alcohols are added into beaker, and (purpose for adding ethanol is to dissolve essential oil, is easy to essential oil to enter in β-CD structures, reaches
To higher embedding rate), it is closed after essential oil is completely dissolved to prevent essential oil from volatilizing；
Mass volume ratio according to cyclodextrin (β-CD) and essential oil is 8：1 ratio precise 16g cyclodextrin (β-CD),
Then it is 1 according to mass volume ratio:10 ratio measures 160mL deionized waters in 200 or 250mL conical flask, by 16g's
β-CD are slowly added into conical flask, are jiggled, and are allowed to be uniformly distributed, then conical flask is placed in the water-bath of 60 DEG C of constant temperature plus
Heat, heats while stirring and (heats magnetic stirring apparatus with instant-heating-type constant-temperature herein)；
After β-CD turn into saturated solution after, the essential oil and alcohol mixeding liquid prepared is slowly added dropwise, after the completion of constant temperature 60~
70 DEG C of 2~3h of water-bath, then conical flask be cooled to be placed in after room temperature in 5~10 DEG C of refrigerator refrigerate 24h；Cone is taken out after 24h
Shape bottle, rocks to precipitation and is uniformly distributed, and forms suspension；Suction filtration device is opened, suspension is inclined in suction funnel, with a small amount of
After the completion of the repeated multiple times cleaning conical flask of distilled water, first time suction filtration, plus distilled water cleans suction funnel suction filtration again, repeatedly 2-
3 times, the ethanol of dilution is added in suction funnel for the last time；After suction filtration terminates, the trapped substance in funnel is taken out in evaporating dish
In, it is positioned over temperature and is not higher than in 30 DEG C of environment or so dry 12 hours, you can the cinnamon essential oil microcapsule that must be dried.
(2) polishing makes Herba Houttuyniae volatile oil microcapsules：
Cordate houttuynia essential oil 2mL is measured with 2mL pipette in clean small beaker, 8mL 95% ethanol is then measured
Dissolving is sufficiently mixed with essential oil；According to β-CD：The mass volume ratio of essential oil is 12：1 ratio precise 24g β-CD are transferred to
In mortar, essential oil-ethanol solution after dissolving is inclined in mortar, with the repeated multiple times cleaning small beaker of a small amount of distilled water, and will
Washing lotion is fallen in mortar, is fully ground；While grinding while adds a small amount of distilled water, up to essential oil smell die down and β-CD surfaces no longer
Stop grinding when having membranoid substance (this process about needs 2-3h)；Mixture in mortar is placed in large beaker, about 50mL is added
Distilled water, it is therefore an objective to make microcapsules fully dispersed, is easy to during filtering and washing below a small amount of volatile oil and ethanol wherein remained
Rinse out, stir；Suction filtration device is opened, suspension is inclined in suction funnel, with the repeated multiple times cleaning of a small amount of distilled water
After the completion of conical flask, first time suction filtration, plus distilled water cleans suction funnel suction filtration again, 2-3 times repeatedly, for the last time will dilution
Ethanol add suction funnel in；After suction filtration terminates, the trapped substance in funnel is taken out in evaporating dish, temperature is positioned over and is not higher than
Or so 15 hours are dried in 30 DEG C of environment, you can the cordate houttuynia essential oil microcapsules that must be dried.
The preparation technology of remaining essential oil microcapsules is identical with both the above method, simply ratio, the essence in essential oil and β-CD
Taken amount, the ethanol consumption that uses of dissolving essential oil of oil, and in water-bath and milling time it is otherwise varied, it is specific as shown in table 1.
The preparation condition of the other essential oils of table 1
| Essential oil | Essential oil：β-CD | Essential oil consumption | Ethanol consumption | Water-bath or milling time |
| It is windproof | 1mL：7g | 2mL | 3.2mL absolute ethyl alcohol | Water-bath 120min |
| Honeysuckle | 1mL：10g | 4mL | 21.5mL absolute ethyl alcohols | Grind 180min |
| The capsule of weeping forsythia | 1mL：10g | 2mL | 7mL95% ethanol | Grind 130min |
| Folium artemisiae argyi | 1mL：12g | 3mL | 6.8mL acetone (does not dissolve in ethanol) | Grind 200min |
| The Radix Astragali | 1mL：11g | 3mL | 2.8mL absolute ethyl alcohol | Grind 170min |
After microcapsules preparation is finished, then talcum powder is prepared, method is as follows：
(1) grind：It is into bulk after being dried due to the microcapsules that ground method makes, need to will be dried all kinds of
Microcapsules are placed in mortar and ground, generally grinding 30min or so；Milling time is short if dispersion effect is preferable, should not during grinding
Too exert oneself, in order to avoid the structure of destruction microcapsules；Other superfine silica gel powder, cornstarch, VC, magnesium stearate grinding 20min are left
The right side, is sub-packed in hermetically drying in small poly-bag by ground each composition and preserves；
(2) sieve：During the slow a small amount of double-deck medicine for inclining to 80~100 mesh of ground microcapsules is sieved, in order to avoid block
Sieve aperture；Microcapsules after sieving are sub-packed in into hermetically drying in small poly-bag to preserve, meanwhile, cornstarch and superfine silica gel powder are carried out
Sieving is handled, and method is identical with essential oil microcapsules；
(3) weigh：The various composition sieved is weighed according to proportion speed stand-by；
(4) mix：By weigh up it is each into being placed in medicine sieve, mortar is placed below in medicine sieve, make after each component sieved by medicine
Fall in mortar, collect mixed-powder in mortar and produce talcum powder.
