CN104556970A - Ceramic product combining celadon and purple clay and preparation method thereof - Google Patents
Ceramic product combining celadon and purple clay and preparation method thereof Download PDFInfo
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- CN104556970A CN104556970A CN201410198857.9A CN201410198857A CN104556970A CN 104556970 A CN104556970 A CN 104556970A CN 201410198857 A CN201410198857 A CN 201410198857A CN 104556970 A CN104556970 A CN 104556970A
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- celadon
- boccaro
- hour
- heated
- tire
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Abstract
The invention relates to a ceramic product combining celadon and purple clay and a preparation method thereof. The ceramic product is characterized in that the body of the same ceramic product comprises two parts, namely, celadon and purple clay, wherein the celadon body comprises the following components in percentage by weight: 60-74% of SiO2, 18-23% of Al2O3, 0.1-2% of Fe2O3, 0.3-1% of CaO, 0.3-1% of MgO, 1.5-3% of K2O and 0.5-1.5% of Na2O; and the purple clay comprises the following components in percentage by weight: 55-68% of SiO2, 20-30% of Al2O3, 3-7% of Fe2O3, 0.5-1% of CaO, 0.3-1% of MgO, 1-2.5% of K2O and 0.5-1% of Na2O. Celadon glaze is applied on the surface of the celadon body and no glaze is applied on the surface of the purple clay body. By preparing a purple clay pre-form body adapted to the requirements of a celadon firing process, the ceramic product combining celadon and purple clay is provided so as to achieve the perfect combination of celadon and purple clay.
Description
Technical field
The present invention relates to a kind of ceramic, particularly the ceramic that combines with boccaro of a kind of celadon and preparation method.
Background technology
Celadon and boccaro Dou Shi China most traditional characteristics, the ceramic kind be loved by the people.The color of celadon goods is just as thousand peaks in emerald colour, and a Hu Chunshui, shows solemn and quiet and elegant invariably, gentle and beautiful elegance, and it, if ice is like beautiful texture, is world-famous for.Purple-clay product color is antique, primitive simplicity and nature, gives the artistic treat of wonderful workmanship excelling nature, and its tire is moist, good permeability, especially adopts metal and stone painting and calligraphy to engrave the purple-clay product of skill decoration, more shows that it is high-end and atmospheric.Celadon adopts celadon glaze to decorate.Celadon glaze take ferric oxide as tinting material, and adopt reducing atmosphere to burn till, firing temperature is generally at about 1300 DEG C.The ferric oxide that the tinting material of boccaro mainly contains in purple clay, boccaro adopts oxidizing atmosphere to burn till, and firing temperature is generally at about 1150 DEG C.If fired by the firing process of celadon by existing boccaro blank, will produce burning defect, combinations color and lustre is deteriorated, and surface irregularity, does not have ventilation property, loses the original characteristic of purple-clay product.Therefore, prior art still can not produce the characteristic that can reflect celadon on same ceramic, can reflect again the ceramic of boccaro characteristic.
Summary of the invention
The object of the invention is to overcome above-mentioned the deficiencies in the prior art, development adapts to the boccaro blank that celadon reducing atmosphere burns till, ceramic providing a kind of celadon to combine with boccaro and preparation method thereof.
Technical scheme of the present invention is as follows:
The ceramic that celadon combines with boccaro, tire is made up of celadon and boccaro two portions, and according to weight percent, the component content of celadon tire is: SiO260 ~ 74%, Al
2o
318 ~ 23%, Fe
2o
30.1 ~ 2%, CaO0.3 ~ 1%, MgO0.3 ~ 1%, K
2o1.5 ~ 3%, Na
2o0.5 ~ 1.5%; The component content of boccaro tire is: SiO255 ~ 68%Al
2o
320 ~ 30%, Fe
2o
33 ~ 7%, CaO0.5 ~ 1%, MgO0.3 ~ 1%, K
2o1 ~ 2.5%, Na
2o0.5 ~ 1%, celadon glaze has been executed on celadon tire surface, the surface not glazing of boccaro tire.
