CN104562785A - Method for cold dyeing of modified soybean protease fiber fabric - Google Patents
Method for cold dyeing of modified soybean protease fiber fabric Download PDFInfo
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- CN104562785A CN104562785A CN201510078074.1A CN201510078074A CN104562785A CN 104562785 A CN104562785 A CN 104562785A CN 201510078074 A CN201510078074 A CN 201510078074A CN 104562785 A CN104562785 A CN 104562785A
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- dyeing
- fiber fabric
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- treatment
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- 239000000835 fiber Substances 0.000 title claims abstract description 38
- 238000000034 method Methods 0.000 title claims abstract description 31
- 239000004744 fabric Substances 0.000 title claims abstract description 30
- 238000004043 dyeing Methods 0.000 title claims abstract description 23
- 235000010469 Glycine max Nutrition 0.000 title claims abstract description 21
- 244000068988 Glycine max Species 0.000 title claims abstract description 21
- 108091005804 Peptidases Proteins 0.000 title abstract 5
- 239000004365 Protease Substances 0.000 title abstract 5
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 title abstract 5
- 239000007788 liquid Substances 0.000 claims abstract description 19
- 230000008569 process Effects 0.000 claims abstract description 19
- 238000001035 drying Methods 0.000 claims abstract description 17
- 238000002203 pretreatment Methods 0.000 claims abstract description 17
- 230000004048 modification Effects 0.000 claims abstract description 14
- 238000012986 modification Methods 0.000 claims abstract description 14
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims description 14
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 108010073771 Soybean Proteins Proteins 0.000 claims description 9
- 235000019710 soybean protein Nutrition 0.000 claims description 9
- CCJAYIGMMRQRAO-UHFFFAOYSA-N 2-[4-[(2-hydroxyphenyl)methylideneamino]butyliminomethyl]phenol Chemical compound OC1=CC=CC=C1C=NCCCCN=CC1=CC=CC=C1O CCJAYIGMMRQRAO-UHFFFAOYSA-N 0.000 claims description 7
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 7
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 7
- 239000004202 carbamide Substances 0.000 claims description 7
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 7
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 7
- 238000004045 reactive dyeing Methods 0.000 claims description 5
- 239000000344 soap Substances 0.000 claims description 5
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 2
- 235000002906 tartaric acid Nutrition 0.000 claims description 2
- 239000011975 tartaric acid Substances 0.000 claims description 2
- 238000005096 rolling process Methods 0.000 abstract 2
- 238000007598 dipping method Methods 0.000 abstract 1
- 238000010409 ironing Methods 0.000 abstract 1
- 238000010025 steaming Methods 0.000 abstract 1
- 239000000975 dye Substances 0.000 description 24
- 238000002386 leaching Methods 0.000 description 4
- 235000018102 proteins Nutrition 0.000 description 4
- 108090000623 proteins and genes Proteins 0.000 description 4
- 102000004169 proteins and genes Human genes 0.000 description 4
- 238000009987 spinning Methods 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000003513 alkali Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229920000793 Azlon Polymers 0.000 description 1
- 206010017389 Frotteurism Diseases 0.000 description 1
- 102000006395 Globulins Human genes 0.000 description 1
- 108010044091 Globulins Proteins 0.000 description 1
- SJEYSFABYSGQBG-UHFFFAOYSA-M Patent blue Chemical compound [Na+].C1=CC(N(CC)CC)=CC=C1C(C=1C(=CC(=CC=1)S([O-])(=O)=O)S([O-])(=O)=O)=C1C=CC(=[N+](CC)CC)C=C1 SJEYSFABYSGQBG-UHFFFAOYSA-M 0.000 description 1
- 235000019764 Soybean Meal Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000980 acid dye Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000002260 anti-inflammatory agent Substances 0.000 description 1
