CN104592815B - Alkali-resistant primer and preparation method thereof - Google Patents
Alkali-resistant primer and preparation method thereof Download PDFInfo
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- CN104592815B CN104592815B CN201410830160.9A CN201410830160A CN104592815B CN 104592815 B CN104592815 B CN 104592815B CN 201410830160 A CN201410830160 A CN 201410830160A CN 104592815 B CN104592815 B CN 104592815B
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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Abstract
The present invention relates to a kind of alkali-resistant primer and preparation method thereof, the alkali-resistant primer is formulated by following components and ratio of weight and number：Water, hydroxyethyl cellulose, water-soluble multifunctional auxiliary agent, aqueous dispersion, aqueous wetting agent, aqueous defoamer, titanium dioxide, mica powder, talcum powder, calcium carbonate, emulsion, coalescents, antifreezing agent, sterilization antiseptic；The emulsion is butadiene styrene copolymer emulsion.Alkali-resistant primer prepared by the present invention not only has alkali resistant effect, and has sealing process, can effectively prevent the wall accumulation of salt in the surface soil.
Description
Technical field
The present invention relates to a kind of architectural decoration coating, more particularly to a kind of alkali-resistant primer and preparation method thereof.
Background technology
Preceding increasing using the building of exterior coating, there is the problems such as decortication, foaming, explosion, discoloration, shadow in some metopes
The using effect of exterior coating is rung.It is largely priming paint to be short in understanding or without just to find out its cause, in addition to coating quality
Caused by true use.External wall base material is mostly cement mortar or concrete surface, is characterized in that more spaces, alkalescence are strong, wherein
Loose structure makes its water imbibition strong, causes coating surface not smooth enough, easily causes film to wrinkle, and may cause dried coating film
It is too fast and cause finish paint cracking waste finish paint；Alkalescence can cause by force the chemical degradation of resin in coating, accelerate ginkgo seeds, subtract
The useful life of few coating.So priming paint must be used in exterior wall application.
Because the osmosis of priming paint is strong, the pore of base material can be formed effectively all rescue measures proved ineffectual closing, so as to avoid
Alkali point and water soluble salt ooze out surface with moisture by the migration of capillarity in base material, while prevent the frosting accumulation of salt in the surface soil, and protect
Mask can avoid porous basal plane from improving the decorative effect of finish paint to the taken in excess of finish paint again not by chemical erosion,
Save finish paint dosage.Because big portion's priming paint is opaque white coating, itself there is certain alkali resistant effect, but make without closing
With, it is impossible to prevent the accumulation of salt in the surface soil.
The content of the invention
The invention aims to overcome weak point of the prior art, there is provided a kind of alkali-resistant primer and its preparation side
Method, alkali-resistant primer prepared by the present invention not only has alkali resistant effect, and has sealing process, can effectively prevent the wall accumulation of salt in the surface soil.
What the present invention was realized in：A kind of alkali-resistant primer, is formulated by following components and ratio of weight and number：
The emulsion is butadiene-styrene copolymer emulsion.
The emulsion is butadiene-styrene copolymer emulsion, and it is 51 ± 1.0% that it contains admittedly, pH value 7.0-9.0, MFFT
About 20 DEG C, viscosity 50-300mPa.S of (MFT), there is excellent adhesive attraction, water resistance, high color stuffing bearing capacity
Milky white liquid；With excellent adhesive attraction, water resistance, low permeability, the milky white liquid of high color stuffing bearing capacity, it is into
Film thing, it is possible to provide good cohesive force.The water can use common running water or other clean waters, and it is as scattered pigment
Dispersion, regulation mashing when slurry viscosity.
Further prioritization scheme is：The hydroxyethyl cellulose is the water dissolvable cellulose ether of nonionic, Ke Yishi
The hydroxyethyl cellulose of different molecular weight, thickener when it is as regulation dispersion mashing, has pigment individual scattered well
Viscosity.The water-soluble multifunctional auxiliary agent uses Tao Shi AMP-95 multifunctional assistants；It is primarily used to adjust acid-base value, has
Wetting, scattered and stabilising system effect.The aqueous dispersion uses the acrylate copolymer ammonia salt aqueous solution, can be poly- carboxylic
Acid sodium-salt type dispersant or acrylic copolymer ammonium salt.
