CN104559670A - Water-based high-temperature-resistant antirust paint and preparation method thereof - Google Patents
Water-based high-temperature-resistant antirust paint and preparation method thereof Download PDFInfo
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- CN104559670A CN104559670A CN201510011044.9A CN201510011044A CN104559670A CN 104559670 A CN104559670 A CN 104559670A CN 201510011044 A CN201510011044 A CN 201510011044A CN 104559670 A CN104559670 A CN 104559670A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
- C09D5/10—Anti-corrosive paints containing metal dust
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a water-based high-temperature-resistant antirust paint. The water-based high-temperature-resistant antirust paint is characterized by being prepared from the following raw materials in parts by weight: 1-2 parts of sodium propionate, 2-3 parts of sodium pyrophosphate, 4-6 parts of mica powder, 2-3 parts of propanediol butyl ether, 23-26 parts of styrene-acrylic emulsion, 1-2 parts of 18-alkyl primary amine acetate, 0.3-0.5 part of organic fluoride modified polysiloxane, 1-2 parts of zinc stearate, 2-3 parts of carbonate pickax, 0.3-0.5 part of sodium oleate, 2-3 parts of polyving akohol, 2-3 parts of a water-based curing agent D230, 0.1-0.3 part of polyxyethylated alkylphenol, 33-36 parts of epoxy resin emulsion, 3-4 parts of barite powder, 4-7 parts of talcum powder, 16-22 parts of deionized water and 4-7 parts of an additive. After the paint is solidified, a paint film is high in hardness, good in abrasive resistance, high in adhesive force and not easy to peel off and also has the functions of resisting high temperature and preventing rust. By utilizing the water-based high-temperature-resistant antirust paint, an out door device shell can withstand harsh environment, the service life is prolonged, the added additive has the effect of reducing noise through damping, outflow of noise is weakened, and harmonious living environment is built.
Description
Technical field
The present invention relates to a kind of paint and preparation method thereof, particularly a kind of aqueous high-temperature-resistant rust-inhibiting paint and preparation method thereof.
Background technology
Rust-inhibiting paint is industrial widely used a kind of coating, and its Main Function is to prevent metal be oxidized in life-time service process and get rusty.A large amount of rust-inhibiting paint used is solvent-borne type substantially in the market, but formaldehyde contained in solvent-borne type rust-inhibiting paint, benzene, dimethylbenzene are all poisonous carcinogenic substances, great hidden danger is caused to HUMAN HEALTH, the requirement of people for health environment-friendly can not be met far away.Along with the raising gradually of people's environmental consciousness, people use water to replace organic solvent as thinner gradually.Every coating using water as solvent or make dispersion medium, all can be described as water-borne coatings.Water-borne coatings comprises water soluble paint, water-reducible coatings, water-dispersible paint 3 kinds.Water-borne coatings, with water as solvent, saves ample resources, and fire hazard when water-borne coatings eliminates construction, reduces topsoil; Water-borne coatings only adopts a small amount of hypotoxicity alcohol ether organic solvent, improves operating environmental condition; Water-borne coatings directly can apply construction in wet structure and wet environment; It is good to material surface adaptability, strong adhesion.
