CN104557165B - Special fertilizer for organic cultivation of black Chinese wolfberry and preparation method of fertilizer - Google Patents

Special fertilizer for organic cultivation of black Chinese wolfberry and preparation method of fertilizer Download PDF

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Publication number
CN104557165B
CN104557165B CN201510014800.3A CN201510014800A CN104557165B CN 104557165 B CN104557165 B CN 104557165B CN 201510014800 A CN201510014800 A CN 201510014800A CN 104557165 B CN104557165 B CN 104557165B
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fertilizer
piddock
western
fresh water
dedicated fertilizer
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CN104557165A (en
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冯立田
刘玉民
苏斌
温莉
孙春萍
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Feng Wenze
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Shandong Haishui Vegetable Science And Technology Development Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F11/00Other organic fertilisers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The invention relates to a special fertilizer for organic cultivation of black Chinese wolfberry and a preparation method of the fertilizer. The special fertilizer for organic cultivation of black Chinese wolfberry comprises sea asparagus. The preparation method of the special fertilizer for organic cultivation of black Chinese wolfberry comprises the following steps: (1) cleaning; (2) leaching; (3) washing residues with fresh water; and (4) mixing, concentrating and drying. The fertilizer is produced from sea asparagus as a raw material and meets the requirements on salt and minerals for enabling black Chinese wolfberry to complete the growth history and ensure that black Chinese wolfberry normally flowers and bears fruits. The fertilizer belongs to an organic fertilizer prepared from plants as raw materials; by the fertilizer, the nutrient needs of the black Chinese wolfberry can be met, no harmful substances can be brought, and thus the use of the chemical fertilizer is reduced or eliminated and the organic cultivation of the black Chinese wolfberry is achieved.

