CN104532687A - Antibacterial PVC wallpaper base paper containing nutmeg oil microcapsules and preparation method thereof - Google Patents
Antibacterial PVC wallpaper base paper containing nutmeg oil microcapsules and preparation method thereof Download PDFInfo
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- CN104532687A CN104532687A CN201410672406.4A CN201410672406A CN104532687A CN 104532687 A CN104532687 A CN 104532687A CN 201410672406 A CN201410672406 A CN 201410672406A CN 104532687 A CN104532687 A CN 104532687A
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Abstract
The invention relates to a wallpaper base paper, and more specifically relates to an antibacterial PVC wallpaper base paper containing nutmeg oil microcapsules and a preparation method thereof. The antibacterial PVC wallpaper base paper is prepared from following raw materials, by weight, 0.1 to 0.2 part of wild chrysanthemum flower water extract, 2 to 3 parts of polycarboxylic acid water reducing agent, 1 to 2 parts of polyhexamethylene guanidine, 0.01 to 0.02 part of nutmeg oil, 40 to 60 parts of softwood fully bleached chemical wood pulp, 20 to 40 parts of hardwood eucalyptus pulp, 1 to 3 parts of polyamide epichlorohydrin resin, 10 to 15 parts of calcium carbonate whisker of 600 to 800 meshes, 0.4 to 0.5 part of Arabic gum, 0.2 to 0.3 part of polyethylene glycol, 0.1 to 0.2 part of white carbon black, 12 to 15 parts of an environmental-friendly pigment of 800 to 1250 meshes, 12t o18 parts of an adhesive, and 3 to 5 parts of an auxiliary agent. The antibacterial PVC wallpaper base paper is friendly to the environment, is non-toxic, possesses long-lasting antibacterial property and mildew resistance, is excellent in physical properties, is convenient for later processing, and is capable of providing production of high-quality wallpaper with foundation.
Description
Technical field
The present invention relates to a kind of hanging raw stock, be specifically related to a kind of antimicrobial form PVC wallpaper body paper containing myristica oil microcapsule and preparation method thereof.
Background technology
What wallpaper became many owners gradually as a kind of wall surfacing material is first-selected, the advantages such as its color is various, pattern abundant, environmental protection attractive in appearance, there is the advantage that many traditional wall coverings are incomparable, improve year by year in the utilization rate of China, PVC wallpaper is the common wallpaper of a class, it is mainly with pure paper as base material, and then at substrate surface coating polyvinyl chloride resin sizing material, then postmenstruation, ornamenting processing process obtained finished product.
Body paper directly has influence on operation effect and the service property (quality) in wallpaper later stage as base material, current body paper material ubiquity intensity, poor toughness, surface absorption are uneven, glue not easily applies, water resistant poor heat resistance, grow bacterium and the shortcoming such as to mildew, have a strong impact on the serviceability of finished product, therefore the composition and engineering improving traditional body paper is had very much, improve its adaptability, improve post-production performance, to realize High-efficient Production, obtain quality product.
Summary of the invention
The object of the invention is to provide a kind of antimicrobial form PVC wallpaper body paper containing myristica oil microcapsule and preparation method thereof, and to achieve these goals, the technical solution used in the present invention is as follows:
A kind of antimicrobial form PVC wallpaper body paper containing myristica oil microcapsule and preparation method thereof, it is characterized in that, this body paper is made up of the raw material of following weight portion: mother chrysanthemum water extract 0.1-0.2, polycarboxylate water-reducer 2-3, polyhexamethylene guanide 1-2, mace oil 0.01-0.02, needle floats chemical wood pulp 40-60 entirely, Eucalyptus dives wood pulp 20-40, polyamine epichlorohydrin resin 1-3, 600-800 order calcium carbonate crystal whisker 10-15, Arabic gum 0.4-0.5, polyethylene glycol 0.2-0.3, white carbon 0.1-0.2, 800-1250 order environmental-friendly pigment 12-15, adhesive 12-18, auxiliary agent 3-5,
Auxiliary agent is made up of the raw material of following weight portion: polymine 4-6, neopelex 0.2-0.5, poly-l-lysine (molecular weight 70000-150000) 2-3, sweet mellow wine 1-1.5, oxidized starch 6-8, water-based defoamer 0.1-0.2, atoleine 1-2, water 12-16, preparation method is: first by polymine, neopelex, atoleine drops in 50-60 DEG C of hot water, fully be uniformly mixed and make material dissolve dispersion completely, add sweet mellow wine more subsequently, oxidized starch, be uniformly mixed 30-40min, finally add other leftover materials again, continue insulated and stirred mixing 40-50min, by the rapid draing of gained material after stirring terminates, removing moisture, and be ground into fine powder and get final product.
Described adhesive is aqueous non-toxic adhesive.