Summary of the invention
The object of this invention is to provide a kind of aqueous high-temperature-resistant rust-inhibiting paint and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of aqueous high-temperature-resistant rust-inhibiting paint, is made up of the raw material of following weight part: Sodium Propionate 1-2, trisodium phosphate 2-3, mica powder 4-6, propandiol butyl ether 2-3, benzene emulsion 23-26, octadecyl primary amine acetate 1-2, Organofluoro Modified Polysiloxane 0.3-0.5, Zinic stearas 1-2, carbonic acid pick 2-3, sodium oleate 0.3-0.5, polyvinyl alcohol 2-3, waterborne curing agent D2302-3, polyxyethylated alkylphenol 0.1-0.3, epoxy resin latex 33-36, ground barium sulfate 3-4, talcum powder 4-7, deionized water 16-22, auxiliary agent 4-7;
Described auxiliary agent is made up of the raw material of following weight part: tripoly phosphate sodium STPP 2-4, alkylphenol polyoxyethylene 1-2, polyvinyl alcohol 2-3, urea 6-8, nanometer silver 4-5, titanate coupling agent 1-2, methyl methacrylate 10-15, ethyl propenoate 3-5, Potassium Persulphate 1-2, water 8-11, hollow glass micropearl 6-8, fly ash micro-sphere 4-6, sepiolite powder 3-5,1.2% chitosan-acetic acid solution 3-5, ammonium molybdate 2-4, polyvinyl acetate emulsion 5-8; Preparation method is that methyl methacrylate, ethyl propenoate, polyvinyl acetate emulsion and water mix by (1), passes into fluidized-bed and makes its fluidisation; (2) hollow glass micropearl, fly ash micro-sphere, sepiolite powder and Potassium Persulphate are mixed, passing into fluidized-bed is boiling state; (3) mixture of step (1) is sprayed on the mixture of step (2) on the surface, under 60-80 ° of C, reacts 1-2 hour, add titanate coupling agent again and remaining surplus materials stirs after reaction terminates, then add rubber mill grinding distribution evenly.
A kind of aqueous high-temperature-resistant rust-inhibiting paint of the present invention, be made up of following concrete steps:
(1) sodium oleate, polyxyethylated alkylphenol, octadecyl primary amine acetate, Organofluoro Modified Polysiloxane and deionized water are mixed, 7-9 minute is stirred under 400-600 rev/min, add mica powder, carbonic acid pick, ground barium sulfate, talcum powder, auxiliary agent ultrasonic disperse 15-25 minute again, obtain mixture A;
(2) be added in Scattered Kettle by benzene emulsion, epoxy resin latex, propandiol butyl ether, waterborne curing agent D230,1200-1400 rev/min of lower high-speed mixing stirs 20-40 minute, obtains mixture B;
(3) mixture A is added in mixture B, then adds all the other surplus materialss, disperse 10-20 minute under the rotating speed of 800-1000 rev/min after, forward in shredder, obtain the material of 20-40 μm, to obtain final product.
Advantage of the present invention is: after paint curing of the present invention, hardness of paint film is high, wear resistance good, sticking power is high, incrust, also there is high temperature resistant, antirust function, outdoor apparatus casing can be allowed more to stand rugged environment, increase the service life, and the auxiliary agent added has the effect reducing noise by damping, reduce spreading out of of noise, build harmonious living environment.
specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of aqueous high-temperature-resistant rust-inhibiting paint, is made up of the raw material of following weight part (kilogram): Sodium Propionate 1, trisodium phosphate 2, mica powder 6, propandiol butyl ether 2, benzene emulsion 25, octadecyl primary amine acetate 1, Organofluoro Modified Polysiloxane 0.4, Zinic stearas 2, carbonic acid pick 2, sodium oleate 0.4, polyvinyl alcohol 3, waterborne curing agent D2303, polyxyethylated alkylphenol 0.3, epoxy resin latex 34, ground barium sulfate 4, talcum powder 4, deionized water 19, auxiliary agent 4;
Described auxiliary agent is made up of the raw material of following weight part (kilogram): tripoly phosphate sodium STPP 3, alkylphenol polyoxyethylene 1, polyvinyl alcohol 3, urea 6, nanometer silver 4, titanate coupling agent 2, methyl methacrylate 13, ethyl propenoate 4, Potassium Persulphate 2, water 8, hollow glass micropearl 6, fly ash micro-sphere 5, the chitosan-acetic acid solution 4 of sepiolite powder 3,1.2%, ammonium molybdate 3, polyvinyl acetate emulsion 7; Preparation method is that methyl methacrylate, ethyl propenoate, polyvinyl acetate emulsion and water mix by (1), passes into fluidized-bed and makes its fluidisation; (2) hollow glass micropearl, fly ash micro-sphere, sepiolite powder and Potassium Persulphate are mixed, passing into fluidized-bed is boiling state; (3) mixture of step (1) is sprayed on the mixture of step (2) on the surface, under 60-80 ° of C, reacts 1-2 hour, add titanate coupling agent again and remaining surplus materials stirs after reaction terminates, then add rubber mill grinding distribution evenly.
