CN104622736A - Tibetan medicinal extract skin-care product and preparation method thereof - Google Patents
Tibetan medicinal extract skin-care product and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a Tibetan medicinal extract skin-care product and a preparation method thereof. The skin-care product comprises the following raw materials in percentage by weight: 7-10% of gentiana macrophylla extract, 3-5% of sapodilla extract and 3-5% of senecio cineraria extract. The skin-care product comprises facial cleanser, essence and emulsion. The main raw materials are Tibetan medicaments, so the skin-care effect is good and the value of the Tibetan medicament can be sufficiently utilized.
Description
Technical field
The present invention relates to cosmetics shower, be specifically related to a kind of Tibetan medicine extract skin care product.
Background technology
Containing various active material in Chinese crude drug, as polysaccharide, saponin, glucosides, aminoacid isoreactivity composition, has moisturizing, antioxidation, anti-ageing beauty functions of waiting for a long time.And according in many ways studying, the active substance of Tibetan medicine material is higher than low altitude area content, even with kind medical material, the effective ingredient of Tibetan medicine material is just high, but also containing various trace elements, aminoacid, belongs to the superior good merchantable brand in crude drug.But the utilization of current Tibetan medicine is comparatively single, is unfavorable for abundant exploitation.
Summary of the invention
The object of the present invention is to provide a kind of at Tibetan medicine extract skin care product, to solve the above-mentioned problems in the prior art.
Technical scheme provided by the invention is as follows:
A kind of Tibetan medicine extract skin care product, it is characterized in that, by weight, its raw material comprises: Radix Gentianae Macrophyllae extract 7-10%, Herba Herminii extract 3-5%, snow chrysanthemum extract 3-5%.
Wherein, the preferred preparation method of Radix Gentianae Macrophyllae extract is: dried in the shade by Gentiana tibetica, pulverizes, takes its powder 10g, add 70% ethanol, and consumption is 6-8 times of medical material, and heat 80 DEG C-85 DEG C, the time is 1-1.5h, should constantly stir in heating process.Centrifugal, filter, collect filtrate, filtering residue repeats extraction twice, merges three filtrates, filtrate is evaporated on a rotary evaporator, treat alcohol-free taste, obtain Radix Gentianae Macrophyllae extract.
Wherein, the preferred preparation method of Herba Herminii extract is: cleaned up by Herba Herminii, puts the oven dry of 40 DEG C, baking oven, then ground, take powder 10g, add distilled water, consumption is 20-25 times of medical material, ultrasound wave 40-45 DEG C is extracted 15-20min, centrifugal, filters, repeat once, merging filtrate, filtrate adds activated carbon decolorizing 10g, filters.Then refining, add chloroform, n-butyl alcohol, is 1: 0.25 by the volume ratio of chloroform and n-butyl alcohol, and the volume ratio of sample and chloroform-n-butyl alcohol is 1: 1, and extraction time is 30min, is separated, and collects, obtains Herba Herminii extract.
Wherein, the preferred preparation method of snow chrysanthemum extract is: chrysanthemum is avenged in Tianshan Mountains and dries in the shade, grind, take 10g, add 50% ethanol, consumption is 15-20 times of medical material, ultrasound wave 100W, temperature 40 DEG C, extracts 40min-60min, centrifugal, filter, collect filtrate, repeat once, merging filtrate, filtrate is evaporated on a rotary evaporator, treat alcohol-free taste, chrysanthemum extract must be avenged.
In a preferred embodiment of the present invention, described skin care item are cleansing milk, by weight, comprising:
Aqueous phase: Radix Gentianae Macrophyllae extract 7-10%, Herba Herminii extract 3-5%, snow chrysanthemum extract 3-5%, potassium hydroxide 2-4%, glycerol 15-20%, propylene glycol 2-4%, sodium alkyl benzene sulfonate 8-10%, deionized water to 100%
Oil phase 10-30%: tetradecylic acid 3-5%, polyoxyethylene stearyl base ether phosphate 8-13%, olive oil 2-5%, myristic acid 5-7%, EDETATE SODIUM 0.1-0.5%
Fructus Fragariae Ananssae quintessence oil 3-5 drips, methyl parahydroxybenzoate 0.002-0.005%.
