CN104498185A - Carambola extract as well as preparation method and application of carambola extract in cigarettes - Google Patents
Carambola extract as well as preparation method and application of carambola extract in cigarettes Download PDFInfo
- Publication number
- CN104498185A CN104498185A CN201410712236.8A CN201410712236A CN104498185A CN 104498185 A CN104498185 A CN 104498185A CN 201410712236 A CN201410712236 A CN 201410712236A CN 104498185 A CN104498185 A CN 104498185A
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- China
- Prior art keywords
- carambola
- filtrate
- cigarette
- cigarettes
- extract
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a carambola extract as well as a preparation method and application of carambola extract in cigarettes. The preparation method comprises the following steps: after crushing and pulping carambola, crushing cleaned carambola to slurry, adding 85-95% ethanol of which the weight is 2-3 times that of carambola, heating to reflux for 2-3 hours, filtering while the solution is hot, using the filter dregs in the next step and remaining the filtrate; adding 30% ethanol of which the weight is 3-4 times that of filter dregs into the filter dregs, heating to reflux for 2-3 hours, and after filtering while the solution is hot, repeating the step, combining the filtrate and concentrating at a reduced pressure to obtain a concentrate A; and after mixing the concentrate A with the primary filtrate, standing and filtering the mixture at 0 to -10 DEG C, and concentrating the filtrate at the reduced pressure to obtain a faint yellow liquid, namely the carambola extract for cigarettes. The preparation method disclosed by the invention is simple and practical and easy to operate and practice. The obtained product used for the cigarettes can be used for effectively improving the agreeable aftertaste of the cigarettes and improving the sour, sweet and moistening senses of the cigarettes, so that the smoke is smooth and fine and the fragrant concentration of the cigarettes is increased.
Description
Technical field
The invention belongs to cigaret additive technical field, be specifically related to a kind of carambola extract and preparation method thereof, the invention still further relates to the application of described carambola extract in cigarette simultaneously.
Background technology
Carambola, has another name called carambola, is a kind of fruit originating in tropical and subtropical zone, has very high nutritive value.Carambola contains abundant sugar, mainly comprises sucrose, fructose, glucose, also containing a large amount of organic acids, comprises oxysuccinic acid, citric acid, oxalic acid, and multivitamin, micro-fat and protein.Every 100 grams of pulp moisture contents 92.5 grams, 0.6 gram, protein, fatty 0.l gram, fiber 1.1 grams, 5.3 grams, carbohydrate, ash content 0.4 gram, carotene 20 microgram, VitB1 0.01 milligram, 0.05 milligram, riboflavin, nicotinic acid 1.0 milligrams, 7 milligrams, xitix, 126 milligrams, potassium, 0.7 milligram, sodium, calcium 3 milligrams, 6 milligrams, magnesium, iron 0.6 milligram, 0.5 milligram, zinc, 27 milligrams, phosphorus, selenium 0.84 microgram.Containing a large amount of volatile components and carotene compounds in Carambola Fruit, containing 1-tricosene 21.4 milligrams in its volatile component, linolic acid 15.5 milligrams, Palmitic acid 12.3 milligrams, l-ppentacosene 10.3 milligrams, r-12 carbon lactone 1.8 milligrams, totally 57 kinds of lipids such as ten tetra-carbonics 1.2 milligrams, 9 kinds of lactones, its carotene compounds includes phytofluene, B-carotene, B-cryptoxanthin, zeaxanthin, B-A Piao, B-Radix Dauci Sativae aldehyde, B-kryptoxanthin, xenthophylls, procrypsis element etc.; Containing glucopyanoside in its fruit juice, support one's family C, B, oxalic acid, citric acid, oxysuccinic acid, sucrose, fructose, glucose etc., and wherein, Vitamin C content is very abundant, containing Catergen 7.2 milligrams in every 100 milliliters of fruit juice.Carambola taste sweet and sour taste, can supplement rapidly the moisture of human body, promote the production of body fluid to quench thirst, diuresis detoxify, and in help digestion, throat clearing and benefiting.
At present, there is not been reported carambola extract to be used for tobacco industry.Be that development of raw materials develops new high-grade cigarette additive with carambola, the suction quality of cigarette can be improved, expand its application in cigarette, there are certain market outlook.
