CN104498283A - Production method of eucommia bark health-maintenance health care wine - Google Patents
Production method of eucommia bark health-maintenance health care wine Download PDFInfo
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- CN104498283A CN104498283A CN201410747273.2A CN201410747273A CN104498283A CN 104498283 A CN104498283 A CN 104498283A CN 201410747273 A CN201410747273 A CN 201410747273A CN 104498283 A CN104498283 A CN 104498283A
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
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Abstract
The invention discloses a production method of a eucommia bark health-maintenance health care wine. The method comprises the following steps: adding crushed eucommia bark leaves in to ethanol, leaching for 3-4 hours at 50+/-5 DEG C while stirring, performing suction filtration on a leaching solution, then adding ethanol equal to 6-10 parts of the mass of the eucommia bark leaves, leaching for two times, combining the leaching solutions, and standing for depositing for 12 hours; performing refined filtration on supernatant of depositing, pumping a refined filtration solution into a vacuum outer circulation concentrator, performing vacuum concentration at 65-70 DEG C, recovering ethanol, and concentrating until the Baume degree is 28-32 DEG Be and the density is 1.2-1.3; pumping a concentrated solution into a spray drying tower, and instantly drying atomized particles into powder at a high temperature between 170 and 180 DEG C, thereby preparing a eucommia bark extract; and mixing white spirit, the eucommia bark leaf extract and a flavoring agent, standing, and filtering to prepare the eucommia bark health-maintenance health care wine. The eucommia bark health-maintenance health care wine produced by the method disclosed by the invention is short in soaking time and high in production speed, and the product does not contain a preservative and a coloring agent, and has health-maintenance health care effects of promoting blood circulation to dispel blood stasis, tonifying the liver and kidneys, strengthening bones and muscles, resisting amnesia, preventing reduction of sexual function and the like.
Description
Technical field
The present invention relates to a kind of production of alcoholic drink, provide a kind of with Chinese medicinal materials Folium Eucommiae extract be raw material bark of eucommia assembled alcoholic drinks production method and standard.
Background technology
The title that wine have " length of hundred medicines ", edible wine is a kind of nourishing drink, can stimulate circulation, clearing and activating the channels and collaterals, and wind-damp dispelling, improves the health.Chinese medicine and wine " molten " are in the medicinal liquor of one, there is preparation convenience, the property of medicine is stable, safe and effective, be easy to the advantages such as preservation, and because alcohol is a kind of good semi-polarity organic solvent, the plurality of active ingredients of Chinese medicine is all soluble in wherein, wine assisting drug, wine help medicine gesture, and give full play to its drug effect, and medicinal liquor becomes the important conventional formulation of Chinese medicine.
Traditional Chinese medicine medicinal liquor is wine base mainly with white wine, and by raw medicinal herbs or medicine materical crude slice chopping, adopt the methods such as cool leaching method, hot dipping method, circumfluence method, percolation to be used as medicine processs of preparing Chinese medicine, ultimate principle take alcohol as solvent, the effective constituent in stripping and preservation medicinal material.The technical barrier of common existence is the best pure concentration difficulty grasp of medicinal liquor, and in medicinal material, functional component utilization ratio is not high; The clarity of wine body is poor, and effective constituent and component concentration instability, quality standard controls the problems such as more difficult.
Chinese medicine standard extract, refers to employing modern science and technology, carries out extracting processing and a kind of tcm product with relatively clear and definite effective substance and strict quality specifications of obtaining, can be used as the bulk drug of Chinese medicine preparation to traditional Chinese medicine material.Its chemical composition is the set that multiple pharmacological active substance forms in specific proportions, and it inherits the multicomponent feature of Chinese medicine and former Chinese medicinal materials given efficacy.At home, existing more than 600 plant Chinese patent medicine uses extract to substitute raw medicinal herbs, with the stability of improving the quality of products and controllability, becomes the new trend of quality standards in Chinese drugs.