The preparation method of aforesaid a kind of Tibetan medicine extract skin care product, comprises the steps: to take respectively material in aqueous phase and oil phase in container, places in water-bath and be heated to 75 DEG C.First oil phase is put into emulsifying pot, open and stir, then aqueous phase is added in oil phase fast, in the process that aqueous phase adds, may be there is the soap blank phenomenon of of short duration a small amount of generation in system, this phenomenon can no matter, waits aqueous phase to add completely to terminate rear soap blank naturally can disappear; After aqueous phase has added, when keeping system temperature to be not less than 80 DEG C, insulation saponification 30-60 minute; Add surfactant after soap blank terminates, now should note avoiding making because of stirring system produce bubble; Add Fructus Fragariae Ananssae quintessence oil and methyl parahydroxybenzoate when being cooled to about 55 DEG C: be cooled to 40-45 DEG C, when system ties cream, keep temperature-resistant, stir more than 30 minutes, stirring can discharging after terminating.Chemically examine after testing qualified after can carry out subpackage, get product.
In a preferred embodiment of the present invention, described skin care item are elite dew, comprise by weight:
A phase: deionized water (To 100%) glycerol 3-5%, butanediol 0.5-1.3%, 1,3 propylene glycol 0.5-1.3%, hyaluronate sodium 0.02-0.05%, carbomer 3-8%,
B phase: Radix Gentianae Macrophyllae extract 6-10%, Herba Herminii extract 4-6%, snow chrysanthemum extract 4-6%, Stigma Croci extract 1.5-2.8%, Flos Hibisci Rosae-Sinensis extract 1.5-2.5%
C phase: PEG-60 castor oil hydrogenated (in right amount), 2-5 drips orange blossom quintessence oil, methyl parahydroxybenzoate (in right amount).
The preparation method of aforesaid a kind of Tibetan medicine extract skin care product, comprise the steps: accurately to take A, B, C phase, A phase be heated to dissolve in 80 DEG C, insulation 15min, is cooled to less than 45 DEG C and adds B phase, stir, the water-soluble system temperature that is cooled to is less than 40 DEG C, then adds C phase, stirs, continue to cool to room temperature, detect qualified use 1 micron and be in fear of discharging after membrane filtration.Chemically examine after testing qualified after can carry out subpackage, get product.
In a preferred embodiment of the present invention, described skin care item are elite breast, and by weight, its raw material comprises:
Aqueous phase: Radix Gentianae Macrophyllae extract 7-12%, snow chrysanthemum extract 4-6%, Herba Herminii extract 4-6%, Stigma Croci 1-2%, oat polypeptide 1-1.8%, Bulbus Lilii extract 1-1.8%, glycerol 10-15%, propylene glycol 1-2%, 1,3 butanediol 1-2%, hyaluronate sodium 0.8-1.5%, triethanolamine 1-2.5%, glycyrrhizic acid dipotassium 0.2-0.8%, Kappa nurse 12-18%, deionized water (To100%)
Oil phase: Fructus oleae europaeae fruit oil 2-4%, American Avocado Tree oil 1-3%, agate breast draws fruit oil 1-2.5%, glyceryl stearate 2-4.5%, glyceryl monostearate 1.5-2.5% squalane 1-1.5%, cetearyl alcohol polyoxyethylenated alcohol olive oil acid esters 1-2%, vitamin E 0.1-0.3%
Orange blossom quintessence oil 2-3 drips, and methyl parahydroxybenzoate 0.002-0.005%, all the other are supplied with distilled water.
The preparation method of aforesaid a kind of Tibetan medicine extract skin care product, it is characterized in that, comprise the steps: to take aqueous phase respectively and oil phase is put in clean beaker, heat at water-bath, rapidly oil phase is poured in aqueous phase when temperature reaches 85 DEG C, use magnetic stirrer immediately, after a few minutes, cream is moved on on magnetic stirring apparatus from water-bath, adds Semen pruni armeniacae quintessence oil and methyl parahydroxybenzoate, continue to stir.Until emulsion temperature is to room temperature state, stop stirring.Until its temperature cooling after, chemically examine after testing qualified after can carry out subpackage, get product.