Summary of the invention
The object of the present invention is to provide a kind of carambola extract and preparation method thereof and the application in cigarette.Described carambola extract joins in the pipe tobacco of production process, can effectively improve cigarette pleasant impression, improves the sour-sweet moisture feeling of cigarette, makes flue gas fine and smooth, increases cigarette flavor concentration.
Object of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage ratio of the present invention is weight percentage.
A preparation method for carambola extract, comprises the following steps:
(1) carambola after clean is broken into pulpous state;
(2) in carambola slurry, add 85% ~ 95% ethanol of its weight 2 ~ 3 times amount, be heated to 90 ± 2 DEG C of backflow 2 ~ 3h, filtered while hot, filter residue is used for next step, and filtrate retains;
(3) add 30% ethanol of its weight 3 ~ 4 times amount to the filter residue in step (2), be heated to 90 ± 2 DEG C of backflow 2 ~ 3h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.0500 ± 0.004g/cm
3, obtain enriched material A;
(4) step (3) gained enriched material A is mixed with step (1) gained filtrate be placed on 0 ~-10 DEG C at leave standstill after 36 ~ 48h and filter, it is 0.980 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C
3, gained weak yellow liquid is cigarette carambola extract.
Described carambola extract can be applicable to production of cigarettes, does not need to change cigarette original complete processing during application, can directly carambola extract be added in cigarette shreds.Concrete grammar is: by carambola extract with after the amount ultrapure water of cigarette shreds weight 0.2 ~ 0.5% dilution 3 ~ 4 times of weight, be evenly sprayed on pipe tobacco, prepare cigarette in existing mode in the mode be atomized.
Beneficial effect of the present invention: the cigarette and the blank cigarette that add carambola extract carry out sensory evaluating smoking, smoking result shows, carambola extract of the present invention can improve cigarette pleasant impression, improves the sour-sweet moisture feeling of cigarette, make flue gas fine and smooth, improve the effect of cigarette flavor concentration.Preparation method of the present invention is simple and practical, and operation is implemented easily.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail, but embodiment is not limited to the technical solution.
embodiment 1
(1) accurately take 2Kg carambola, put in juice extractor fragmentation of pulling an oar and obtain carambola slurry.By 85% alcohol immersion of carambola slurry by its weight 2 times amount, reflux 2h at temperature 90 DEG C, filtered while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(2) add 30% ethanol of its weight 3 times amount to the filter residue in step (1), be heated to 90 ± 2 DEG C of backflow 2h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.050 ± 0.004g/cm
3, obtain enriched material A;
(3) step (2) gained enriched material A is mixed with step (1) gained filtrate be placed on 0 DEG C at leave standstill after 48h and filter, it is 0.980 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C
3, obtain weak yellow liquid 252g, be cigarette carambola extract.
Above-mentioned carambola extract is used for cloud and mist tobacco leaf formulation, carambola extract is got by 0.2% of cigarette shreds weight, after diluting 3 times of weight with ultrapure water, be sprayed onto on cigarette shreds in the mode of atomization, balance 48h under constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2%), roll into Cigarette.
embodiment 2
(1) accurately take 2Kg carambola, put in juice extractor fragmentation of pulling an oar and obtain carambola slurry.By 95% alcohol immersion of carambola slurry by its weight 3 times amount, reflux 3h at temperature 90 DEG C, filtered while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(2) add 30% ethanol of its weight 4 times amount to the filter residue in step (1), be heated to 90 ± 2 DEG C of backflow 3h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.050 ± 0.004g/cm
3, obtain enriched material A;
(3) step (2) gained enriched material A is mixed with step (1) gained filtrate be placed on-10 DEG C at leave standstill after 36h and filter, it is 0.980 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C
3, obtain weak yellow liquid 278g, be cigarette carambola extract.