Described a kind of antimicrobial form PVC wallpaper body paper containing myristica oil microcapsule and preparation method thereof, its preparation method is:
(1) first white carbon is mixed with mace oil, white carbon is made to adsorb mace oil completely, gained powder is for subsequent use, subsequently Arabic gum and water are mixed with the solution that concentration is 30-40%, and white carbon-mace oil mixed powder, polyethylene glycol are dropped in solution, high-speed stirred dispersion 40-60min, makes powder dispersed in the solution, finally by gained mixed solution drying at room temperature, it is for subsequent use that gained solidfied material is prepared into 400-600 order micro mist;
(2) needle is floated full thin up making beating in chemical wood pulp, Eucalyptus dives wood pulp, mother chrysanthemum water extract, polycarboxylate water-reducer, polyhexamethylene guanide mixing input beater, beating degree is 20-30
0sR;
(3) step (1), step (2) gained material are mixed with other residual components except pigment, adhesive, auxiliary agent, after being fully uniformly mixed 1-2h, mixed slurry manufactured paper with pulp through long mesh paper making machine, dry, obtain semi-finished product body paper;
(4) adhesive input is doubled in the water of its weight portion, auxiliary agent, pigment is added after dilution evenly, high-speed stirred makes it mix completely, obtain surface coating liquid, subsequently this surface coating liquid is coated the semi-finished product body paper surface of step (3) gained, then drying, surface pressure polishing decorations, batch after namely obtain body paper and become paper.
Body paper advantage of the present invention is: by mace oil after white carbon absorption, then carry out coated process with Arabic gum, make its microencapsulation, the raw material after process better disperses, combines in fibre stuff, and can keep fragrance lastingly and play antibacterial action; Mother chrysanthemum extract in raw material, polyhexamethylene guanide also have good sterilization and press down mould effect, and the semi-finished product body paper of preparation compacts smooth; It is full that auxiliary agent, pigment and adhesive dilute the surface coating liquid uniform color prepared, and keeps effective, be easily coated with, and can effectively promote body paper intensity, strengthens water resistant ability, and make body paper smooth surface fine and close, postorder process is more efficient.To sum up, hanging raw stock environment-protecting asepsis of the present invention, durable antibiotic mildew-resistant, good physical properties, is easy to post-production, lays a good foundation for producing high-quality wallpaper finished product.
Detailed description of the invention
Embodiment
The body paper of the present embodiment is obtained by the raw material of following weight portion: mother chrysanthemum water extract 0.2, polycarboxylate water-reducer 2, polyhexamethylene guanide 2, mace oil 0.01, needle float chemical wood pulp 55, Eucalyptus dives wood pulp 35, polyamine epichlorohydrin resin 4.2,800 order calcium carbonate crystal whisker 15, Arabic gum 0.4, polyethylene glycol 0.2, white carbon 0.1,1250 order environmental-friendly pigment 13, adhesive 15, auxiliary agent 4 entirely.
Auxiliary agent is made up of the raw material of following weight portion: polymine 5, neopelex 0.3, poly-l-lysine (molecular weight 70000-150000) 3, sweet mellow wine 1.2, oxidized starch 8, water-based defoamer 0.1, atoleine 1.5, water 16, preparation method is: first by polymine, neopelex, atoleine drops in 50-60 DEG C of hot water, fully be uniformly mixed and make material dissolve dispersion completely, add sweet mellow wine more subsequently, oxidized starch, be uniformly mixed 40min, finally add other leftover materials again, continue insulated and stirred mixing 45min, by the rapid draing of gained material after stirring terminates, removing moisture, and be ground into fine powder and get final product.
Wherein adhesive to be solid content be 45 ± 1% phenylethylene-maleic anhydride polymer emulsion.
The preparation method of the present embodiment body paper is:
(1) first white carbon is mixed with mace oil, white carbon is made to adsorb mace oil completely, gained powder is for subsequent use, subsequently Arabic gum and water are mixed with the solution that concentration is 36.5%, and white carbon-mace oil mixed powder, polyethylene glycol are dropped in solution, high-speed stirred dispersion 55min, makes powder dispersed in the solution, finally by gained mixed solution drying at room temperature, it is for subsequent use that gained solidfied material is prepared into 600 order micro mists;
(2) needle is floated full thin up making beating in chemical wood pulp, Eucalyptus dives wood pulp, mother chrysanthemum water extract, polycarboxylate water-reducer, polyhexamethylene guanide mixing input beater, beating degree is 28
0sR;
(3) step (1), step (2) gained material are mixed with other residual components except pigment, adhesive, auxiliary agent, after being fully uniformly mixed 1.8h, mixed slurry manufactured paper with pulp through long mesh paper making machine, dry, obtain semi-finished product body paper;
(4) adhesive input is doubled in the water of its weight portion, auxiliary agent, pigment is added after dilution evenly, high-speed stirred makes it mix completely, obtain surface coating liquid, subsequently this surface coating liquid is coated the semi-finished product body paper surface of step (3) gained, then drying, surface pressure polishing decorations, batch after namely obtain body paper and become paper.