The main active gentiopicrin Scavenging ability of Radix Gentianae Macrophyllae is remarkable, and gentiopicrin standard concentration is at 0.25 ~ 10.00g/L, and removing OH free radical ability shows a rising trend with the increase of concentration, reaches 40.74% ~ 87.03%.。There are some researches show, the RC50 of gentiopicrin antioxidant activity is 7.5 × 10-2mg/ml.Herba Herminii contains ginsenoside, crude polysaccharides.Ginsenoside's Main Function is the low physiological system of stimulatory function, makes its biochemical reactions be tending towards normal, and stops the vicious cycle because a variety of causes causes, and has the function of postponing cell ageing, extending cell survival; And crude polysaccharides can play anti-aging effects by improving Radical Metabolism.Tianshan Mountains snow chrysanthemum extract is to hydroxy radical (OH), Superoxide anion free radical (O
2-) and the scavenging action that had of 1,1-diphenyl-2-trinitrophenyl-hydrazine (DPPH) free radical.When the mass concentration of 50% ethanol snow chrysanthemum extract is 1.0g/L, OH, O
2-be respectively 86%, 97% and 71% with the clearance rate of DPPH free radical, Scavenging activity is suitable with VC, has good antioxidation.
Seen from the above description, the invention provides a kind of Tibetan medicine extract skin care product, its raw material is mainly Radix Gentianae Macrophyllae, Tianshan Mountains Tibetan medicine such as pure natural such as snow chrysanthemum, Herba Herminii etc.Its Scavenging ability is remarkable, and the protein be rich in and aminoacid, can effectively regulate human body acid-base value, strengthens body immunity and resisting fatigue, anti-aging effects; Increase water and the effect of skin self, wake the energy of skin self up, strengthen self-repairing capability and the moisture-keeping functions of skin, by the enough nutrition of supply melanocyte, activate its metabolic ability, thus accelerate melanic homergy, reach whitening function; SPF (sun protection factor) is quite high, can effectively protect skin to be subject to ultraviolet damage, improve cutaneous pigmentation, delaying human body caducity.Have broad prospects in skin care item of new generation, also make the purposes of Tibetan medicine further expand.
Detailed description of the invention
Embodiment 1
The preparation method of Radix Gentianae Macrophyllae extract is: dried in the shade by Gentiana tibetica, pulverizes, takes its powder 10g, add 70% ethanol, and consumption is 6-8 times of medical material, and heat 80 DEG C-85 DEG C, the time is 1-1.5h, should constantly stir in heating process.Centrifugal, filter, collect filtrate, filtering residue repeats extraction twice, merges three filtrates, filtrate is evaporated on a rotary evaporator, treat alcohol-free taste, obtain Radix Gentianae Macrophyllae extract.
The preparation method of Herba Herminii extract is: cleaned up by Herba Herminii, puts the oven dry of 40 DEG C, baking oven, is then ground, take powder 10g, add distilled water, consumption is 20-25 times of medical material, and ultrasound wave 40-45 DEG C is extracted 15-20min, centrifugal, filter, repeat once, merging filtrate, filtrate adds activated carbon decolorizing 10g, filters.Then refining, add chloroform, n-butyl alcohol, is 1: 0.25 by the volume ratio of chloroform and n-butyl alcohol, and the volume ratio of sample and chloroform-n-butyl alcohol is 1: 1, and extraction time is 30min, is separated, and collects, obtains Herba Herminii extract.
The preparation method of snow chrysanthemum extract is: chrysanthemum is avenged in Tianshan Mountains and dries in the shade, grind, take 10g, add 50% ethanol, consumption is 15-20 times of medical material, ultrasound wave 100W, temperature 40 DEG C, extracts 40min-60min, centrifugal, filter, collect filtrate, repeat once, merging filtrate, filtrate is evaporated on a rotary evaporator, treats alcohol-free taste, chrysanthemum extract must be avenged.
Embodiment 2 cleansing milk
By weight, comprising:
Aqueous phase: Radix Gentianae Macrophyllae extract 7-10%, Herba Herminii extract 3-5%, snow chrysanthemum extract 3-5%, potassium hydroxide 2-4%, glycerol 15-20%, propylene glycol 2-4%, sodium alkyl benzene sulfonate 8-10%, deionized water To 100%
Oil phase 10-30%: tetradecylic acid 3-5%, polyoxyethylene stearyl base ether phosphate 8-13%, olive oil 2-5%, myristic acid 5-7%, EDETATE SODIUM 0.1-0.5%
Fructus Fragariae Ananssae quintessence oil 3-5 drips, methyl parahydroxybenzoate 0.002-0.005%.