- 230000001741 anti-phlogistic effect Effects 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000000985 reactive dye Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 239000004455 soybean meal Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 1
- 208000021021 weak cry Diseases 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
- 238000002166 wet spinning Methods 0.000 description 1
Abstract
The invention relates to a method for cold dyeing of a modified soybean protease fiber fabric. The method comprises the following steps: (1) preparing a modified finishing liquid; (2) carrying out grafting treatment: carrying out pre-treatment on the soybean protease fiber fabric; dipping and rolling twice; drying; baking for 8 minutes at 150 DEG C, wherein the use level of the modified finishing liquid is 5% (owf.) and the bath ratio is 1: (10-30); and (3) dyeing by an active dye after modification: namely dyeing the modified soybean protease fiber fabric prepared in the step 2, wherein the dyeing process flow comprises the following steps: pre-treatment of a gray fabric; padding of dye liquor; rolling and piling; squeezing and drying; printing; steaming; soaping; ironing; and batching; the padding temperature is room temperature, the vehicle speed is 20-40 meter/minute and the piling time is 2-4 hours. The soybean protease fiber fabric treated by the invention is good in dyeing effect, high in fiber strength, and not late to fade, and the finished product is high in surface smoothness, attractive and durable. The method provided by the invention is simple in process, low in cost and easy to operate.
Description
Technical field
The present invention relates to field of fabric producing technology, particularly fabric-modifying dyeing.
Background technology
Soybean fiber is a kind of azlon, isolate globulin from the Soybean Meal pressed the oil, through linearization process, with polyhydroxy polymer Graft copolymerisation, blended, make protein spinning solution, through the fiber of wet spinning, there is excellent wet guilding, gas permeability, and soft smooth, drapability good, has many advantages of chemical fibre and natural fabric concurrently.Soybean fiber, in spinning process, adds people's bactericidal antiphlogistic class medicine or ultra-violet absorber etc., can obtain various health care.But soybean fiber heat resistance is poor, and not resistance to caustic soda, protein fibre highly basic or weak cry out in all can be subject in various degree infringement, even cause decomposing.The fastness of acid dyeing is very poor, albumen is in separation, purifying and spinning process process, suffer obvious damage. the amino negligible amounts in amino acid composition, therefore the ability of combination dye reduces greatly, again because the protein of this fiber is mainly distributed in fibrous outer, negligible amounts, and easily swellingly to come off, even if so the upper a large amount of ACID DYES of absorption, dyestuff is also easy to come off under damp and hot and Frotteurism with protein, and color is not bright-coloured yet.In addition, we prove, quite a few dyestuff is also adsorbed in the cellulose composition of fiber internal layer, but fastness is very poor, low in glossiness.More easily fade under Ultraviolet radiation.
This project is carried out modified to soybean protein fibre, have employed the production technology of low temperature dyeing after first graft modification.Add REACTIVE DYES, the COLOR FASTNESS overcoming common process be poor, the shortcoming of low in glossiness, eliminate the rear technique in former fabrication processes, to spinning material, very favourable to environmental protection.
Modified soybean protein fibres of the present invention overcomes soybean protein fibre heat resistance, alkali resistance difference and achromatic problem.
Summary of the invention
For above-mentioned defect, the object of the invention is to, provide the method for the modified cold dyeing look of a kind of soybean fiber fabric, modified fiber is because of the reaction of a large amount of ion, fiber surface electric charge is changed, thus the heat resistance of azelon, alkali resistance and dyeability are made moderate progress.