Embodiment 2
Natural volatile oil microcapsule talcum powder, is counted composed of the following components by weight：80 parts of cornstarch, micro mist silicon
7 parts of glue, 6 parts of magnesium stearate, 3 parts of ascorbic acid, 6 parts of volatile honeysuckle oil microcapsules, 6 parts of Forsythia volatile oil microcapsules, fish raw meat
Careless 7 parts of volatile oil microcapsule, 6 parts of Radix Saposhnikoviae volatile oil microcapsules, 5 parts of Cortex Cinnamomi volatile oil microcapsules, volatile argyi leaf oil microcapsules 6
Part, 5 parts of Radix Astragali volatile oil microcapsule.
The preparation method be the same as Example 1 of above-mentioned talcum powder.
Embodiment 3
Natural volatile oil microcapsule talcum powder, is counted composed of the following components by weight：85 parts of cornstarch, micro mist silicon
10 parts of glue, 8 parts of magnesium stearate, 5 parts of ascorbic acid, 10 parts of volatile honeysuckle oil microcapsules, 10 parts of Forsythia volatile oil microcapsules, fish
Raw meat 10 parts of volatile oil microcapsule of grass, 8 parts of Radix Saposhnikoviae volatile oil microcapsules, 8 parts of Cortex Cinnamomi volatile oil microcapsules, volatile argyi leaf oil microcapsules
10 parts, 8 parts of Radix Astragali volatile oil microcapsule.
The preparation method be the same as Example 1 of above-mentioned talcum powder.
Embodiment 4
Natural each quality index of volatile oil microcapsule talcum powder prepared by embodiment 1-3 is as follows：
(1) sanitary standard
The method as specified in health legislation prison sends out [2002] No. 229 examines qualified.
(2) sense index
Color and luster
Materials and be placed in white backing, visual observations are generally white micro- partially yellow under room temperature and non-direct sunlight.
Fragrance
Materials and differentiated with smell, do not add any essence in this formula, fragrance, which is entirely derived from, each naturally to be waved
Hair oil, mainly Radix Astragali volatile oil.
Powder
Materials and in white backing, visual observations are in attritive powder under room temperature and non-direct sunlight.
(3) physical and chemical index
Fineness
Powder about 5g is weighed, is placed in 120 mesh standard sieves, with banister brush brush powder falling body, the substance weight sifted out, knot is weighed
It is 4.85g that fruit, which takes and weighs average value twice, then
Fineness (%)=4.85/5 × 100%=97%.
A small amount of talcum powder is taken to be applied to the palm of the hand, the back of the hand (having sweat at the palm of the hand).During smearing, there is light fragrance to overflow, it is main
It to be the taste of Radix Astragali volatile oil.Talcum powder is evenly distributed on skin surface quickly, skin is become more moist, skin
Color slightly bleaches.After 5min, palm of the hand sweat is reduced, and the palm of the hand becomes to dry smooth.Talcum powder of the present invention is applied to skin
There is good antipruritic function (referring to itch caused by bite by mosquitos) at skin itch.In addition, talcum powder of the present invention is due to adding
Radix Astragali volatile oil microcapsule and Cortex Cinnamomi volatile oil microcapsules, not only treat the effect of sore, suitable prolonged illness does not rise is easy to detumescence
The effect of the old group, also anti-inflammatory of raw sore, is adapted to arthritic.
Embodiment 5
To test the using effect of talcum powder of the present invention, the talcum powder that the present invention is prepared to embodiment 1 is tried
With investigation experiment, control time：On January 25 day -2015 year 2 month 5th, 2015, investigation result is as shown in table 2.