Above-mentioned carambola extract is used for cloud and mist tobacco leaf formulation, carambola extract is got by 0.5% of cigarette shreds weight, after diluting 4 times of weight with ultrapure water, be sprayed onto on cigarette shreds in the mode of atomization, balance 48h under constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2%), roll into Cigarette.
embodiment 3
(1) accurately take 2Kg carambola, put in juice extractor fragmentation of pulling an oar and obtain carambola slurry.By 90% alcohol immersion of carambola slurry by its weight 2.5 times amount, reflux 2.5h at temperature 90 DEG C, filtered while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(2) add 30% ethanol of its weight 3.5 times amount to the filter residue in step (1), be heated to 90 ± 2 DEG C of backflow 2.5h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.050 ± 0.004g/cm
3, obtain enriched material A;
(3) step (2) gained enriched material A is mixed with step (1) gained filtrate be placed on-5 DEG C at leave standstill after 40h and filter, it is 0.980 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C
3, obtain weak yellow liquid 278g, be cigarette carambola extract.
Above-mentioned carambola extract is used for cloud and mist tobacco leaf formulation, carambola extract is got by 0.3% of cigarette shreds weight, after diluting 3.5 times of weight with ultrapure water, be sprayed onto on cigarette shreds in the mode of atomization, balance 48h under constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2%), roll into Cigarette.
The cigarette of above embodiment gained and blank cigarette transfer to specialty member of smoking carry out sense organ contrast smoke panel test, result is as follows:
Above content is the further description made the present invention in conjunction with concrete preferred implementation.For general technical staff of the technical field of the invention, the obvious modification made without departing from the inventive concept of the premise, performance or purposes identical, all should be considered as protection scope of the present invention.
Claims (3)
1. a preparation method for carambola extract, is characterized in that comprising following steps:
Carambola after clean is broken into pulpous state;
In carambola slurry, add 85% ~ 95% ethanol of its weight 2 ~ 3 times amount, be heated to 90 ± 2 DEG C of backflow 2 ~ 3h, filtered while hot, filter residue is used for next step, and filtrate retains;
Add 30% ethanol of its weight 3 ~ 4 times amount to the filter residue in step (2), be heated to 90 ± 2 DEG C of backflow 2 ~ 3h, repeat this step after filtered while hot, at 40 ± 2 DEG C, be evaporated to density after merging filtrate is 1.050 ± 0.004g/cm
3, obtain enriched material A;
Mixed with step (1) gained filtrate by step (3) gained enriched material A after leaving standstill 36 ~ 48h at being placed on 0 ~-10 DEG C and filter, it is 0.980 ± 0.004 g/cm that filtrate is evaporated to density at 40 DEG C
3, gained is faint yellow is cigarette carambola extract.
2. the carambola extract prepared of the preparation method of a carambola extract as claimed in claim 1.
3. the application of carambola extract in cigarette as claimed in claim 2, after it is characterized in that carambola extract is diluted 3 ~ 4 times of weight with the amount ultrapure water of cigarette shreds weight 0.2 ~ 0.5%, is sprayed onto on cigarette shreds in the mode be atomized, prepares cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410712236.8A CN104498185A (en) | 2014-12-02 | 2014-12-02 | Carambola extract as well as preparation method and application of carambola extract in cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410712236.8A CN104498185A (en) | 2014-12-02 | 2014-12-02 | Carambola extract as well as preparation method and application of carambola extract in cigarettes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104498185A true CN104498185A (en) | 2015-04-08 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410712236.8A Pending CN104498185A (en) | 2014-12-02 | 2014-12-02 | Carambola extract as well as preparation method and application of carambola extract in cigarettes |
Country Status (1)
| Country | Link |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111772187A (en) * | 2020-07-02 | 2020-10-16 | 吕剑 | Sour carambola extract, extraction method thereof and product thereof |
| CN113367376A (en) * | 2021-06-01 | 2021-09-10 | 广东中烟工业有限责任公司 | Carambola extract, preparation method thereof and application thereof in cigarettes |
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| CN102277236A (en) * | 2011-05-10 | 2011-12-14 | 无锡华海香料有限公司 | Preparation method and application of fig concentrate |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111772187A (en) * | 2020-07-02 | 2020-10-16 | 吕剑 | Sour carambola extract, extraction method thereof and product thereof |
| CN111772187B (en) * | 2020-07-02 | 2023-04-07 | 吕剑 | Sour carambola extract, extraction method thereof and product thereof |
| CN113367376A (en) * | 2021-06-01 | 2021-09-10 | 广东中烟工业有限责任公司 | Carambola extract, preparation method thereof and application thereof in cigarettes |
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20150408 |