Description

A kind of dedicated fertilizer for Lycium ruthenicum Murr. organic farming and preparation method thereof
Technical field
The present invention relates to a kind of dedicated fertilizer for Lycium ruthenicum Murr. organic farming.
Background technology
Lycium ruthenicum Murr. be it is a kind of with important medicines and health protection value economic halophytess, in the last few years, Lycium ruthenicum Murr. it is artificial Cultivation is gradually taken seriously and is constantly promoted.Lycium ruthenicum Murr. belongs to typical halophytess, and so-called halophytess have just referred to The Flora of certain soil salt is needed into history orthobiosiss.
Organic plantation in the last few years is increasingly taken seriously, and the critically important aspect of organic plantation is exactly the use that prevents or limit the quantity Chemical fertilizer or chemical pesticide.In the organic farming practice of Lycium ruthenicum Murr., administration meets the organic of Lycium ruthenicum Murr. growth promoter needs Special fertilizer for cultivating material is critically important premise.
The content of the invention
The technical problem to be solved in the present invention is:A kind of dedicated fertilizer for Lycium ruthenicum Murr. organic farming is provided, is also provided A kind of preparation method of the dedicated fertilizer for Lycium ruthenicum Murr. organic farming.
In order to solve above-mentioned technical problem, dedicated fertilizer of the present invention for Lycium ruthenicum Murr. organic farming includes Western sea Radix Crotalariae szemoensis.Western piddock is a kind of halophytess, and another name salicornia europaeal, Salicornia Bigelovii Torr. etc., are that one kind can be vigorous under the conditions of seawater irrigation The higher plant of growth, salification ability are very powerful, in vivo rich in the various mineral in sea water.
In order to be conducive to the Crop nutrient such as Lycium ruthenicum Murr., dedicated fertilizer of the present invention to be obtained by the following method:Use fresh water The Western piddock of extraction obtains lixiviating solution, and after lixiviating solution is concentrated, re-dry is obtained.
In order that nutrient as much as possible is entered in special fertilizer, dedicated fertilizer of the present invention is obtained by the following method:The party Method comprises the steps:(1)Western piddock is cleaned with sea water or saline that saliferous weight is 2.5-3%;(2)By the west after washing Foreign piddock is extracted with fresh water insulation, and the weight ratio of Western piddock and fresh water is equal to or less than 1:10, extraction temperature 50-80 degree, leaching Put forward time 6-12 hour;(3)The residue that extraction is obtained is cleaned 2-3 time with fresh water, each residue is equal to the weight ratio of fresh water Or it is less than 1:5;(4)Combining step(2)The lixiviating solution for obtaining and step(3)The wash filtrate for obtaining, after reconcentration amalgamation liquid again It is dried prepared dedicated fertilizer.
In order to prevent Western piddock from rotting before extraction, described Western piddock wants dry in the sun to do before cleaning.
In order to improve the holding time of special fertilizer, by obtained dedicated fertilizer vacuum sealed package.
The present invention comprises the steps for the preparation method of the dedicated fertilizer of Lycium ruthenicum Murr. organic farming:(1)By Western sea Radix Crotalariae szemoensis saliferous weight is that the sea water or saline of 2.5-3% are cleaned;(2)Western piddock after washing is extracted with fresh water insulation, the West sea The weight ratio of Radix Crotalariae szemoensis and fresh water is equal to or less than 1:10, extraction temperature 50-80, extraction time 6-12 hours;(3)Extraction is obtained Residue is cleaned 2-3 time with fresh water, and each residue is equal to or less than 1 with the weight ratio of fresh water:5;(4)Combining step(2)Obtain Lixiviating solution and step(3)The wash filtrate for obtaining, after reconcentration amalgamation liquid, re-dry is obtained dedicated fertilizer.
In order to prevent Western piddock from rotting before extraction, described Western piddock be fresh Western piddock or The dry Western piddock of dry in the sun immediately after after harvesting.
In order to improve the holding time of special fertilizer, by obtained dedicated fertilizer vacuum sealed package.
The invention has the beneficial effects as follows:With Western piddock as raw material production, it is complete that fertilizer meets Lycium ruthenicum Murr. to fertilizer of the present invention Into life cycle to salinity and the needs of mineral, it is ensured that Lycium ruthenicum Murr. is normally yielded positive results, fertilizer of the present invention belongs to plant as original The fertilizer of material, can both meet the nutrient demand of Lycium ruthenicum Murr., will not bring harmful substance again, so as to reducing or prevent using chemistry Fertilizer, realizes the organic farming of Lycium ruthenicum Murr..
Specific embodiment
Example one
Western piddock is extracted with fresh water and obtains lixiviating solution, re-dry is obtained for Lycium ruthenicum Murr. organic farming after lixiviating solution is concentrated Dedicated fertilizer.