A kind of aqueous high-temperature-resistant rust-inhibiting paint of the present invention, be made up of following concrete steps:
(1) sodium oleate, polyxyethylated alkylphenol, octadecyl primary amine acetate, Organofluoro Modified Polysiloxane and deionized water are mixed, 7-9 minute is stirred under 400-600 rev/min, add mica powder, carbonic acid pick, ground barium sulfate, talcum powder, auxiliary agent ultrasonic disperse 15-25 minute again, obtain mixture A;
(2) be added in Scattered Kettle by benzene emulsion, epoxy resin latex, propandiol butyl ether, waterborne curing agent D230,1200-1400 rev/min of lower high-speed mixing stirs 20-40 minute, obtains mixture B;
(3) mixture A is added in mixture B, then adds all the other surplus materialss, disperse 10-20 minute under the rotating speed of 800-1000 rev/min after, forward in shredder, obtain the material of 20-40 μm, to obtain final product.
Paint flat appearance of the present invention is smooth, without lump, and snappiness mm≤2, hardness: 4H, shock-resistance: 50, water tolerance experiment (29 ± 1 ° of C, 40h): non-foaming, do not come off, thermotolerance experiment (100 ± 2 DEG C, 5h): non-foaming wrinkling, without cracking, resistance to artificial weathering experiment: by 500 hours, cold-hot is experiment (5 cycle) alternately: without bubbling, without cracking, without coming off, recombination loss Factor Experiment: 10 ° of C:0.098,30 ° of C:0.132.
Claims (2)
1. an aqueous high-temperature-resistant rust-inhibiting paint, it is characterized in that, be made up of the raw material of following weight part: Sodium Propionate 1-2, trisodium phosphate 2-3, mica powder 4-6, propandiol butyl ether 2-3, benzene emulsion 23-26, octadecyl primary amine acetate 1-2, Organofluoro Modified Polysiloxane 0.3-0.5, Zinic stearas 1-2, carbonic acid pick 2-3, sodium oleate 0.3-0.5, polyvinyl alcohol 2-3, waterborne curing agent D2302-3, polyxyethylated alkylphenol 0.1-0.3, epoxy resin latex 33-36, ground barium sulfate 3-4, talcum powder 4-7, deionized water 16-22, auxiliary agent 4-7;
Described auxiliary agent is made up of the raw material of following weight part: tripoly phosphate sodium STPP 2-4, alkylphenol polyoxyethylene 1-2, polyvinyl alcohol 2-3, urea 6-8, nanometer silver 4-5, titanate coupling agent 1-2, methyl methacrylate 10-15, ethyl propenoate 3-5, Potassium Persulphate 1-2, water 8-11, hollow glass micropearl 6-8, fly ash micro-sphere 4-6, sepiolite powder 3-5,1.2% chitosan-acetic acid solution 3-5, ammonium molybdate 2-4, polyvinyl acetate emulsion 5-8; Preparation method is that methyl methacrylate, ethyl propenoate, polyvinyl acetate emulsion and water mix by (1), passes into fluidized-bed and makes its fluidisation; (2) hollow glass micropearl, fly ash micro-sphere, sepiolite powder and Potassium Persulphate are mixed, passing into fluidized-bed is boiling state; (3) mixture of step (1) is sprayed on the mixture of step (2) on the surface, under 60-80 ° of C, reacts 1-2 hour, add titanate coupling agent again and remaining surplus materials stirs after reaction terminates, then add rubber mill grinding distribution evenly.