Preparation method, comprises the steps: to take respectively material in aqueous phase and oil phase in container, places in water-bath and be heated to 75 DEG C.First oil phase is put into emulsifying pot, open and stir, then aqueous phase is added in oil phase fast, in the process that aqueous phase adds, may be there is the soap blank phenomenon of of short duration a small amount of generation in system, this phenomenon can no matter, waits aqueous phase to add completely to terminate rear soap blank naturally can disappear; After aqueous phase has added, when keeping system temperature to be not less than 80 DEG C, insulation saponification 30-60 minute; Add surfactant after soap blank terminates, now should note avoiding making because of stirring system produce bubble; Add Fructus Fragariae Ananssae quintessence oil and methyl parahydroxybenzoate when being cooled to about 55 DEG C: be cooled to 40-45 DEG C, when system ties cream, keep temperature-resistant, stir more than 30 minutes, stirring can discharging after terminating.Chemically examine after testing qualified after can carry out subpackage, get product.
Embodiment 3 elite is revealed,
Comprise by weight:
A phase: deionized water (To 100%) glycerol 3-5%, butanediol 0.5-1.3%, 1,3 propylene glycol 0.5-1.3%, hyaluronate sodium 0.02-0.05%, carbomer 3-8%,
B phase: Radix Gentianae Macrophyllae extract 6-10%, Herba Herminii extract 4-6%, snow chrysanthemum extract 4-6%, Stigma Croci extract 1.5-2.8%, Flos Hibisci Rosae-Sinensis extract 1.5-2.5%
C phase: PEG-60 castor oil hydrogenated (in right amount), 2-5 drips orange blossom quintessence oil, methyl parahydroxybenzoate (in right amount).
Preparation method, comprise the steps: accurately to take A, B, C phase, A phase be heated to dissolve in 80 DEG C, insulation 15min, is cooled to less than 45 DEG C and adds B phase, stir, the water-soluble system temperature that is cooled to is less than 40 DEG C, then adds C phase, stirs, continue to cool to room temperature, detect qualified use 1 micron and be in fear of discharging after membrane filtration.Chemically examine after testing qualified after can carry out subpackage, get product.
Embodiment 4 elite breast,
By weight, its raw material comprises:
Aqueous phase: Radix Gentianae Macrophyllae extract 7-12%, snow chrysanthemum extract 4-6%, Herba Herminii extract 4-6%, Stigma Croci 1-2%, oat polypeptide 1-1.8%, Bulbus Lilii extract 1-1.8%, glycerol 10-15%, propylene glycol 1-2%, 1,3 butanediol 1-2%, hyaluronate sodium 0.8-1.5%, triethanolamine 1-2.5%, glycyrrhizic acid dipotassium 0.2-0.8%, Kappa nurse 12-18%, deionized water (To 100%)
Oil phase: Fructus oleae europaeae fruit oil 2-4%, American Avocado Tree oil 1-3%, agate breast draws fruit oil 1-2.5%, glyceryl stearate 2-4.5%, glyceryl monostearate 1.5-2.5% squalane 1-1.5%, cetearyl alcohol polyoxyethylenated alcohol olive oil acid esters 1-2%, vitamin E 0.1-0.3%
Orange blossom quintessence oil 2-3 drips, and methyl parahydroxybenzoate 0.002-0.005%, all the other are supplied with distilled water.
Preparation method is as follows: take aqueous phase respectively and oil phase is put in clean beaker, heat at water-bath, rapidly oil phase is poured in aqueous phase when temperature reaches 85 DEG C, use magnetic stirrer immediately, after a few minutes, cream is moved on on magnetic stirring apparatus from water-bath, adds Semen pruni armeniacae quintessence oil and methyl parahydroxybenzoate, continue to stir.Until emulsion temperature is to room temperature state, stop stirring.Until its temperature cooling after, chemically examine after testing qualified after can carry out subpackage, get product.