Further, the component content of celadon tire is: SiO272.0%, Al
2o
321.5%, Fe
2o
30.8%, CaO0.8%, MgO0.7%, K
2o3.0%, Na
2o1.2%; The component content of boccaro tire is: SiO265.4%, Al
2o
325.3%, Fe
2o
35.4%, CaO0.8%, MgO0.8%, K
2o1.6%, Na
2o0.7%.
The preparation method of the ceramic that above-mentioned celadon combines with boccaro, is realized by following steps:
(1) become assignment system celadon plastic mass or slip casting blank by above-mentioned celadon tire, then carry out shaping;
(2) by above-mentioned boccaro tire composition, preparation boccaro plastic mass or slurry;
(3) ((spend the skill and technique such as) ﹑ Shua ﹑ spray boccaro blank or slurry to be decorated at the surperficial position preset of celadon base, boccaro decorative layer thickness is not less than 0.5mm to flower) ﹑ heap in employing subsides.
(4) base substrate is through super-dry, for improving blank strength and water-intake rate, celadon glaze is executed on celadon tire surface, the surface not glazing of boccaro tire, first carries out low temperature biscuiting in oxidizing atmosphere, and firing temperature is 550 ~ 1105 DEG C, continue to adopt reducing atmosphere to fire, firing temperature is 1250 ~ 1320 DEG C, 5-10 minute before burning till end, adopts short-term oxidizing atmosphere to burn till; Firing time is 9-11 hour.
Biscuiting firing temperature control process under above-mentioned oxidizing atmosphere: be heated to 200 DEG C by room temperature in 0-1 hour, is heated to 400 DEG C in 1-2 hour, within 2-3 hour, is heated to 550 DEG C, within 3-4 hour, is heated to 700 DEG C, within 4-5 hour, is heated to 900 DEG C, within 5-6 hour, is heated to 1105 DEG C; Under reducing atmosphere, firing temperature control process: 6-7 hour is heated to 1100 DEG C, within 7-8 hour, is heated to 1180 DEG C, within 8-9 hour, is heated to 1260 DEG C, within 9-10 hour, is heated to 1310 DEG C, is incubated half an hour at 1310 DEG C; Cool to 1300 DEG C carry out oxidizing atmosphere under fire, the time is 5-10 minute.
Beneficial effect: the boccaro blank being adapted to the requirement of celadon firing process by preparation, the ceramic providing a kind of celadon to combine with boccaro, reaches the perfect adaptation of celadon and boccaro.Boccaro adopts oxidizing atmosphere to burn till, and combinations color and lustre is good, and smooth surface has ventilation property, embodies the original characteristic of purple-clay product.
Embodiment
Embodiment 1:
According to weight percent, the component content of celadon tire is: SiO274%, Al
2o
320%, Fe
2o
31.5%, CaO0.5%, MgO0.5%, K
2o2%, Na
2o1.5%; The component content of boccaro tire is: SiO268%Al
2o
328%, Fe
2o
35%, CaO0.8%, MgO0.7%, K
2o1.5%, Na
2o0.5%, celadon glaze has been executed on celadon tire surface, the surface not glazing of boccaro tire.
Preparation method, is realized by following steps:
(1) become assignment system celadon plastic mass or slip casting blank by above-mentioned celadon tire, then carry out shaping;
(2) by above-mentioned boccaro tire composition, preparation boccaro plastic mass or slurry;
(3) ((spend the skill and technique such as) ﹑ Shua ﹑ spray boccaro blank or slurry to be decorated at the surperficial position preset of celadon base, boccaro decorative layer thickness is not less than 0.5mm to flower) ﹑ heap in employing subsides.