2. a kind of aqueous high-temperature-resistant rust-inhibiting paint according to claim 1, is characterized in that, be made up of following concrete steps:
(1) sodium oleate, polyxyethylated alkylphenol, octadecyl primary amine acetate, Organofluoro Modified Polysiloxane and deionized water are mixed, 7-9 minute is stirred under 400-600 rev/min, add mica powder, carbonic acid pick, ground barium sulfate, talcum powder, auxiliary agent ultrasonic disperse 15-25 minute again, obtain mixture A;
(2) be added in Scattered Kettle by benzene emulsion, epoxy resin latex, propandiol butyl ether, waterborne curing agent D230,1200-1400 rev/min of lower high-speed mixing stirs 20-40 minute, obtains mixture B;
(3) mixture A is added in mixture B, then adds all the other surplus materialss, disperse 10-20 minute under the rotating speed of 800-1000 rev/min after, forward in shredder, obtain the material of 20-40 μm, to obtain final product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510011044.9A CN104559670A (en) | 2015-01-10 | 2015-01-10 | Water-based high-temperature-resistant antirust paint and preparation method thereof |
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| CN201510011044.9A CN104559670A (en) | 2015-01-10 | 2015-01-10 | Water-based high-temperature-resistant antirust paint and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106046967A (en) * | 2016-07-18 | 2016-10-26 | 天长市巨龙车船涂料有限公司 | Air-dry finishing paint on surface of injection-molding plastic part |
| CN106118275A (en) * | 2016-08-04 | 2016-11-16 | 安徽罗伯特科技股份有限公司 | High-temperature-resisting transformer and preparation method thereof |
| CN106118274A (en) * | 2016-08-04 | 2016-11-16 | 安徽罗伯特科技股份有限公司 | High temperature resistant flat-top cabinet and preparation method thereof |
| CN106118304A (en) * | 2016-07-29 | 2016-11-16 | 蚌埠市佳爱电子有限公司 | A kind of young-generating machine internal layer modification antirust paint |
| CN106243850A (en) * | 2016-08-04 | 2016-12-21 | 安徽罗伯特科技股份有限公司 | High temperature resistant spark gap and preparation method thereof |
| CN106243848A (en) * | 2016-08-04 | 2016-12-21 | 安徽罗伯特科技股份有限公司 | High temperature resistant high-low cabinet and preparation method thereof |
| CN106243849A (en) * | 2016-08-04 | 2016-12-21 | 安徽罗伯特科技股份有限公司 | High temperature resistant earthed switch and preparation method thereof |
| CN107236390A (en) * | 2017-08-01 | 2017-10-10 | 合肥择浚电气设备有限公司 | A kind of antirust coat of high and low voltage electrical equipment cabinet shell and preparation method thereof |
| CN111690309A (en) * | 2020-07-16 | 2020-09-22 | 程浩源 | Normal-temperature curing water-based epoxy resin coating and preparation method thereof |
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2015
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Patent Citations (5)
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| CN1962770A (en) * | 2005-11-10 | 2007-05-16 | 上海兑宸商贸有限公司 | Metal anti-corrosion dewetting agent for use in oily paint |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106046967A (en) * | 2016-07-18 | 2016-10-26 | 天长市巨龙车船涂料有限公司 | Air-dry finishing paint on surface of injection-molding plastic part |
| CN106118304A (en) * | 2016-07-29 | 2016-11-16 | 蚌埠市佳爱电子有限公司 | A kind of young-generating machine internal layer modification antirust paint |
| CN106118275A (en) * | 2016-08-04 | 2016-11-16 | 安徽罗伯特科技股份有限公司 | High-temperature-resisting transformer and preparation method thereof |
| CN106118274A (en) * | 2016-08-04 | 2016-11-16 | 安徽罗伯特科技股份有限公司 | High temperature resistant flat-top cabinet and preparation method thereof |
| CN106243850A (en) * | 2016-08-04 | 2016-12-21 | 安徽罗伯特科技股份有限公司 | High temperature resistant spark gap and preparation method thereof |
| CN106243848A (en) * | 2016-08-04 | 2016-12-21 | 安徽罗伯特科技股份有限公司 | High temperature resistant high-low cabinet and preparation method thereof |
| CN106243849A (en) * | 2016-08-04 | 2016-12-21 | 安徽罗伯特科技股份有限公司 | High temperature resistant earthed switch and preparation method thereof |
| CN107236390A (en) * | 2017-08-01 | 2017-10-10 | 合肥择浚电气设备有限公司 | A kind of antirust coat of high and low voltage electrical equipment cabinet shell and preparation method thereof |
| CN111690309A (en) * | 2020-07-16 | 2020-09-22 | 程浩源 | Normal-temperature curing water-based epoxy resin coating and preparation method thereof |
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Application publication date: 20150429 |