Claims (10)
1. a Tibetan medicine extract skin care product, is characterized in that, by weight, its raw material comprises: Radix Gentianae Macrophyllae extract 7-10%, Herba Herminii extract 3-5%, snow chrysanthemum extract 3-5%.
2. a kind of Tibetan medicine extract skin care product as claimed in claim 1, it is characterized in that, the preparation method of Radix Gentianae Macrophyllae extract 7-10% is: dried in the shade by Gentiana tibetica, pulverize, take its powder, add 70% ethanol, consumption is 6-8 times of medical material, heat 80 DEG C-85 DEG C, the time is 1-1.5h, should constantly stir in heating process.Centrifugal, filter, collect filtrate, filtering residue repeats extraction twice, merges three filtrates, filtrate is evaporated on a rotary evaporator, treat alcohol-free taste, obtain Radix Gentianae Macrophyllae extract.
3. a kind of Tibetan medicine extract skin care product as claimed in claim 1, is characterized in that, the preparation method of Herba Herminii extract is: cleaned up by Herba Herminii, put oven for drying, then ground, take powder, add distilled water, consumption is 20-25 times of medical material, and ultrasound wave 40-45 DEG C is extracted 15-20min, centrifugal, filter, repeat once, merging filtrate, filtrate adds activated carbon decolorizing 10g, filters.Then refining, add chloroform, n-butyl alcohol, is 1: 0.25 by the volume ratio of chloroform and n-butyl alcohol, and the volume ratio of sample and chloroform-n-butyl alcohol is 1: 1, and extraction time is 30min, is separated, and collects, obtains Herba Herminii extract.
4. a kind of Tibetan medicine extract skin care product as claimed in claim 1, is characterized in that, the preparation method of snow chrysanthemum extract is: chrysanthemum is avenged in Tianshan Mountains and dries in the shade, grind, take, add 50% ethanol, consumption is 15-20 times of medical material, ultrasound wave 100W, temperature 40 DEG C, extract 40min-60min, centrifugal, filter, collect filtrate, repeat once, merging filtrate, filtrate is evaporated on a rotary evaporator, treats alcohol-free taste, chrysanthemum extract must be avenged.
5. a kind of Tibetan medicine extract skin care product as claimed in claim 1, is characterized in that: described skin care item are cleansing milk, by weight, comprising:
Aqueous phase: Radix Gentianae Macrophyllae extract 7-10%, Herba Herminii extract 3-5%, snow chrysanthemum extract 3-5%, potassium hydroxide 2-4%, glycerol 15-20%, propylene glycol 2-4%, sodium alkyl benzene sulfonate 8-10%, deionized water is supplemented to 100%;
Oil phase 10-30%: tetradecylic acid 3-5%, polyoxyethylene stearyl base ether phosphate 8-13%, olive oil 2-5%, myristic acid 5-7%, EDETATE SODIUM 0.1-0.5%;
Fructus Fragariae Ananssae quintessence oil 3-5 drips, methyl parahydroxybenzoate 0.002-0.005%.
6. the preparation method of a kind of Tibetan medicine extract skin care product as claimed in claim 5, comprises the steps: to take respectively material in aqueous phase and oil phase in container, places in water-bath and be heated to 75 DEG C; First oil phase is put into emulsifying pot, open and stir, then aqueous phase is added in oil phase fast; After aqueous phase has added, when keeping system temperature to be not less than 80 DEG C, insulation saponification 30-60 minute; Add surfactant after soap blank terminates, now should note avoiding making because of stirring system produce bubble; Add Fructus Fragariae Ananssae quintessence oil and methyl parahydroxybenzoate when being cooled to about 55 DEG C: be cooled to 40-45 DEG C, when system starts to tie cream, keep temperature-resistant, stir more than 30 minutes, stirring can discharging after terminating; Chemically examine after testing qualified after carry out subpackage, get product.