For achieving the above object, technical scheme of the present invention is the method for the modified cold dyeing look of a kind of soybean fiber fabric:
(1) modification liquid (with parts by weight) is prepared:
N hydroxymethyl acrylamide 50-70
Triethanolamine 60-90
Methyl acrylate 6-8
ZnCl
2 10-15
Water 100-150;
(2) grafting process: soybean fiber fabric → bis-leaching two through pre-treatment is rolled → dried →
Bake about 8min at 150 DEG C, wherein, the consumption of modification liquid is 5%(owf.), bath raio 1:10-30;
(3) modified reactive dyeing: modified soy-bean protein fiber step 2 prepared dyes, its dye liquor technical recipe following (in grams per liter):
Activated red X-3B 10-15
Urea 25-30
Reservehao S 10-12
Sodium bicarbonate 15-20
Water 80-100;
The technological process of described dyeing is grey cloth pre-treatment → pad dye liquor → roll volume to bank up → squezzing drying → stamp → evaporate → soap → dry → clot; Wherein, after grey cloth pre-treatment, liquid carrying rate is 70-75%, and even end to end, and after dye, pick-up is 90-95%; Padding temperature is room temperature; The speed of a motor vehicle is 20-40 m/min, and the time of banking up is 2-4h; When padding dye liquor, nip pressure is air pressure 147KPa, oil pressure 118KPa; Drying steam pressure is 49-147KPa, and each drying cylinder is gradually high successively.
Preferably, the consisting of (with parts by weight) of described modification liquid:
N hydroxymethyl acrylamide 60 parts,
Triethanolamine 75 parts,
Methyl acrylate 7 parts,
ZnCl
212.5 part,
125 parts, water.
Preferably, its dye liquor technical recipe following (in grams per liter):
Activated red X-3B 12
Urea 28
Reservehao S 11
Sodium bicarbonate 17
Water 90
Preferably, tartaric acid adjust ph is used during described dyeing.
The invention has the advantages that the soybean protein fibre with process of the present invention, Color is good, and fibre strength is high, not lately fades, and finished surface is highly polished, more attractive and durable.Present invention process is simple, with low cost, easy to operate, has higher promotional value.
Detailed description of the invention
Below by embodiment, technical scheme of the present invention is described in further detail.
Embodiment one:
(1) modification liquid (with parts by weight) is prepared:
N hydroxymethyl acrylamide 50
Triethanolamine 60
Methyl acrylate 6
ZnCl
2 10
Water 100;
(2) grafting process: soybean fiber fabric → bis-leaching two through pre-treatment is rolled → dried →
Bake 8min at 150 DEG C, wherein, the consumption of modification liquid is 5%(owf.), bath raio 1:10;
(3) modified reactive dyeing: modified soy-bean protein fiber step 2 prepared dyes, its dye liquor technical recipe following (in grams per liter):
Activated red X-3B 10
Urea 25
Reservehao S 10
Sodium bicarbonate 15
Water 80;
The technological process of described dyeing is grey cloth pre-treatment → pad dye liquor → roll volume to bank up → squezzing drying → stamp → evaporate → soap → dry → clot; Wherein, after grey cloth pre-treatment, liquid carrying rate is 70%, and even end to end, and after dye, pick-up is 90%; Padding temperature is room temperature; The speed of a motor vehicle is 20 ms/min, and the time of banking up is 2h; When padding dye liquor, nip pressure is air pressure 147KPa, oil pressure 118KPa; Drying steam pressure is 49KPa, and each drying cylinder is gradually high successively.
Embodiment two:
(1) modification liquid (with parts by weight) is prepared:
N hydroxymethyl acrylamide 70
Triethanolamine 90
Methyl acrylate 8
ZnCl
2 15
Water 150;
(2) grafting process: soybean fiber fabric → bis-leaching two through pre-treatment is rolled → dried →
Bake 8min at 150 DEG C, wherein, the consumption of modification liquid is 5%(owf.), bath raio 1:30;
(3) modified reactive dyeing: modified soy-bean protein fiber step 2 prepared dyes, its dye liquor technical recipe following (in grams per liter):
Activated red X-3B 15
Urea 30
Reservehao S 12
Sodium bicarbonate 20
Water 100;
The technological process of described dyeing is grey cloth pre-treatment → pad dye liquor → roll volume to bank up → squezzing drying → stamp → evaporate → soap → dry → clot; Wherein, after grey cloth pre-treatment, liquid carrying rate is 75%, and even end to end, and after dye, pick-up is 95%; Padding temperature is room temperature; The speed of a motor vehicle is 40 ms/min, and the time of banking up is 4h; When padding dye liquor, nip pressure is air pressure 147KPa, oil pressure 118KPa; Drying steam pressure is 147KPa, and each drying cylinder is gradually high successively.