Further prioritization scheme is：The aqueous wetting agent environment-friendly type non-ionic emulsifier wetting agent, without APEO, for applying
Material wetting, the mashing viscosity of color stuffing is reduced, improve the compatibility of color stuffing and emulsion, there is excellent penetration and reduce table
The wetting aid disperseed as color stuffing of face tension force；The aqueous defoamer is nonionic defoamer, molecular antifoaming agent
Or mineral oil antifoam agent or organic silicon defoamer；Using the defoamer without compatibility and recoating problem, rise and disappear in formula system
Infusion acts on.The titanium dioxide is anatase thpe white powder or rutile type titanium white, and hiding rare is provided in formula system.
Further prioritization scheme is：The mica powder is that proportion is 2.8-2.9g/cm3, oil absorption 40-70, average specific
Hold for 35, the white powder that rate is 1.58 is hit in refraction；The mica powder reduces the permeability of coating in formulation for coating material system, from
And reduce the permeability rate of paint film.The talcum powder is 1250 mesh talcum powder, and the permeability of coating is reduced in formula system, so as to
Reduce the permeability rate of paint film.The calcium carbonate can use 800 mesh powdered whitings；Filling is played in formula system and reduces cost
Effect.
Further prioritization scheme is：The coalescents are Yi Shiman Texanol, and purity is more than 98.5%, and acidity is small
In 0.05, proportion 0.945-0.955g/ml, moisture content is less than 0.1%, and index of refraction is the limpid clean of 1.4411-1.4433
Coalescents liquid, film forming matter can be helped to turn into a continuous film more than 5 DEG C.
Further prioritization scheme is：The antifreezing agent is 1,2-PD, its purity >=99.7%, moisture≤0.08%,
Boiling range is 184-190 DEG C, relative density 1.037-1.039, the colourless transparent liquid or ethylene glycol of colourity≤10；Can
Prevent that film forming matter is freezing when storing for -5 DEG C to 0 DEG C.
Further prioritization scheme is：The sterilization antiseptic uses isothiazolinone disinfecting agent, has sterilization and anticorrosion effect.
The preparation method of above-mentioned alkali-resistant primer, it includes following the step of sequentially carrying out：
(1), 29-36 parts water is added in dispersion cylinder, 0.5-0.6 parts are sequentially added under 350-550r/min stirrings
Hydroxyethyl cellulose and 0.1-0.2 part water-soluble multifunctional auxiliary agents, stir 1min-3min；
(2) rotating speed, is improved to after 800-1000r/min, sequentially adds 0.5-0.7 parts aqueous dispersion, 0.1-0.2 part water
Property wetting agent, 0.35-0.4 parts aqueous defoamer, 1-10 parts titanium dioxide, 10-15 parts mica powder, 5-10 parts talcum powder, 10-15 parts
After calcium carbonate, improve rotating speed again and disperse 15min-20min to 1800-2000r/min and under this rotating speed, detection afterwards until
System fineness≤60；
(3), reduce rotating speed to 1000-1200r/min stirrings under sequentially add 20-25 parts emulsion, 1.0-1.5 parts into
Film auxiliary agent, 1.2-1.5 parts antifreezing agent, 0.2-0.3 part sterilization antiseptics, alkali-resistant primer is obtained after being sufficiently stirred 15-20min.
Alkali-resistant primer prepared by the present invention has the following advantages that：Combine what is prepared using component of the present invention and proportioning
Alkali-resistant primer not only has alkali resistant effect, and has sealing process, can effectively prevent the wall accumulation of salt in the surface soil.
The selected various Material cladding collocation of the present invention, using experiment of many factor design method, Orthogonal Experiment and Design determines group
Part and its weight proportion, are a kind of alkali-resistant primers for priming paint exploitation, and alkali-resistant primer of the present invention has compared with the alkali-resistant paint of biography
Have the following advantages：Not only there is alkali resistant effect, also with sealing process, effectively prevent the wall accumulation of salt in the surface soil, its environmental protection index can also lead to
Cross HJ2537-2014《Environmental labelling product technical requirements water paint》Exterior coating priming paint limits of harmful substances standard.
Specific advantage is as follows：
(1), alkali-resistant primer of the present invention can effectively prevent water soluble salt and alkali from separating out, and protective topcoat is from saline and alkaline erosion.