The bark of eucommia (formal name used at school Eucommia ulmoides Oliver), having another name called bakelite, is Eucommiaceae plant, is Chinese famous and precious tonic herb.Its taste is sweet, warm in nature.Have tonify the liver and kidney, strengthen muscles and bones, recuperating CHONG and REN meridians, solid through antiabortive effect.Can treat the pain in the waist and lower extremities or aching and limp unable that insufficiency of kidney-YANG causes, born of the same parents' tire that deficiency of liver-QI causes is solid, and scrotum is wet the disease such as to itch.Be listed in top grade in Shennong's Herbal.The modern study bark of eucommia has rubbish in purged body, strengthens human body cell substance metabolism, prevents muscle skeleton aging, balanced human's blood pressure, decomposer inner cholesterol, reduces body fat, recovers blood vessel elasticity, diuresis heat-clearing, broad-spectrum antimicrobial, stimulating central nervous system, improves white cell pharmacological action.For a long time, people make the tradition of health promoting wine with regard to the useful bark of eucommia, and the multiplex bark of eucommia and other herbal medicine white wine directly soak to be made.Disclosed in Chinese patent, a kind of " making method of eucommia wine " (CN1081109) take the bark of eucommia as main ingredient, the medicine such as the red sage root, Ligusticum wallichii is adjuvant, mix with sugar by a certain percentage, be immersed in white wine, the eucommia wine produced after degree of falling, seasoning, toning and filtration treatment.The eucommia wine active constituent content that this method is made is less, have impact on health care's effect
.
Summary of the invention
The object of the invention is to provide a kind of medicinal efficacy definite ingredients, the production method of eucommia bark health-care health promoting wine stable and controllable for quality.
Technical solution of the present invention is: a kind of production method of eucommia bark health-care health promoting wine, comprises the following steps:
(1) select the 6-8 month fine day pluck Fresh Folium Eucommiae, dry or dry, moisture containing control 12% with, be crushed to 10 ~ 20 orders;
(2) Folium Eucommiae pulverized is dropped in stainless steel extractor, add ethanol, feed liquid mass ratio 1:8 ~ 12, stirring and leaching 3 ~ 4h at 50 DEG C ± 5 DEG C temperature, vat liquor adds the ethanol of Folium Eucommiae quality 6 ~ 10 again after suction filtration, twice lixiviate under the same terms, merges vat liquor, quiescent setting 12h;
(3) precipitate the filter of supernatant liquor essence, pump into smart filtrate tanks, bottom feed liquid, first by filter press, pumps into smart filtrate tanks after the filter of pressing filtering liquid essence;
(4) by smart filtrate suction vacuum outer circulation thickener, vacuum concentration at 65 ~ 70 DEG C, reclaim ethanol, concentrated solution to degree Beaume 28-32 ° of B é, density 1.2 ~ 1.3;
(5) concentrated solution pumps in spray-drying tower by high-pressure homogeneous, under 170 ~ 180 DEG C of high temperature, and the particle wink-dry powdering of atomization, obtained Cortex Eucommiae extract;
(6) by white wine, Folium Eucommiae extract, seasonings mixing preparation, leave standstill and filter, be i.e. obtained eucommia bark health-care health promoting wine, the quality proportioning of described white wine, Folium Eucommiae extract, seasonings is 100:1.5 ~ 2.5:0.5 ~ 1.
In step (2), the concentration of described ethanol is 70%.
In step (6), described seasonings is honey, rock sugar or fructose.It is raw material that described wine adopts with Cereals, and the white wine brewageed through solid-state or semi-solid fermentation method is wine based raw material, alcoholic strength 30 ~ 56 degree.
Through the eucommia bark health-care health promoting wine that invention is produced, primary medicinal component content: total flavones >=55mg/L, Geniposidic acid >=30mg/L, chlorogenic acid >=25mg/L.
The eucommia bark health-care health promoting wine that the present invention produces, soak time is short, and production rate is fast, and product is not containing sanitas and tinting material; Have promoting blood circulation and removing blood stasis, invigorating the liver and kidney, strengthening the bones and muscles, the health-care effect such as anti-amnesic, preventative function reduction.
Embodiment
Below in conjunction with concrete case study on implementation, the present invention is described further.
