CN104592008B - 一种dl-苹果酸氢钠的制备方法 - Google Patents
一种dl-苹果酸氢钠的制备方法 Download PDFInfo
- Publication number
- CN104592008B CN104592008B CN201510001761.3A CN201510001761A CN104592008B CN 104592008 B CN104592008 B CN 104592008B CN 201510001761 A CN201510001761 A CN 201510001761A CN 104592008 B CN104592008 B CN 104592008B
- Authority
- CN
- China
- Prior art keywords
- malic acid
- hydrogen sodium
- acid hydrogen
- preparation
- sodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- BJEPYKJPYRNKOW-UHFFFAOYSA-N malic acid Chemical compound OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 title claims abstract description 40
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 title claims abstract description 32
- 229910052708 sodium Inorganic materials 0.000 title claims abstract description 32
- 239000011734 sodium Substances 0.000 title claims abstract description 32
- 229910052739 hydrogen Inorganic materials 0.000 title claims abstract description 21
- 239000001257 hydrogen Substances 0.000 title claims abstract description 21
- 125000004435 hydrogen atom Chemical class [H]* 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000013078 crystal Substances 0.000 claims abstract description 11
- 239000007787 solid Substances 0.000 claims abstract description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 7
- 230000036571 hydration Effects 0.000 claims abstract description 7
- 238000006703 hydration reaction Methods 0.000 claims abstract description 7
- 238000006243 chemical reaction Methods 0.000 claims abstract description 6
- 239000002904 solvent Substances 0.000 claims abstract description 3
- 238000001291 vacuum drying Methods 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 2
- CBVOCNWSAAUNIY-UHFFFAOYSA-N 2-hydroxybutanedioic acid;sodium Chemical compound [Na].[Na].OC(=O)C(O)CC(O)=O CBVOCNWSAAUNIY-UHFFFAOYSA-N 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 6
- ODIGIKRIUKFKHP-UHFFFAOYSA-N (n-propan-2-yloxycarbonylanilino) acetate Chemical compound CC(C)OC(=O)N(OC(C)=O)C1=CC=CC=C1 ODIGIKRIUKFKHP-UHFFFAOYSA-N 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 239000000843 powder Substances 0.000 description 8
- 239000004570 mortar (masonry) Substances 0.000 description 4
- 235000013305 food Nutrition 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 206010020772 Hypertension Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003130 cardiopathic effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 208000017169 kidney disease Diseases 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510001761.3A CN104592008B (zh) | 2015-01-04 | 2015-01-04 | 一种dl-苹果酸氢钠的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510001761.3A CN104592008B (zh) | 2015-01-04 | 2015-01-04 | 一种dl-苹果酸氢钠的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104592008A CN104592008A (zh) | 2015-05-06 |
CN104592008B true CN104592008B (zh) | 2016-06-15 |
Family
ID=53118118
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510001761.3A Active CN104592008B (zh) | 2015-01-04 | 2015-01-04 | 一种dl-苹果酸氢钠的制备方法 |
Country Status (1)
Country | Link |
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CN (1) | CN104592008B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2020260194A1 (en) * | 2019-06-26 | 2020-12-30 | Purac Biochem B.V. | Particulate composition containing co-crystal of malic acid and alkali metal hydrogen malate |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5084524A (zh) * | 1973-12-07 | 1975-07-08 | ||
JPS61161239A (ja) * | 1985-01-11 | 1986-07-21 | Taiyo Kagaku Kogyo Kk | dl−リンゴ酸ジナトリウム水和物の製造方法 |
JPH0584524A (ja) * | 1991-09-27 | 1993-04-06 | Furukawa Alum Co Ltd | 絞りしごき缶の製造方法 |
CN101717332B (zh) * | 2009-11-26 | 2012-11-07 | 广东光华化学厂有限公司 | 一种电子级高纯dl-苹果酸的精制方法 |
CN103601631A (zh) * | 2013-12-06 | 2014-02-26 | 湖北神舟化工有限公司 | 饲料添加剂丁酸钠的制备方法 |
-
2015
- 2015-01-04 CN CN201510001761.3A patent/CN104592008B/zh active Active
Also Published As
Publication number | Publication date |
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CN104592008A (zh) | 2015-05-06 |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method of DL-sodium hydrogen malate Effective date of registration: 20190821 Granted publication date: 20160615 Pledgee: Bengbu Industrial Guidance Fund Co.,Ltd. Pledgor: ANHUI SEALONG BIOTECHNOLOGY Co.,Ltd. Registration number: Y2019340000021 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20220823 Granted publication date: 20160615 Pledgee: Bengbu Industrial Guidance Fund Co.,Ltd. Pledgor: ANHUI SEALONG BIOTECHNOLOGY Co.,Ltd. Registration number: Y2019340000021 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method of DL sodium hydrogen malate Effective date of registration: 20231228 Granted publication date: 20160615 Pledgee: Bengbu Branch of China Postal Savings Bank Co.,Ltd. Pledgor: ANHUI SEALONG BIOTECHNOLOGY Co.,Ltd. Registration number: Y2023980075323 |