The talcum powder of table 2 is summarized and overall assessment table for 12 days using feedback
Conclusion：The whole structure positive rating of talcum powder is higher as shown in Table 2, amounts to up to 85.8%, trier is to powder
Fragrance, sophistication and the salubrious degree after all give higher evaluation.Talcum powder preferably can be attached on skin, and
And more favor special natural volatile oil fragrance in the present invention compared to the strong fragrance part trier of traditional talcum powder.By
Natural material all is used in of the invention, allergic phenomena is not produced during trying out.
Finally illustrate, preferred embodiment above is merely illustrative of the technical solution of the present invention and unrestricted, although logical
Cross above preferred embodiment the present invention is described in detail, it is to be understood by those skilled in the art that can be
Various changes are made to it in form and in details, without departing from claims of the present invention limited range.
Claims (8)
1. natural volatile oil microcapsule talcum powder, it is characterised in that count by weight composed of the following components：Cornstarch
70-85 parts, 4-10 parts of superfine silica gel powder, 4-8 parts of magnesium stearate, 1-5 parts of ascorbic acid, 2-10 parts of volatile honeysuckle oil microcapsules,
2-10 parts of Forsythia volatile oil microcapsules, 3-10 parts of Herba Houttuyniae volatile oil microcapsules, 4-8 parts of Radix Saposhnikoviae volatile oil microcapsules, Chinese cassia tree is waved
3-8 parts of hair oil microcapsules, 4-10 parts of volatile argyi leaf oil microcapsules, 3-8 parts of Radix Astragali volatile oil microcapsule；
The Cortex Cinnamomi volatile oil microcapsules or Radix Saposhnikoviae volatile oil microcapsule preparation method are：By cyclodextrin and the mass body of component A
Product is than being 7 ~ 8：1 ratio weighs cyclodextrin and component A；Component A ethanol is dissolved, the ethanol solution of component A, cyclodextrin is obtained
Saturated solution is configured to water；The ethanol solution of component A is added dropwise into cyclodextrin saturated solution, component A-cyclodextrin mixing is made
Solution；24h is placed by 60 ~ 70 DEG C of 2 ~ 3h of water-bath of mixed solution, then under the conditions of 5 ~ 10 DEG C, then stirs and filters, obtain
Trapped substance；Trapped substance is dried under conditions of not higher than 30 DEG C, the volatile oil microcapsule containing component A is produced；The component A is
Cinnamon essential oil or windproof essential oil；
The Herba Houttuyniae volatile oil microcapsules, volatile honeysuckle oil microcapsules, Radix Astragali volatile oil microcapsule, the micro- glue of Forsythia volatile oil
Capsule or volatile argyi leaf oil microcapsule preparation method are：It is 10 ~ 12 by cyclodextrin and the mass volume ratio of B component:1 ratio is weighed
Cyclodextrin and B component；Mixed after B component ethanol is dissolved with cyclodextrin, obtain mixture；Mixture is ground, Bian Yan
Edging adds water, untill B component smell disappears and cyclodextrin surface no longer membranoid substance occurs；Cut after filtering mixture
Thing is stayed, trapped substance is dried under conditions of not higher than 30 DEG C, the volatile oil microcapsule containing B component is produced；The B component is
Cordate houttuynia essential oil, honeysuckle essential oil, Radix Astragali essential oil, Forsythia suspense essential oil or P-Cymene.
2. natural volatile oil microcapsule talcum powder according to claim 1, it is characterised in that count by weight by following
Component is constituted：70 parts of cornstarch, 4 parts of superfine silica gel powder, 4 parts of magnesium stearate, 1 part of ascorbic acid, volatile honeysuckle oil microcapsules 2
Part, 2 parts of Forsythia volatile oil microcapsules, 3 parts of Herba Houttuyniae volatile oil microcapsules, 4 parts of Radix Saposhnikoviae volatile oil microcapsules, Cortex Cinnamomi volatile oil is micro-
3 parts of capsule, 4 parts of volatile argyi leaf oil microcapsules, 3 parts of Radix Astragali volatile oil microcapsule.
3. natural volatile oil microcapsule talcum powder according to claim 1, it is characterised in that count by weight by following
Component is constituted：80 parts of cornstarch, 7 parts of superfine silica gel powder, 6 parts of magnesium stearate, 3 parts of ascorbic acid, volatile honeysuckle oil microcapsules 6
Part, 6 parts of Forsythia volatile oil microcapsules, 7 parts of Herba Houttuyniae volatile oil microcapsules, 6 parts of Radix Saposhnikoviae volatile oil microcapsules, Cortex Cinnamomi volatile oil is micro-
5 parts of capsule, 6 parts of volatile argyi leaf oil microcapsules, 5 parts of Radix Astragali volatile oil microcapsule.