(4) base substrate is through super-dry, for improving blank strength and water-intake rate, celadon glaze is executed on celadon tire surface, the surface not glazing of boccaro tire, first carries out low temperature biscuiting in oxidizing atmosphere, and firing temperature is 1105 DEG C, continue to adopt reducing atmosphere to fire, firing temperature is 1310 DEG C, is burning till first 5 minutes of end, adopts short-term oxidizing atmosphere to burn till.
Biscuiting firing temperature control process under above-mentioned oxidizing atmosphere: be heated to 200 DEG C by room temperature in 0-1 hour, is heated to 400 DEG C in 1-2 hour, within 2-3 hour, is heated to 550 DEG C, within 3-4 hour, is heated to 700 DEG C, within 4-5 hour, is heated to 900 DEG C, within 5-6 hour, is heated to 1105 DEG C; Under reducing atmosphere, firing temperature control process: 6-7 hour is heated to 1100 DEG C, within 7-8 hour, is heated to 1180 DEG C, within 8-9 hour, is heated to 1260 DEG C, within 9-10 hour, is heated to 1310 DEG C, is incubated half an hour at 1310 DEG C; Cool to 1300 DEG C carry out oxidizing atmosphere under fire, the time is 5 minutes.Embodiment 2:
According to weight percent, the component content of celadon tire is: SiO268.5%, Al
2o
323%, Fe
2o
32%, CaO1%, MgO1%, K
2o3%, Na
2o1.5%; The component content of boccaro tire is: SiO268%Al
2o
320%, Fe
2o
37%, CaO1%, MgO1%, K
2o2%, Na
2o1%, celadon glaze has been executed on celadon tire surface, the surface not glazing of boccaro tire.
Preparation method, is realized by following steps:
(1) become assignment system celadon plastic mass or slip casting blank by above-mentioned celadon tire, then carry out shaping;
(2) by above-mentioned boccaro tire composition, preparation boccaro plastic mass or slurry;
(3) ((spend the skill and technique such as) ﹑ Shua ﹑ spray boccaro blank or slurry to be decorated at the surperficial position preset of celadon base, boccaro decorative layer thickness is not less than 0.5mm to flower) ﹑ heap in employing subsides.
(4) base substrate is through super-dry, for improving blank strength and water-intake rate, executes celadon glaze on celadon tire surface, the surface not glazing of boccaro tire, first carries out low temperature biscuiting in oxidizing atmosphere, and firing temperature is 550 DEG C, continue to adopt reducing atmosphere to fire, firing temperature is 1250 DEG C; Burn till first 10 minutes of end, adopt short-term oxidizing atmosphere to burn till.
Biscuiting firing temperature control process under above-mentioned oxidizing atmosphere: be heated to 100 DEG C by room temperature in 0-1 hour, is heated to 200 DEG C in 1-2 hour, within 2-3 hour, is heated to 310 DEG C, within 3-4 hour, is heated to 380 DEG C, within 4-5 hour, is heated to 500 DEG C, within 5-6 hour, is heated to 550 DEG C; Under reducing atmosphere, firing temperature control process: 6-7 hour is heated to 900 DEG C, within 7-8 hour, is heated to 950 DEG C, within 8-9 hour, is heated to 1000 DEG C, within 9-10 hour, is heated to 1250 DEG C, is incubated half an hour at 1250 DEG C; Cool to 1200 DEG C carry out oxidizing atmosphere under fire, the time is 10 minutes.
Embodiment 3:
According to weight percent, the component content of celadon tire is: SiO272.0%, Al
2o
321.5%, Fe
2o
30.8%, CaO0.8%, MgO0.7%, K
2o3.0%, Na
2o1.2%; The component content of boccaro tire is: SiO265.4%, Al
2o
325.3%, Fe
2o
35.4%, CaO0.8%, MgO0.8%, K
2o1.6%, Na
2o0.7%.