(2), the water-tolerant of alkali-resistant primer of the present invention, low permeability rate, the wall accumulation of salt in the surface soil is effectively prevented, and adhesive force is strong, tool
There is penetrating power, can effectively reinforce bulk matrix.
(3), alkali-resistant primer of the present invention has the excellent feature of environmental protection：Low VOC, without APEO, formaldehyde.
Embodiment
With reference to specific embodiment, the present invention will be described in detail.
(1) embodiment is as follows：
A kind of alkali-resistant primer, is formulated by following components and ratio of weight and number：
The emulsion is butadiene-styrene copolymer emulsion.
A kind of preparation method of alkali-resistant primer, it includes following the step of sequentially carrying out：
(1), 29-36 parts water is added in dispersion cylinder, 0.5-0.6 parts are sequentially added under 350-550r/min stirrings
Hydroxyethyl cellulose and 0.1-0.2 part water-soluble multifunctional auxiliary agents, stir 1min-3min；
(2) rotating speed, is improved to after 800-1000r/min, sequentially adds 0.5-0.7 parts aqueous dispersion, 0.1-0.2 part water
Property wetting agent, 0.35-0.4 parts aqueous defoamer, 1-10 parts titanium dioxide, 10-15 parts mica powder, 5-10 parts talcum powder, 10-15 parts
After calcium carbonate, improve rotating speed again and disperse 15min-20min to 1800-2000r/min and under this rotating speed, detection afterwards until
System fineness≤60；
(3), reduce rotating speed to 1000-1200r/min stirrings under sequentially add 20-25 parts emulsion, 1.0-1.5 parts into
Film auxiliary agent, 1.2-1.5 parts antifreezing agent, 0.2-0.3 part sterilization antiseptics, alkali-resistant primer is obtained after being sufficiently stirred 15-20min.
Emulsion described in said components uses 7623 emulsions of BASF.The water uses ordinary tap water.The hydroxyl second
Base cellulose is using Asia across imperial 250HBR hydroxyethyl celluloses.The water-soluble multifunctional auxiliary agent is multi-functional using Tao Shi AMP-95
Auxiliary agent.The aqueous dispersion uses the DISPEX A40 aqueous dispersions of vapour bar.The aqueous wetting agent is using sea profit 2405
Aqueous wetting agent.CF-246 and extra large river A10 defoamer of the aqueous defoamer using Bu Levin gram Lays.The titanium dioxide uses one hundred
Profit connection BLR-699 titanium dioxides.The mica powder is using U.S. high mica powder.Talcum powder uses the rich mesh talcum powder of powder 1250 of the rising sun.
The calcium carbonate uses the mesh powdered whiting of agriculture-countryside-farmer 700.The coalescents use Yi Shiman Texanol coalescents.Institute
State the propane diols that antifreezing agent uses Shandong Depew chemical industry.The sterilization antiseptic uses Troy RS sterilization antiseptics.It is described every
Kind component can also use similar other type products.
(2) embodiment is as follows：
Embodiment 1：A kind of alkali-resistant primer, is formulated by following components and ratio of weight and number：
A kind of preparation method of alkali-resistant primer, it includes following the step of sequentially carrying out：
(1), 32.1 parts of water are added in dispersion cylinder, 0.5 part of ethoxy fibre is sequentially added under 550r/min stirrings
Dimension element and 0.1 part of water-soluble multifunctional auxiliary agent, stir 1min；
(2), improve rotating speed to after 1000r/min, sequentially add 0.6 part of aqueous dispersion, 0.1 part of aqueous wetting agent,
After 0.35 part of aqueous defoamer, 5 parts of titanium dioxides, 12 parts of mica powders, 8 parts of talcum powder, 15 parts of calcium carbonate, rotating speed is improved extremely again
2000r/min simultaneously disperses 15min under this rotating speed, and detection is until system fineness≤60 afterwards；
(3), reduce rotating speed to 1200r/min stirrings under sequentially add 23 parts of emulsions, 1.5 parts of coalescents, 1.5 parts
Antifreezing agent, 0.2 part of sterilization antiseptic, are sufficiently stirred after 15min and obtain alkali-resistant primer of the present invention.