7. a kind of Tibetan medicine extract skin care product as claimed in claim 1, is characterized in that: described skin care item are elite dew, comprise by weight:
A phase: deionized water, glycerol 3-5%, butanediol 0.5-1.3%, 1,3 propylene glycol 0.5-1.3%, hyaluronate sodium 0.02-0.05%, carbomer 3-8%,
B phase: Radix Gentianae Macrophyllae extract 6-10%, Herba Herminii extract 4-6%, snow chrysanthemum extract 4-6%, Stigma Croci extract 1.5-2.8%, Flos Hibisci Rosae-Sinensis extract 1.5-2.5%;
C phase: PEG-60 castor oil hydrogenated is appropriate, and 2-5 drips orange blossom quintessence oil, and methyl parahydroxybenzoate is appropriate.
8. the preparation method of a kind of Tibetan medicine extract skin care product as claimed in claim 7, comprise the steps: accurately to take A, B, C phase, A phase be heated to dissolve in 80 DEG C, insulation 15min, is cooled to less than 45 DEG C and adds B phase, stir, the water-soluble system temperature that is cooled to is less than 40 DEG C, then adds C phase, stirs, continue to cool to room temperature, detect qualified use 1 micron and be in fear of discharging after membrane filtration; Chemically examine after testing qualified after carry out subpackage, get product.
9. a kind of Tibetan medicine extract skin care product as claimed in claim 1, is characterized in that: described skin care item are elite breast, and by weight, its raw material comprises:
Aqueous phase: Radix Gentianae Macrophyllae extract 7-12%, snow chrysanthemum extract 4-6%, Herba Herminii extract 4-6%, Stigma Croci 1-2%, oat polypeptide 1-1.8%, Bulbus Lilii extract 1-1.8%, glycerol 10-15%, propylene glycol 1-2%, 1,3 butanediol 1-2%, hyaluronate sodium 0.8-1.5%, triethanolamine 1-2.5%, glycyrrhizic acid dipotassium 0.2-0.8%, Kappa nurse 12-18%, deionized water;
Oil phase: Fructus oleae europaeae fruit oil 2-4%, American Avocado Tree oil 1-3%, agate breast draws fruit oil 1-2.5%, glyceryl stearate 2-4.5%, glyceryl monostearate 1.5-2.5%, squalane 1-1.5%, cetearyl alcohol polyoxyethylenated alcohol olive oil acid esters 1-2%, vitamin E 0.1-0.3%;
Orange blossom quintessence oil 2-3 drips, and methyl parahydroxybenzoate 0.002-0.005%, all the other are supplied with distilled water.
10. the preparation method of a kind of Tibetan medicine extract skin care product as claimed in claim 9, it is characterized in that, comprise the steps: to take aqueous phase respectively and oil phase is put in clean beaker, heat at water-bath, rapidly oil phase is poured in aqueous phase when temperature reaches 85 DEG C, use magnetic stirrer immediately, after a few minutes, cream is moved on on magnetic stirring apparatus from water-bath, add Semen pruni armeniacae quintessence oil and methyl parahydroxybenzoate, continue to stir, until emulsion temperature is to room temperature state, stop stirring.Until its temperature cooling after, chemically examine after testing qualified after carry out subpackage, get product.
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| CN105902420A (en) * | 2015-10-16 | 2016-08-31 | 湖北文理学院 | Exfoliating facial cleanser |
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| CN108567600A (en) * | 2017-03-10 | 2018-09-25 | 香港科技大学 | Flower of Radix Gentianae extracting solution and its preparation method and application |
| CN106994108A (en) * | 2017-03-25 | 2017-08-01 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of gentle eye shadow cream |
| CN106798718A (en) * | 2017-03-28 | 2017-06-06 | 佛山汇沐化学科技有限公司 | A kind of moisture surge treatment formula |
| CN107397707A (en) * | 2017-07-25 | 2017-11-28 | 山东圣洲海洋生物科技股份有限公司 | A kind of skin care topical composition and preparation method thereof |
| CN108354869A (en) * | 2018-04-28 | 2018-08-03 | 广东巴松那生物科技有限公司 | A kind of essence lotion and preparation method thereof that fixes of the coreopsis tinctoria extract containing Tianshan Mountains |
| CN108721174A (en) * | 2018-08-24 | 2018-11-02 | 项佳红 | A kind of anti-aging skin care product and preparation method thereof of addition Fructus Cannabis extract |
| CN109620768A (en) * | 2018-11-19 | 2019-04-16 | 范梦婷 | Polypeptide targets factor coniplexes |
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Application publication date: 20150520 |