Body paper prepared by the present embodiment becomes each performance indications of paper as follows:
Presentation quality: uniform in color, surface smoothing, even tissue; Machine direction tensile strength: 3.1KN/m; Wet strength: 2.4KN/m; Tightness: 0.62g/m
3; Opacity: 94.2%; Air permeability: 2150ml/min; Surface absorption: 56g/m
2(60s); Expansion and contraction 0.3%, killing fungus rate: 95.4%.
Claims (3)
1. antimicrobial form PVC wallpaper body paper containing myristica oil microcapsule and preparation method thereof, it is characterized in that, this body paper is made up of the raw material of following weight portion: mother chrysanthemum water extract 0.1-0.2, polycarboxylate water-reducer 2-3, polyhexamethylene guanide 1-2, mace oil 0.01-0.02, needle floats chemical wood pulp 40-60 entirely, Eucalyptus dives wood pulp 20-40, polyamine epichlorohydrin resin 4-5, 600-800 order calcium carbonate crystal whisker 10-15, Arabic gum 0.4-0.5, polyethylene glycol 0.2-0.3, white carbon 0.1-0.2, 800-1250 order environmental-friendly pigment 12-15, adhesive 12-18, auxiliary agent 3-5,
Auxiliary agent is made up of the raw material of following weight portion: polymine 4-6, neopelex 0.2-0.5, poly-l-lysine (molecular weight 70000-150000) 2-3, sweet mellow wine 1-1.5, oxidized starch 6-8, water-based defoamer 0.1-0.2, atoleine 1-2, water 12-16, preparation method is: first by polymine, neopelex, atoleine drops in 50-60 DEG C of hot water, fully be uniformly mixed and make material dissolve dispersion completely, add sweet mellow wine more subsequently, oxidized starch, be uniformly mixed 30-40min, finally add other leftover materials again, continue insulated and stirred mixing 40-50min, by the rapid draing of gained material after stirring terminates, removing moisture, and be ground into fine powder and get final product.
2. a kind of antimicrobial form PVC wallpaper body paper containing myristica oil microcapsule and preparation method thereof as claimed in claim 1, it is characterized in that, described adhesive is aqueous non-toxic adhesive.
3. a kind of antimicrobial form PVC wallpaper body paper containing myristica oil microcapsule and preparation method thereof as claimed in claim 1, its preparation method is:
(1) first white carbon is mixed with mace oil, white carbon is made to adsorb mace oil completely, gained powder is for subsequent use, subsequently Arabic gum and water are mixed with the solution that concentration is 30-40%, and white carbon-mace oil mixed powder, polyethylene glycol are dropped in solution, high-speed stirred dispersion 40-60min, makes powder dispersed in the solution, finally by gained mixed solution drying at room temperature, it is for subsequent use that gained solidfied material is prepared into 400-600 order micro mist;
(2) needle is floated full thin up making beating in chemical wood pulp, Eucalyptus dives wood pulp, mother chrysanthemum water extract, polycarboxylate water-reducer, polyhexamethylene guanide mixing input beater, beating degree is 20-30
0sR;
(3) step (1), step (2) gained material are mixed with other residual components except pigment, adhesive, auxiliary agent, after being fully uniformly mixed 1-2h, mixed slurry manufactured paper with pulp through long mesh paper making machine, dry, obtain semi-finished product body paper;
(4) adhesive input is doubled in the water of its weight portion, auxiliary agent, pigment is added after dilution evenly, high-speed stirred makes it mix completely, obtain surface coating liquid, subsequently this surface coating liquid is coated the semi-finished product body paper surface of step (3) gained, then drying, surface pressure polishing decorations, batch after namely obtain body paper and become paper.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105064138A (en) * | 2015-08-10 | 2015-11-18 | 桂林威迈壁纸有限公司 | Mildewproof aromatic wallpaper |
CN105239457A (en) * | 2015-09-07 | 2016-01-13 | 龚灿锋 | Mildew-proofing, drying and anti-bacterial treatment agent for printing paper |
CN105298073A (en) * | 2015-11-25 | 2016-02-03 | 安徽索亚装饰材料有限公司 | Wallpaper containing nano calcium carbonate crystal whisker-polylactic acid porous fiber modified acrylic resin emulsion coating |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104005260A (en) * | 2013-02-21 | 2014-08-27 | 甘木林 | Wallpaper base produced with recycled pulp |
-
2014
- 2014-11-22 CN CN201410672406.4A patent/CN104532687A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104005260A (en) * | 2013-02-21 | 2014-08-27 | 甘木林 | Wallpaper base produced with recycled pulp |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105064138A (en) * | 2015-08-10 | 2015-11-18 | 桂林威迈壁纸有限公司 | Mildewproof aromatic wallpaper |
CN105239457A (en) * | 2015-09-07 | 2016-01-13 | 龚灿锋 | Mildew-proofing, drying and anti-bacterial treatment agent for printing paper |
CN105298073A (en) * | 2015-11-25 | 2016-02-03 | 安徽索亚装饰材料有限公司 | Wallpaper containing nano calcium carbonate crystal whisker-polylactic acid porous fiber modified acrylic resin emulsion coating |
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Application publication date: 20150422 |
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