Preparation method, is realized by following steps:
(1) become assignment system celadon plastic mass or slip casting blank by above-mentioned celadon tire, then carry out shaping;
(2) by above-mentioned boccaro tire composition, preparation boccaro plastic mass or slurry;
(3) ((spend the skill and technique such as) ﹑ Shua ﹑ spray boccaro blank or slurry to be decorated at the surperficial position preset of celadon base, boccaro decorative layer thickness is not less than 0.5mm to flower) ﹑ heap in employing subsides.
(4) base substrate is through super-dry, for improving blank strength and water-intake rate, executes celadon glaze on celadon tire surface, the surface not glazing of boccaro tire, first carries out low temperature biscuiting in oxidizing atmosphere, and firing temperature is 900 DEG C, continue to adopt reducing atmosphere to fire, firing temperature is 1310 DEG C; Burn till first 8 minutes of end, adopt short-term oxidizing atmosphere to burn till.
Biscuiting firing temperature control process under above-mentioned oxidizing atmosphere: be heated to 200 DEG C by room temperature in 0-1 hour, is heated to 400 DEG C in 1-2 hour, within 2-3 hour, is heated to 550 DEG C, within 3-4 hour, is heated to 700 DEG C, within 4-5 hour, is heated to 800 DEG C, within 5-6 hour, is heated to 900 DEG C; Under reducing atmosphere, firing temperature control process: 6-7 hour is heated to 1100 DEG C, within 7-8 hour, is heated to 1180 DEG C, within 8-9 hour, is heated to 1260 DEG C, within 9-10 hour, is heated to 1310 DEG C, is incubated half an hour at 1310 DEG C; Cool to 1300 DEG C carry out oxidizing atmosphere under fire, the time is 8 minutes.
Claims (4)
1. the ceramic that combines with boccaro of celadon, is characterized in that: the tire of same ceramic is made up of celadon and boccaro two portions.According to weight percent, the component content of celadon tire is: SiO260 ~ 74%, Al
2o
318 ~ 23%, Fe
2o
30.1 ~ 2%, CaO0.3 ~ 1%, MgO0.3 ~ 1%, K
2o1.5 ~ 3%, Na
2o0.5 ~ 1.5%; The component content of boccaro tire is: SiO255 ~ 68%Al
2o
320 ~ 30%, Fe
2o
33 ~ 7%, CaO0.5 ~ 1%, MgO0.3 ~ 1%, K
2o1 ~ 2.5%, Na
2o0.5 ~ 1%, celadon glaze has been executed on celadon tire surface, the surface not glazing of boccaro tire.
2. the ceramic that combines with boccaro of celadon according to claim 1, is characterized in that the component content of described celadon tire is: SiO272.0%, Al
2o
321.5%, Fe
2o
30.8%, CaO0.8%, MgO0.7%, K
2o3.0%, Na
2o1.2%; The component content of boccaro tire is: SiO265.4%, Al
2o
325.3%, Fe
2o
35.4%, CaO0.8%, MgO0.8%, K
2o1.6%, Na
2o0.7%.
3. the preparation method of the ceramic that a kind of celadon combines with boccaro according to claim 1 or 2, it is characterized in that being realized by following steps:
(1) become assignment system celadon plastic mass or slip casting blank by above-mentioned celadon tire, then carry out shaping;
(2) by above-mentioned boccaro tire composition, preparation boccaro plastic mass or slurry;
(3) ((spend the skill and technique such as) ﹑ Shua ﹑ spray boccaro blank or slurry to be decorated at the surperficial position preset of celadon base, boccaro decorative layer thickness is not less than 0.5mm to flower) ﹑ heap in employing subsides.
(4) base substrate is through super-dry, celadon glaze is executed on celadon tire surface, the surface not glazing of boccaro tire, in oxidizing atmosphere, first carry out low temperature biscuiting, firing temperature is 550 ~ 1105 DEG C, continues to adopt reducing atmosphere to fire, firing temperature is 1250 ~ 1320 DEG C, before burning till end, adopt short-term oxidizing atmosphere to burn till, firing time is 9-11 hour.