Embodiment three:
(1) modification liquid (with parts by weight) is prepared:
N hydroxymethyl acrylamide 60
Triethanolamine 75
Methyl acrylate 7
ZnCl
2 12.5
Water 125;
(2) grafting process: soybean fiber fabric → bis-leaching two through pre-treatment is rolled → dried →
Bake 8min at 150 DEG C, wherein, the consumption of modification liquid is 5%(owf.), bath raio 1:20;
(3) modified reactive dyeing: modified soy-bean protein fiber step 2 prepared dyes, its dye liquor technical recipe following (in grams per liter):
Activated red X-3B 12
Urea 28
Reservehao S 11
Sodium bicarbonate 17
Water 90;
The technological process of described dyeing is grey cloth pre-treatment → pad dye liquor → roll volume to bank up → squezzing drying → stamp → evaporate → soap → dry → clot; Wherein, after grey cloth pre-treatment, liquid carrying rate is 73%, and even end to end, and after dye, pick-up is 92%; Padding temperature is room temperature; The speed of a motor vehicle is 30 ms/min, and the time of banking up is 2-4h; When padding dye liquor, nip pressure is air pressure 147KPa, oil pressure 118KPa; Drying steam pressure is 100KPa, and each drying cylinder is gradually high successively.
By the soybean fiber after above embodiment process, the product color after weaving is bright-coloured and not easily fade, and product quality can significantly improve by the time.
The above; be only the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the technical scope disclosed by the present invention; the change can expected without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, the protection domain that protection scope of the present invention should limit with claims is as the criterion.
Claims (4)
1. a method for the modified cold dyeing look of soybean fiber fabric, is characterized in that:
(1) modification liquid (with parts by weight) is prepared:
N hydroxymethyl acrylamide 50-70
Triethanolamine 60-90
Methyl acrylate 6-8
ZnCl
2 10-15
Water 100-150;
(2) grafting process: soybean fiber fabric → bis-through pre-treatment are soaked two roll → dry → 150 DEG C at bake about 8min, wherein, the consumption of modification liquid is 5%(owf.), bath raio 1:10-30;
(3) modified reactive dyeing: modified soy-bean protein fiber prepared by step (2) is dyeed, its dye liquor technical recipe following (in grams per liter):
Activated red X-3B 10-15
Urea 25-30
Reservehao S 10-12
Sodium bicarbonate 15-20
Water 80-100;
The technological process of described dyeing is grey cloth pre-treatment → pad dye liquor → roll volume to bank up → squezzing drying → stamp → evaporate → soap → dry → clot etc.; Wherein, after grey cloth pre-treatment, liquid carrying rate is 70-75%, and even end to end, and after dye, pick-up is 90-95%; Padding temperature is room temperature; The speed of a motor vehicle is 20-40 m/min, and the time of banking up is 2-4h; When padding dye liquor, nip pressure is air pressure 147KPa, oil pressure 118KPa; Drying steam pressure is 49-147KPa, and each drying cylinder is gradually high successively.
2. the method for the modified cold dyeing look of soybean fiber fabric according to claim 1, is characterized in that: consisting of (with parts by weight) of described modification liquid:
N hydroxymethyl acrylamide 80 parts
Triethanolamine 75 parts
Methyl acrylate 7 parts
ZnCl
212.5 parts
125 parts, water.