Embodiment 1
Pluck the fresh leaf 500kg of 4 years raws bark of eucommia of mid-June, the same day dries at 65 DEG C of temperature with dryer, to water content 10.8%, obtains the bark of eucommia and bakes leaf 132kg, for subsequent use; The bark of eucommia is baked leaf to drop in stainless steel extractor, add 70% ethanol 1530L, be heated to 50 DEG C, stirring and leaching 3h, vat liquor suction filtration pumps into storage tank; Add 70% ethanol 928L, bis-lixiviates, after merging the filter of vat liquor essence, clarify 12h; The supernatant liquor of clarification pumps into storage tank, and essence filter after the feed liquid filter press of bottom, merges clear liquor and vacuumize concentrated under 65 DEG C of conditions, reclaim ethanol; Concentrated solution to degree Beaume 30 ° of B é, density 1.26; Concentrated solution pumps into spray-drying tower drying, obtains Folium Eucommiae extract 37.6kg.56 degree of grain Chinese liquor 200kg that solid state fermentation of learning from else's experience is brewageed, add Folium Eucommiae extract 4kg, honey 0.5kg, blends, and mixes thoroughly evenly, leaves standstill and filter, tasting.Through quality inspection, bark of eucommia assembled alcoholic drinks alcoholic strength 54 degree, primary medicinal component content in wine: total flavones 68mg/L, Geniposidic acid 37mg/L, chlorogenic acid 32mg/L, meets target level of product quality, and storing can be filling after 5 days.
Embodiment 2
Get the Folium Eucommiae extract 4kg of preparation in example 1.Add the 36 degree of grain Chinese liquor 200kg brewageed through solid state fermentation, the rock sugar syrup 1kg(degree Beaume 40 ° of B é boiled in advance), blend, mix thoroughly evenly, leave standstill and filter, tasting.Through quality inspection, alcoholic strength 35 degree, primary medicinal component content in wine: total flavones 52mg/L, Geniposidic acid 39mg/L, chlorogenic acid 29mg/L, meets target level of product quality, and storing 10 days can be filling.
Claims (4)
1. a production method for eucommia bark health-care health promoting wine, is characterized in that, comprises the following steps:
(1) select the 6-8 month fine day pluck Fresh Folium Eucommiae, dry or dry, moisture containing control 12% with, be crushed to 10 ~ 20 orders;
(2) Folium Eucommiae pulverized is dropped in stainless steel extractor, add ethanol, feed liquid mass ratio 1:8 ~ 12, stirring and leaching 3 ~ 4h at 50 DEG C ± 5 DEG C temperature, vat liquor adds the ethanol of Folium Eucommiae quality 6 ~ 10 again after suction filtration, twice lixiviate under the same terms, merges vat liquor, quiescent setting 12h;
(3) precipitate the filter of supernatant liquor essence, pump into smart filtrate tanks, bottom feed liquid, first by filter press, pumps into smart filtrate tanks after the filter of pressing filtering liquid essence;
(4) by smart filtrate suction vacuum outer circulation thickener, vacuum concentration at 65 ~ 70 DEG C, reclaim ethanol, concentrated solution to degree Beaume 28-32 ° of B é, density 1.2 ~ 1.3;
(5) concentrated solution pumps in spray-drying tower by high-pressure homogeneous, under 170 ~ 180 DEG C of high temperature, and the particle wink-dry powdering of atomization, obtained Cortex Eucommiae extract;
By white wine, Folium Eucommiae extract, seasonings mixing preparation, leave standstill and filter, be i.e. obtained eucommia bark health-care health promoting wine, the quality proportioning of described white wine, Folium Eucommiae extract, seasonings is 100:1.5 ~ 2.5:0.5 ~ 1.
2. the production method of eucommia bark health-care health promoting wine according to claim 1, is characterized in that, in step (2), the concentration of described ethanol is 70%.
3. the production method of eucommia bark health-care health promoting wine according to claim 1, is characterized in that, in step (6), described seasonings is honey, rock sugar or fructose.