Emulsion described in said components uses 7623 emulsions of BASF.The water uses ordinary tap water.The hydroxyl second
Base cellulose is using Asia across imperial 250HBR hydroxyethyl celluloses.The water-soluble multifunctional auxiliary agent is multi-functional using Tao Shi AMP-95
Auxiliary agent.The aqueous dispersion uses the DISPEX A40 aqueous dispersions of vapour bar.The aqueous wetting agent is using sea profit 2405
Aqueous wetting agent.The aqueous defoamer uses the CF-246 defoamers of Bu Levin gram Lays.The titanium dioxide joins BLR- using one hundred profit
699 titanium dioxides.The mica powder is using U.S. high mica powder.Talcum powder uses the rich mesh talcum powder of powder 1250 of the rising sun.The carbonic acid
Calcium uses the mesh powdered whiting of agriculture-countryside-farmer 700.The coalescents use Yi Shiman Texanol coalescents.The antifreezing agent
Using the propane diols of Shandong Depew chemical industry.The sterilization antiseptic uses Troy RS sterilization antiseptics.
Embodiment 2：A kind of alkali-resistant primer, is formulated by following components and ratio of weight and number：
The preparation method of above-mentioned alkali-resistant primer, it includes following the step of sequentially carrying out：
(1), 36 parts of water are added in dispersion cylinder, 0.5 part of hydroxy ethyl fiber is sequentially added under 350r/min stirrings
Element and 0.1 part of water-soluble multifunctional auxiliary agent, stir 3min；
(2) rotating speed, is improved to after 800r/min, sequentially adds 0.5 part of aqueous dispersion, 0.1 part of aqueous wetting agent, 0.38
After part aqueous defoamer, 1 part of titanium dioxide, 15 parts of mica powders, 10 parts of talcum powder, 14 parts of calcium carbonate, rotating speed is improved extremely again
1800r/min simultaneously disperses 20min under this rotating speed, and detection is until system fineness≤60 afterwards；
(3), reduce rotating speed to 1000r/min stirrings under sequentially add 20 parts of emulsions, 1.0 parts of coalescents, 1.2 parts
Antifreezing agent, 0.3 part of sterilization antiseptic, are sufficiently stirred after 20min and obtain alkali-resistant primer of the present invention.
Emulsion described in said components uses 7623 emulsions of BASF.The water uses ordinary tap water.The hydroxyl second
Base cellulose is using Asia across imperial 250HBR hydroxyethyl celluloses.The water-soluble multifunctional auxiliary agent is multi-functional using Tao Shi AMP-95
Auxiliary agent.The aqueous dispersion uses the DISPEX A40 aqueous dispersions of vapour bar.The aqueous wetting agent is using sea profit 2405
Aqueous wetting agent.The aqueous defoamer uses extra large river A10 defoamers.The titanium dioxide joins BLR-699 titanium dioxides using one hundred profit.
The mica powder is using U.S. high mica powder.Talcum powder uses the rich mesh talcum powder of powder 1250 of the rising sun.The calcium carbonate uses agriculture-countryside-farmer
700 mesh powdered whitings.The coalescents use Yi Shiman Texanol coalescents.The antifreezing agent uses Shandong moral
The propane diols of general chemical industry.The sterilization antiseptic uses Troy RS sterilization antiseptics.
Embodiment 3：A kind of alkali-resistant primer, is formulated by following components and ratio of weight and number：
The preparation method of above-mentioned alkali-resistant primer, it includes following the step of sequentially carrying out：
(1), 29 parts of water are added in dispersion cylinder, 0.55 part of hydroxy ethyl fiber is sequentially added under 500r/min stirrings
Element and 0.15 part of water-soluble multifunctional auxiliary agent, stir 2min；
(2) rotating speed, is improved to after 900r/min, sequentially adds 0.7 part of aqueous dispersion, 0.2 part of aqueous wetting agent, 0.4
After part aqueous defoamer, 10 parts of titanium dioxides, 10 parts of mica powders, 5 parts of talcum powder, 15 parts of calcium carbonate, rotating speed is improved extremely again
1900r/min simultaneously disperses 16min under this rotating speed, and detection is until system fineness≤60 afterwards；
(3), reduce rotating speed to 1100r/min stirrings under sequentially add 25 parts of emulsions, 1.5 parts of coalescents, 1.4 parts
Antifreezing agent, 0.25 part of sterilization antiseptic, alkali-resistant primer of the present invention is obtained after being sufficiently stirred 1,8min.