Example two
Harvesting Herb the West piddock, dry in the sun is done, then Western piddock is cleaned with the sea water that saliferous weight is 3%;(2)To wash Western piddock afterwards is extracted with fresh water insulation, and the weight ratio of Western piddock and fresh water is 1:10,52 degree of extraction temperature, extraction time 12 hours;(3)The residue that extraction is obtained is cleaned with fresh water 2 times, each residue is 1 with the weight ratio of fresh water:6;(4)Merge step Suddenly(2)The lixiviating solution for obtaining and step(3)The wash filtrate for obtaining, after reconcentration amalgamation liquid, re-dry is obtained and has for Lycium ruthenicum Murr. The dedicated fertilizer of machine cultivation.
Example three
The aerial partss of the Western piddock of harvesting, dry in the sun is done, then Western piddock is cleaned with the saline that saliferous weight is 2.5%; (2)Western piddock after washing is extracted with fresh water insulation, and the weight ratio of Western piddock and fresh water is 1:20,80 degree of extraction temperature, Extraction time 6 hours;(3)The residue that extraction is obtained is cleaned with fresh water 3 times, each residue is 1 with the weight ratio of fresh water:10; (4)Combining step(2)The lixiviating solution for obtaining and step(3)The wash filtrate for obtaining, after reconcentration amalgamation liquid, re-dry is obtained and uses In the dedicated fertilizer of Lycium ruthenicum Murr. organic farming.
Example four
The aerial partss of the Western piddock of harvesting are cleaned with the saline that saliferous weight is 2.8%;(2)Western piddock after washing Extracted with fresh water insulation, the weight ratio of Western piddock and fresh water is 1:30,68 degree of extraction temperature, extraction time 9 hours;(3)Will The residue that extraction is obtained is cleaned with fresh water 3 times, and each residue is 1 with the weight ratio of fresh water:20;(4)Combining step(2)Obtain Lixiviating solution and step(3)The wash filtrate for obtaining, after reconcentration amalgamation liquid, re-dry is obtained for the special of Lycium ruthenicum Murr. organic farming With fertilizer, by obtained dedicated fertilizer vacuum sealed package.
Example five
The aerial partss of the Western piddock of harvesting, dry in the sun are done, are then polished into powder, then vacuum sealed package is obtained for black Chinese holly The dedicated fertilizer of Qi organic farming.
In example one, example two, example three and example four, concentration is also adopted by present using current existing Conventional concentration means, drying Existing conventional drying means, such as hot air drying, spray drying or lyophilization.Fertilizer obtained in above-mentioned one-example of example four Good water solubility, can spread fertilizer over the fields, and spread manuer in holes or spray.Obtained in example five, fertilizer can spread fertilizer over the fields or spread manuer in holes.
Test is proved:
Test method, hillside of on the March 15th, 2014 in Jing Cang villages of Tai'an Dongping County east plant 3 years black Chinese hollys of life Qi Seedling, is divided into 7 groups of experimental plots, plants equal number of Lycium ruthenicum Murr. Seedling, sets three repetitions per group, results averaged, first to 5th group of experimental plot sprays above-mentioned five kinds of dedicated fertilizers respectively, and the 6th group of experimental plot sprays common water-soluble chemical compound fertilizer (N:P2O5:K2O5=15:15:15), the 7th group of spray clear water is used as control.Spray from the beginning of 10 days April in 2014, every 15 My god, sprinkling is once.Weight ratio of the spray liquid containing fertilizer is 0.2 %, and each spray liquid total amount in every piece of experimental plot is 32 liters.Spray altogether Spill 6 times.Spraying time fills spray once if running into rainy in six hours after spray at dusk.
On September 30th, 2014, all harvesting is finished Lycium ruthenicum Murr., is carried out index test, is obtained following table data:
Using fertilizer Lycium ruthenicum Murr. yield(Unit:Kg/ mus) Lycium ruthenicum Murr. anthocyanin content (mg/100g) Lycium ruthenicum Murr. potassium content (mg/100g)
1 Example one 135.06 355.26 203.76
2 Example two 140.32 392.25 211.68
3 Example three 145.56 389.92 219.71
4 Example four 149.12 391.01 225.01
5 Example five 130.18 339.67 200.88
6 Water-soluble chemical compound fertilizer 139.34 359.77 224.35
7 Control 115.08 295.96 180.66
Find out from upper table, compared with the control, after applying fertilizer of the present invention, compared with matched group, no matter the yield of Lycium ruthenicum Murr., The content of the effective ingredient anthocyanin of Lycium ruthenicum Murr., or the content of mineral potassium ion is all significantly increased.It is multiple with chemistry is applied Hefei material is compared, and applies example two, example three, example four in addition to mineral potassium content is essentially identical, and applying fertilizer of the present invention can Promote Lycium ruthenicum Murr. yield, the increase of effective ingredient anthocyanin content.Therefore, the present invention can substitute traditional chemistry fertilizer completely Material, so as to meet the needs of Lycium ruthenicum Murr. organic farming.