3. the method for the modified cold dyeing look of soybean fiber fabric according to claim 1, is characterized in that: its dye liquor technical recipe following (in grams per liter):
Activated red X-3B 12
Urea 28
Reservehao S 11
Sodium bicarbonate 17
Water 90.
4. the method for the modified cold dyeing look of soybean fiber fabric according to claim 1, its feature: use tartaric acid adjust ph during described dyeing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510078074.1A CN104562785B (en) | 2015-02-14 | 2015-02-14 | The method of the modified cold dyeing look of a kind of soybean fiber fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510078074.1A CN104562785B (en) | 2015-02-14 | 2015-02-14 | The method of the modified cold dyeing look of a kind of soybean fiber fabric |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104562785A true CN104562785A (en) | 2015-04-29 |
| CN104562785B CN104562785B (en) | 2015-11-11 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510078074.1A Expired - Fee Related CN104562785B (en) | 2015-02-14 | 2015-02-14 | The method of the modified cold dyeing look of a kind of soybean fiber fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104562785B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105297174A (en) * | 2015-11-16 | 2016-02-03 | 安徽绿朋实业有限公司 | Soybean protein fiber and production technology |
| CN107558259A (en) * | 2017-09-29 | 2018-01-09 | 张新文 | Fiber treatment modifying agent and its method of modifying |
| CN107700245A (en) * | 2017-09-29 | 2018-02-16 | 张新文 | The online modified technique of fiber |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1804206A (en) * | 2005-12-13 | 2006-07-19 | 苏州大学 | One-bath dyeing method for soybean fiber/tencel blended fabric |
| CN101070676A (en) * | 2007-05-18 | 2007-11-14 | 广东德美精细化工股份有限公司 | Fiber-material modifying method and dyeing process |
| CN102134806A (en) * | 2011-04-27 | 2011-07-27 | 广州湘中纺织助剂有限公司 | Salt-free rolling, baking, dying and low-temperature soaping method for fiber reactive dyes |
-
2015
- 2015-02-14 CN CN201510078074.1A patent/CN104562785B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1804206A (en) * | 2005-12-13 | 2006-07-19 | 苏州大学 | One-bath dyeing method for soybean fiber/tencel blended fabric |
| CN101070676A (en) * | 2007-05-18 | 2007-11-14 | 广东德美精细化工股份有限公司 | Fiber-material modifying method and dyeing process |
| CN102134806A (en) * | 2011-04-27 | 2011-07-27 | 广州湘中纺织助剂有限公司 | Salt-free rolling, baking, dying and low-temperature soaping method for fiber reactive dyes |
Non-Patent Citations (1)
| Title |
|---|
| 黄晨等: "蚕丝织物辐射接枝丙烯酰胺的改性", 《纺织学报》, vol. 29, no. 03, 15 March 2008 (2008-03-15) * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105297174A (en) * | 2015-11-16 | 2016-02-03 | 安徽绿朋实业有限公司 | Soybean protein fiber and production technology |
| CN107558259A (en) * | 2017-09-29 | 2018-01-09 | 张新文 | Fiber treatment modifying agent and its method of modifying |
| CN107700245A (en) * | 2017-09-29 | 2018-02-16 | 张新文 | The online modified technique of fiber |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104562785B (en) | 2015-11-11 |
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Effective date of registration: 20151014 Address after: 311800 Zhejiang city in Shaoxing Province, Zhuji City, East Street and East Road No. 469 Applicant after: Li Hailan Address before: 311805 Zhejiang city of Shaoxing province Zhuji city Zhoucun Town, No. 185 Jieting Applicant before: Ye Cheng |
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Effective date of registration: 20170612 Address after: 528425 Guangdong Province, Zhongshan City Dongsheng Town 7 Siu Yick Road No. 112 card Patentee after: Zhongshan liquid Cotton Textile Co.,Ltd. Address before: 311800 Zhejiang city in Shaoxing Province, Zhuji City, East Street and East Road No. 469 Patentee before: Li Hailan |
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