4. the preparation method of ceramic that combines with boccaro of a kind of celadon according to claim 3, it is characterized in that: biscuiting firing temperature control process under oxidizing atmosphere: be heated to 200 DEG C by room temperature in 0-1 hour, within 1-2 hour, be heated to 400 DEG C, within 2-3 hour, be heated to 550 DEG C, within 3-4 hour, be heated to 700 DEG C, within 4-5 hour, be heated to 900 DEG C, within 5-6 hour, be heated to 1105 DEG C; Under reducing atmosphere, firing temperature control process: 6-7 hour is heated to 1100 DEG C, within 7-8 hour, is heated to 1180 DEG C, within 8-9 hour, is heated to 1260 DEG C, within 9-10 hour, is heated to 1310 DEG C, is incubated half an hour at 1310 DEG C; Cool to 1300 DEG C carry out oxidizing atmosphere under fire, the time is 5-10 minute.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410198857.9A CN104556970B (en) | 2014-05-12 | 2014-05-12 | Ceramic that a kind of celadon combines with boccaro and preparation method thereof |
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|---|---|---|---|
| CN201410198857.9A CN104556970B (en) | 2014-05-12 | 2014-05-12 | Ceramic that a kind of celadon combines with boccaro and preparation method thereof |
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|---|---|
| CN104556970A true CN104556970A (en) | 2015-04-29 |
| CN104556970B CN104556970B (en) | 2016-08-24 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105819831A (en) * | 2016-03-11 | 2016-08-03 | 遵义泥牛黄工艺品有限公司 | Green ceramic product and production method thereof |
| CN106830894A (en) * | 2016-05-12 | 2017-06-13 | 程新 | A kind of boccaro porcelain paints technique |
| CN106938911A (en) * | 2017-04-01 | 2017-07-11 | 福建德化陶知然陶瓷文化创意有限公司 | Ceramic and its preparation technology that Dehua ceramic whiteware is combined with boccaro |
| CN107266020A (en) * | 2016-04-07 | 2017-10-20 | 大埔县汇丰源陶瓷工艺有限公司 | Boccaro ceramic board pictures and preparation method thereof |
| CN107265863A (en) * | 2017-08-02 | 2017-10-20 | 宜兴市金鱼陶瓷有限公司 | A kind of celadon with iron oxide red gold ring glaze layer and preparation method thereof |
| CN110615666A (en) * | 2019-10-16 | 2019-12-27 | 杭州茂华工贸有限公司 | Firing process for combination of purple sand and ceramic |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105819831A (en) * | 2016-03-11 | 2016-08-03 | 遵义泥牛黄工艺品有限公司 | Green ceramic product and production method thereof |
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| CN107266020A (en) * | 2016-04-07 | 2017-10-20 | 大埔县汇丰源陶瓷工艺有限公司 | Boccaro ceramic board pictures and preparation method thereof |
| CN106830894A (en) * | 2016-05-12 | 2017-06-13 | 程新 | A kind of boccaro porcelain paints technique |
| CN106938911A (en) * | 2017-04-01 | 2017-07-11 | 福建德化陶知然陶瓷文化创意有限公司 | Ceramic and its preparation technology that Dehua ceramic whiteware is combined with boccaro |
| CN106938911B (en) * | 2017-04-01 | 2020-08-14 | 福建德化陶知然陶瓷文化创意有限公司 | Ceramic product combining German white porcelain and purple sand and preparation process thereof |
| CN107265863A (en) * | 2017-08-02 | 2017-10-20 | 宜兴市金鱼陶瓷有限公司 | A kind of celadon with iron oxide red gold ring glaze layer and preparation method thereof |
| CN110615666A (en) * | 2019-10-16 | 2019-12-27 | 杭州茂华工贸有限公司 | Firing process for combination of purple sand and ceramic |
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| CN104556970B (en) | 2016-08-24 |
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