Claims (6)

1. a kind of dedicated fertilizer for Lycium ruthenicum Murr. organic farming, it is characterised in that:Include Western piddock, by the following method It is obtained:The method comprises the steps:(1)Western piddock is cleaned with sea water or saline that saliferous weight is 2.5-3%;(2)Will Western piddock after washing is extracted with fresh water insulation, and the weight ratio of Western piddock and fresh water is equal to or less than 1:10, extraction temperature 50- 80 degree, extraction time 6-12 hours;(3)The residue that extraction is obtained is cleaned 2-3 time with fresh water, the weight of each residue and fresh water Than equal to or less than 1:5;(4)Combining step(2)The lixiviating solution for obtaining and step(3)The wash filtrate for obtaining, reconcentration merge After liquid, re-dry is obtained dedicated fertilizer.
2. the dedicated fertilizer for Lycium ruthenicum Murr. organic farming according to claim 1, it is characterised in that:Described the West sea Radix Crotalariae szemoensis be fresh Western piddock or after harvesting the dry Western piddock of dry in the sun immediately.
3. the dedicated fertilizer for Lycium ruthenicum Murr. organic farming according to claim 1 and 2, it is characterised in that:Will be obtained Dedicated fertilizer vacuum sealed package.
4. a kind of preparation method of the dedicated fertilizer for Lycium ruthenicum Murr. organic farming, it is characterised in that:Comprise the steps:(1) Western piddock is cleaned with sea water or saline that saliferous weight is 2.5-3%;(2)Western piddock after washing is soaked with fresh water insulation Carry, the weight ratio of Western piddock and fresh water is equal to or less than 1:10, extraction temperature 50-80, extraction time 6-12 hours;(3)Will The residue that extraction is obtained is cleaned 2-3 time with fresh water, and each residue is equal to or less than 1 with the weight ratio of fresh water:5;(4)Combining step (2)The lixiviating solution for obtaining and step(3)The wash filtrate for obtaining, after reconcentration amalgamation liquid, re-dry is obtained dedicated fertilizer.
5. preparation method according to claim 4, it is characterised in that:Described Western piddock be fresh Western piddock or Person is the dry Western piddock of dry in the sun immediately after harvesting.
6. preparation method according to claim 5, it is characterised in that:By obtained dedicated fertilizer vacuum sealed package.
CN201510014800.3A 2015-01-12 2015-01-12 Special fertilizer for organic cultivation of black Chinese wolfberry and preparation method of fertilizer Active CN104557165B (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1594227A (en) * 2003-09-08 2005-03-16 中国科学院南海海洋研究所 Natural organic fertilizer extracted from seaweed and its preparation method
CN101704690A (en) * 2009-10-27 2010-05-12 窦观一 Fertilizer/feed produced by using wind farm and non-grainfield energy plants
CN102160656A (en) * 2011-03-14 2011-08-24 盐城工学院 Comprehensive application method of salicornia bigelovii

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1594227A (en) * 2003-09-08 2005-03-16 中国科学院南海海洋研究所 Natural organic fertilizer extracted from seaweed and its preparation method
CN101704690A (en) * 2009-10-27 2010-05-12 窦观一 Fertilizer/feed produced by using wind farm and non-grainfield energy plants
CN102160656A (en) * 2011-03-14 2011-08-24 盐城工学院 Comprehensive application method of salicornia bigelovii

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
响应曲面法优化海蓬子蛋白质的提取工艺研究;任燕秋;《食品工业》;20121231;第33卷(第11期);21-23 *

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Application publication date: 20150429

Assignee: SHANDONG HUAMUTIANYUAN A & H STOCK Co.,Ltd.

Assignor: SHANDONG SEAWATER VEGETABLE TECHNOLOGY DEVELOPMENT Co.,Ltd.

Contract record no.: X2021980010557

Denomination of invention: The invention relates to a special fertilizer for organic cultivation of black Lycium barbarum and a preparation method thereof

Granted publication date: 20170426

License type: Exclusive License

Record date: 20211012

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Effective date of registration: 20230327

Address after: No. 999, Hucheng Ring Road, Pudong New Area, Shanghai, 200120

Patentee after: Feng Wenze

Address before: Room 611, No. 322, Shunfeng Road, Gaoxin District, Jinan City, Shandong Province, 250000

Patentee before: SHANDONG SEAWATER VEGETABLE TECHNOLOGY DEVELOPMENT Co.,Ltd.