CN104449261A - Freezing weather end carboxyl bromine carbon polyester resin fire-retardant coating and preparation method thereof - Google Patents

Freezing weather end carboxyl bromine carbon polyester resin fire-retardant coating and preparation method thereof Download PDF

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Publication number
CN104449261A
CN104449261A CN201410741578.2A CN201410741578A CN104449261A CN 104449261 A CN104449261 A CN 104449261A CN 201410741578 A CN201410741578 A CN 201410741578A CN 104449261 A CN104449261 A CN 104449261A
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CN
China
Prior art keywords
parts
polyester resin
end carboxyl
bromine carbon
carbon polyester
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410741578.2A
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Chinese (zh)
Inventor
张和庆
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TAIXING HEQING MACHINERY FITTINGS FACTORY
Original Assignee
TAIXING HEQING MACHINERY FITTINGS FACTORY
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Publication date
Application filed by TAIXING HEQING MACHINERY FITTINGS FACTORY filed Critical TAIXING HEQING MACHINERY FITTINGS FACTORY
Priority to CN201410741578.2A priority Critical patent/CN104449261A/en
Publication of CN104449261A publication Critical patent/CN104449261A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C09D5/185—Intumescent paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/02—Flame or fire retardant/resistant

Abstract

The invention relates to a freezing weather end carboxyl bromine carbon polyester resin fire-retardant coating and a preparation method thereof. The freezing weather end carboxyl bromine carbon polyester resin fire-retardant coating consists of the following raw materials in parts by mass: 80-90 parts of end carboxyl bromine carbon polyester resin, 3.5-4 parts of triethanolamine, 10-15 parts of melamine, 5-10 parts of titanium dioxide, 8-14 parts of expanded perlite, 8-12 parts of hydroxyethyl cellulose, 3-6 parts of sodium methylsilanolate, 4-7 parts of aluminum sulfate, 15-20 parts of ethylene glycol and 5-8 parts of water-soluble amide. The preparation method comprises the following steps: firstly mixing the end carboxyl bromine carbon polyester resin with triethanolamine, ethylene glycol and water-soluble amide, then adding melamine, titanium dioxide, expanded perlite and hydroxyethyl cellulose, mixing to prepare primary pulp, mixing and blending sodium methylsilanolate and aluminum sulfate, then adding the primary pulp for mixing, and finally sequentially performing melting extrusion and crushing by virtue of an extruding machine to obtain the coating.