4. it is raw material that wine described in adopts with Cereals, and the white wine brewageed through solid-state or semi-solid fermentation method is wine based raw material, alcoholic strength 30 ~ 56 degree.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410747273.2A CN104498283A (en) | 2014-12-10 | 2014-12-10 | Production method of eucommia bark health-maintenance health care wine |
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| CN201410747273.2A CN104498283A (en) | 2014-12-10 | 2014-12-10 | Production method of eucommia bark health-maintenance health care wine |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106047620A (en) * | 2016-08-25 | 2016-10-26 | 贵州国台酒业有限公司 | Chili wine and preparation method thereof |
| CN107841437A (en) * | 2017-12-06 | 2018-03-27 | 广州馥来民心酒业有限公司 | One seed ginseng honey health liquor and preparation method thereof |
| CN108191658A (en) * | 2018-01-09 | 2018-06-22 | 保定冀中药业有限公司 | A kind of extracting method of Chlorogenic Acid in Eucommia ulmoides Oliv. Leaves |
| CN110463760A (en) * | 2019-07-30 | 2019-11-19 | 广东省测试分析研究所（中国广州分析测试中心） | A kind of Cortex Eucommiae Yoghourt and preparation method thereof |
| CN116265574A (en) * | 2021-12-18 | 2023-06-20 | 上海宝肝科技有限公司 | Dynamic wine soaking method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1381559A (en) * | 2002-05-21 | 2002-11-27 | 张泽川 | Eucommia bark wine |
| CN1400199A (en) * | 2001-08-06 | 2003-03-05 | 西北农林科技大学 | Method for continuously extracting active substances from eucommia leaves |
| CN102145042A (en) * | 2010-11-17 | 2011-08-10 | 苏州市天灵中药饮片有限公司 | Eucommia wine |
| CN102757880A (en) * | 2012-07-25 | 2012-10-31 | 北京中科健宇生物科技有限公司 | Maca health-care wine and preparation method thereof |
| CN103829038A (en) * | 2014-03-05 | 2014-06-04 | 张家界恒兴生物科技有限公司 | Novel eucommia feed additive and production method thereof |
-
2014
- 2014-12-10 CN CN201410747273.2A patent/CN104498283A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1400199A (en) * | 2001-08-06 | 2003-03-05 | 西北农林科技大学 | Method for continuously extracting active substances from eucommia leaves |
| CN1381559A (en) * | 2002-05-21 | 2002-11-27 | 张泽川 | Eucommia bark wine |
| CN102145042A (en) * | 2010-11-17 | 2011-08-10 | 苏州市天灵中药饮片有限公司 | Eucommia wine |
| CN102757880A (en) * | 2012-07-25 | 2012-10-31 | 北京中科健宇生物科技有限公司 | Maca health-care wine and preparation method thereof |
| CN103829038A (en) * | 2014-03-05 | 2014-06-04 | 张家界恒兴生物科技有限公司 | Novel eucommia feed additive and production method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106047620A (en) * | 2016-08-25 | 2016-10-26 | 贵州国台酒业有限公司 | Chili wine and preparation method thereof |
| CN107841437A (en) * | 2017-12-06 | 2018-03-27 | 广州馥来民心酒业有限公司 | One seed ginseng honey health liquor and preparation method thereof |
| CN108191658A (en) * | 2018-01-09 | 2018-06-22 | 保定冀中药业有限公司 | A kind of extracting method of Chlorogenic Acid in Eucommia ulmoides Oliv. Leaves |
| CN108191658B (en) * | 2018-01-09 | 2021-02-26 | 保定冀中药业有限公司 | Method for extracting chlorogenic acid from eucommia ulmoides leaves |
| CN110463760A (en) * | 2019-07-30 | 2019-11-19 | 广东省测试分析研究所（中国广州分析测试中心） | A kind of Cortex Eucommiae Yoghourt and preparation method thereof |
| CN116265574A (en) * | 2021-12-18 | 2023-06-20 | 上海宝肝科技有限公司 | Dynamic wine soaking method |
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Application publication date: 20150408 |