Emulsion described in said components uses 7623 emulsions of BASF.The water uses ordinary tap water.The hydroxyl second
Base cellulose is using Asia across imperial 250HBR hydroxyethyl celluloses.The water-soluble multifunctional auxiliary agent is multi-functional using Tao Shi AMP-95
Auxiliary agent.The aqueous dispersion uses the DISPEX A40 aqueous dispersions of vapour bar.The aqueous wetting agent is using sea profit 2405
Aqueous wetting agent.The aqueous defoamer uses the CF-246 defoamers of Bu Levin gram Lays.The titanium dioxide joins BLR- using one hundred profit
699 titanium dioxides.The mica powder is using U.S. high mica powder.Talcum powder uses the rich mesh talcum powder of powder 1250 of the rising sun.The carbonic acid
Calcium uses the mesh powdered whiting of agriculture-countryside-farmer 700.The coalescents use Yi Shiman Texanol coalescents.The antifreezing agent
Using the propane diols of Shandong Depew chemical industry.The sterilization antiseptic uses Troy RS sterilization antiseptics.
Embodiment 4：A kind of alkali-resistant primer, is formulated by following components and ratio of weight and number：
The preparation method of above-mentioned alkali-resistant primer, it includes following the step of sequentially carrying out：
(1), 35.5 parts of water are added in dispersion cylinder, 0.55 part of ethoxy fibre is sequentially added under 450r/min stirrings
Dimension element and 0.15 part of water-soluble multifunctional auxiliary agent, stir 3min；
(2), improve rotating speed to after 1000r/min, sequentially add 0.6 part of aqueous dispersion, 0.15 part of aqueous wetting agent,
After 0.35 part of aqueous defoamer, 7 parts of titanium dioxides, 15 parts of mica powders, 8 parts of talcum powder, 10 parts of calcium carbonate, rotating speed is improved extremely again
1800r/min simultaneously disperses 20min under this rotating speed, and detection is until system fineness≤60 afterwards；
(3), reduce rotating speed to 1200r/min stirrings under sequentially add 23 parts of emulsions, 1.5 parts of coalescents, 1.5 parts
Antifreezing agent, 0.2 part of sterilization antiseptic, are sufficiently stirred after 15min and obtain alkali-resistant primer of the present invention.
Emulsion described in said components uses 7623 emulsions of BASF.The water uses ordinary tap water.The hydroxyl second
Base cellulose is using Asia across imperial 250HBR hydroxyethyl celluloses.The water-soluble multifunctional auxiliary agent is multi-functional using Tao Shi AMP-95
Auxiliary agent.The aqueous dispersion uses the DISPEX A40 aqueous dispersions of vapour bar.The aqueous wetting agent is using sea profit 2405
Aqueous wetting agent.The aqueous defoamer uses extra large river A10 defoamers.The titanium dioxide joins BLR-699 titanium dioxides using one hundred profit.
The mica powder is using U.S. high mica powder.Talcum powder uses the rich mesh talcum powder of powder 1250 of the rising sun.The calcium carbonate uses agriculture-countryside-farmer
700 mesh powdered whitings.The coalescents use Yi Shiman Texanol coalescents.The antifreezing agent uses Shandong moral
The propane diols of general chemical industry.The sterilization antiseptic uses Troy RS sterilization antiseptics.
By the test to each embodiment, the every technical performance index and experimental data of alkali-resistant primer of the present invention are each as follows
Shown in table：Examination criteria：JG/T210-2007《Primer for interior and exterior wall》Exterior wall base paint I standards；HJ2537-2014《Environment mark
Will product technology requires water paint》Exterior coating priming paint limits of harmful substances standard.
From above-mentioned table it will be evident that above-described embodiment 1- embodiments 4 after tested, embodiment 1- embodiments 4
Alkali-resistant primer not only has alkali resistant effect, but also has sealing process, can effectively prevent the wall accumulation of salt in the surface soil；Its environmental protection index also can
Pass through HJ2537-2014《Environmental labelling product technical requirements water paint》Exterior coating priming paint limits of harmful substances standard.