4. natural volatile oil microcapsule talcum powder according to claim 1, it is characterised in that count by weight by following
Component is constituted：85 parts of cornstarch, 10 parts of superfine silica gel powder, 8 parts of magnesium stearate, 5 parts of ascorbic acid, volatile honeysuckle oil microcapsules
10 parts, 10 parts of Forsythia volatile oil microcapsules, 10 parts of Herba Houttuyniae volatile oil microcapsules, 8 parts of Radix Saposhnikoviae volatile oil microcapsules, Chinese cassia tree volatilization
8 parts of oil microcapsule, 10 parts of volatile argyi leaf oil microcapsules, 8 parts of Radix Astragali volatile oil microcapsule.
5. the preparation method of the natural volatile oil microcapsule talcum powder described in claim any one of 1-4, it is characterised in that including
Following steps：
A. the preparation of the volatile oil microcapsule containing component A：It is 7 ~ 8 by cyclodextrin and the mass volume ratio of component A：1 ratio claims
Take cyclodextrin and component A；Component A ethanol is dissolved, the ethanol solution of component A is obtained, cyclodextrin is configured to saturated solution with water；
The ethanol solution of component A is added dropwise into cyclodextrin saturated solution, component A-cyclodextrin mixed solution is made；By mixed solution 60 ~
70 DEG C of 2 ~ 3h of water-bath, then 24h is placed under the conditions of 5 ~ 10 DEG C, then stir and filter, obtain trapped substance；By trapped substance not
Dried under conditions of higher than 30 DEG C, produce the volatile oil microcapsule containing component A；
The component A is cinnamon essential oil or windproof essential oil；
B. the preparation of the volatile oil microcapsule containing B component：It is 10 ~ 12 by cyclodextrin and the mass volume ratio of B component:1 ratio
Weigh cyclodextrin and B component；Mixed after B component ethanol is dissolved with cyclodextrin, obtain mixture；Mixture is ground,
Added water in grinding, untill B component smell disappears and cyclodextrin surface no longer membranoid substance occurs；Filter and obtained after mixture
To trapped substance, trapped substance is dried under conditions of not higher than 30 DEG C, the volatile oil microcapsule containing B component is produced；
The B component is cordate houttuynia essential oil, honeysuckle essential oil, Radix Astragali essential oil, Forsythia suspense essential oil or P-Cymene；
C. by Radix Saposhnikoviae volatile oil microcapsules, Cortex Cinnamomi volatile oil microcapsules, the micro- glue of volatile honeysuckle oil made from step a and step b
Capsule, Forsythia volatile oil microcapsules, Herba Houttuyniae volatile oil microcapsules, volatile argyi leaf oil microcapsules and Radix Astragali volatile oil microcapsule, with
And cornstarch, superfine silica gel powder, magnesium stearate and ascorbic acid are ground, cross 80 ~ 100 mesh sieves respectively, are mixed by proportional quantity
After produce talcum powder.
6. preparation method according to claim 5, it is characterised in that cyclodextrin saturated solution described in the step a
Preparation process is as follows：It is 1 by mass volume ratio:Cyclodextrin is dissolved in after water by 10 ratio, is placed in 60 DEG C of water-baths in heating
Stirring, treats that cyclodextrin is completely dissolved and produces.
7. preparation method according to claim 5, it is characterised in that component A described in the step a-cyclodextrin mixing
Solution places 24h in 60 DEG C of water-bath 2h, then under the conditions of 5 DEG C.
8. preparation method according to claim 5, it is characterised in that grind talcum powder each component respectively in the step c
100 mesh sieves are crossed after mill.
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| CN106265276A (en) * | 2016-08-30 | 2017-01-04 | 瑞普（天津）生物药业有限公司 | One boar talcum powder and preparation method thereof |
| CN106265435A (en) * | 2016-08-30 | 2017-01-04 | 瑞普（天津）生物药业有限公司 | A kind of dog talcum powder and preparation method thereof |
| CN106361618B (en) * | 2016-09-12 | 2019-06-18 | 华南理工大学 | A kind of sustained release mosquito-repellent essential oil microcapsules children's talcum powder and preparation method thereof |
| CN107854338A (en) * | 2017-12-20 | 2018-03-30 | 安徽省旌德博仕达农业科技有限公司 | A kind of sealwort talcum powder and preparation method thereof |
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| CN102895163B (en) * | 2012-09-21 | 2014-08-13 | 乔海平 | Natural green talcum powder |
| CN103271849A (en) * | 2013-05-10 | 2013-09-04 | 周卫忠 | Improved baby powder |
| CN103651589B (en) * | 2013-09-26 | 2016-06-08 | 信阳农林学院 | Herba Chenopodii volatile oil microcapsule agent and preparation method |
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