Simply technical scheme is explained in detail for above-mentioned embodiment, the present invention not only only office
It is limited to above-described embodiment, every any improvement or replacement according to the principle of the invention all should be within protection scope of the present invention.
Claims (2)
1. a kind of alkali-resistant primer, it is characterised in that be formulated by following components and ratio of weight and number：
The emulsion is butadiene-styrene copolymer emulsion；
The hydroxyethyl cellulose is the water dissolvable cellulose ether of nonionic；
The aqueous dispersion is the acrylate copolymer ammonia salt aqueous solution；The aqueous wetting agent moistens for environment-friendly type non-ionic emulsifier
Humectant；
The aqueous defoamer is nonionic defoamer, molecular antifoaming agent or mineral oil antifoam agent or organic silicon defoamer；
The titanium dioxide is anatase thpe white powder or rutile type titanium white；
The mica powder is that proportion is 2.8-2.9g/cm3, oil absorption be 40-70 white powder mica powder；The calcium carbonate is
Powdered whiting；
The emulsion is solid containing being 51 ± 1.0%, and pH value 7.0-9.0, viscosity is 50-300mPa.S milky white liquid；
The coalescents are that purity is more than 98.5%, and acidity is less than 0.05, proportion 0.945-0.955g/ml, and moisture content is small
In 0.1%, limpid clean coalescents liquid that index of refraction is 1.4411-1.4433；
The antifreezing agent is 1,2-PD；
The sterilization antiseptic is isothiazolinone disinfecting agent.
A kind of 2. preparation method of the alkali-resistant primer described in claim 1, it is characterised in that：It includes following sequentially carrying out
Step：
(1), 29-36 parts water is added in dispersion cylinder, 0.5-0.6 part hydroxyl second is sequentially added under 350-550r/min stirrings
Base cellulose and 0.1-0.2 part water-soluble multifunctional auxiliary agents, stir 1min-3min；
(2) rotating speed, is improved to after 800-1000r/min, sequentially adds 0.5-0.7 parts aqueous dispersion, the water-based profit of 0.1-0.2 parts
Humectant, 0.35-0.4 parts aqueous defoamer, 1-10 parts titanium dioxide, 10-15 parts mica powder, 5-10 parts talcum powder, 10-15 part carbonic acid
After calcium, rotating speed is improved again and disperses 15min-20min to 1800-2000r/min and under this rotating speed, detection is until system afterwards
Fineness≤60；
(3), reduce under rotating speed to 1000-1200r/min stirrings and sequentially add 20-25 parts emulsion, 1.0-1.5 part film forming helps
Agent, 1.2-1.5 parts antifreezing agent, 0.2-0.3 part sterilization antiseptics, alkali-resistant primer is obtained after being sufficiently stirred 15-20min.
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| CN109880448A (en) * | 2019-03-14 | 2019-06-14 | 赵雪亮 | Novel anti-stick patch black backing varnish of one kind and preparation method thereof |
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| CN105295595A (en) * | 2015-11-20 | 2016-02-03 | 天津美士邦涂料化工有限公司 | Environmentally-friendly alkali-resistant coating |
| CN105295577A (en) * | 2015-11-25 | 2016-02-03 | 广东嘉宝莉科技材料有限公司 | Antirust alkali-proof interior wall priming paint with high sealing property and preparation method thereof |
| CN105505017A (en) * | 2015-11-26 | 2016-04-20 | 王学素 | Exterior wall osmol waterproof material |
| CN106147459A (en) * | 2016-08-31 | 2016-11-23 | 常熟市优德爱涂料有限公司 | A kind of aqueous low permeability rate priming paint and preparation method thereof |
| CN107022284A (en) * | 2017-05-25 | 2017-08-08 | 滕晓明 | A kind of alkali-resistant paint |
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| CN110655836A (en) * | 2019-10-29 | 2020-01-07 | 西洞庭凯兴建材有限公司 | Alkali-resistant primer and preparation method thereof |
| CN112778875A (en) * | 2020-12-31 | 2021-05-11 | 滁州圣好材料科技有限公司 | Water-based alkali-resistant primer for exterior wall and manufacturing method thereof |
| CN117327414A (en) * | 2023-09-28 | 2024-01-02 | 共享新材料(山东)有限公司 | Quick-drying water-based paint and production method thereof |
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