Description

A kind of frost climate end carboxyl bromine carbon polyester resin frie retardant coating and preparation method
Technical field
The present invention relates to a kind of frie retardant coating, is a kind of frost climate end carboxyl bromine carbon polyester resin frie retardant coating and preparation method thereof specifically.
Background technology
Polyester powder coating has good physical and mechanical properties; decoration and the protection of metallic surface can be widely used in; equipment requirements coating fire prevention under frost climate, resistance toly to freeze, fragility requires higher; polyester powder coating on existing market is excellent performance in fire prevention mostly only, but cannot meet the use of frost climate particular requirement.
Summary of the invention
For above-mentioned deficiency of the prior art, the invention provides a kind of easily manufactured, cost is low, fire prevention, resistance toly to freeze, the good a kind of frost climate end carboxyl bromine carbon polyester resin frie retardant coating of fragility and preparation method.
The technical solution used in the present invention is: a kind of frost climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 80-90 part, trolamine 3.5-4 part, trimeric cyanamide 10-15 part, titanium dioxide 5-10 part, pearlstone 8-14 part, Natvosol 8-12 part, methyl silicon sodium alcoholate 3-6 part, Tai-Ace S 150 4-7 part, ethylene glycol 15-20 part, water-soluble amide 5-8 part.
A kind of preparation method of frost climate end carboxyl bromine carbon polyester resin frie retardant coating, comprise the following steps: first end carboxyl bromine carbon polyester resin is mixed with trolamine, ethylene glycol, water-soluble amide, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol carry out being mixed into magma, mixing adding magma after methyl silicon sodium alcoholate, Tai-Ace S 150 mixing preparation, finally melt extruding through forcing machine successively, pulverize and obtain coating.
The present invention adds trolamine, trimeric cyanamide, titanium dioxide, pearlstone, Natvosol in end carboxyl bromine carbon polyester resin, be equipped with methyl silicon sodium alcoholate, Tai-Ace S 150, ethylene glycol and water-soluble amide, fire prevention, the requirement that water-fast, fragility is little can be taken into account, be applicable to Special use requirement under frost climate.
Embodiment
Below in conjunction with embodiment, the invention will be further described.
Embodiment one
A kind of frost climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 80 parts, trolamine 3.5 parts, trimeric cyanamide 10 parts, titanium dioxide 5 parts, pearlstone 8 parts, Natvosol 8 parts, methyl silicon sodium alcoholate 3 parts, 4 parts, Tai-Ace S 150, ethylene glycol 15 parts, water-soluble amide 5 parts.Preparation method comprises the following steps: first mixed with trolamine, ethylene glycol, water-soluble amide by end carboxyl bromine carbon polyester resin, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol carry out being mixed into magma, mixing adding magma after methyl silicon sodium alcoholate, Tai-Ace S 150 mixing preparation, finally melt extruding through forcing machine successively, pulverize and obtain coating.
Embodiment two
A kind of frost climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 90 parts, trolamine 4 parts, trimeric cyanamide 15 parts, titanium dioxide 10 parts, pearlstone 14 parts, Natvosol 12 parts, methyl silicon sodium alcoholate 6 parts, 7 parts, Tai-Ace S 150, ethylene glycol 20 parts, water-soluble amide 8 parts.Preparation method comprises the following steps: first mixed with trolamine, ethylene glycol, water-soluble amide by end carboxyl bromine carbon polyester resin, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol carry out being mixed into magma, mixing adding magma after methyl silicon sodium alcoholate, Tai-Ace S 150 mixing preparation, finally melt extruding through forcing machine successively, pulverize and obtain coating.
Embodiment three
A kind of frost climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 83 parts, trolamine 3.7 parts, trimeric cyanamide 12 parts, titanium dioxide 7 parts, pearlstone 10 parts, Natvosol 9 parts, methyl silicon sodium alcoholate 4 parts, 5 parts, Tai-Ace S 150, ethylene glycol 16 parts, water-soluble amide 7 parts.Preparation method comprises the following steps: first mixed with trolamine, ethylene glycol, water-soluble amide by end carboxyl bromine carbon polyester resin, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol carry out being mixed into magma, mixing adding magma after methyl silicon sodium alcoholate, Tai-Ace S 150 mixing preparation, finally melt extruding through forcing machine successively, pulverize and obtain coating.

Claims (4)

1. a frost climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 80-90 part, trolamine 3.5-4 part, trimeric cyanamide 10-15 part, titanium dioxide 5-10 part, pearlstone 8-14 part, Natvosol 8-12 part, methyl silicon sodium alcoholate 3-6 part, Tai-Ace S 150 4-7 part, ethylene glycol 15-20 part, water-soluble amide 5-8 part.
2. a frost climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 80-85 part, trolamine 3.5-4 part, trimeric cyanamide 10-15 part, titanium dioxide 5-10 part, pearlstone 8-14 part, Natvosol 8-12 part, methyl silicon sodium alcoholate 3-6 part, Tai-Ace S 150 4-7 part, ethylene glycol 15-20 part, water-soluble amide 5-8 part.
3. a frost climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 83 parts, trolamine 3.7 parts, trimeric cyanamide 12 parts, titanium dioxide 7 parts, pearlstone 10 parts, Natvosol 9 parts, methyl silicon sodium alcoholate 4 parts, 5 parts, Tai-Ace S 150, ethylene glycol 16 parts, water-soluble amide 7 parts.
4. the preparation method of a frost climate end carboxyl bromine carbon polyester resin frie retardant coating, comprise the following steps: first end carboxyl bromine carbon polyester resin is mixed with trolamine, ethylene glycol, water-soluble amide, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol carry out being mixed into magma, mixing adding magma after methyl silicon sodium alcoholate, Tai-Ace S 150 mixing preparation, finally melt extruding through forcing machine successively, pulverize and obtain coating.
CN201410741578.2A 2014-12-09 2014-12-09 Freezing weather end carboxyl bromine carbon polyester resin fire-retardant coating and preparation method thereof Pending CN104449261A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410741578.2A CN104449261A (en) 2014-12-09 2014-12-09 Freezing weather end carboxyl bromine carbon polyester resin fire-retardant coating and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410741578.2A CN104449261A (en) 2014-12-09 2014-12-09 Freezing weather end carboxyl bromine carbon polyester resin fire-retardant coating and preparation method thereof

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CN104449261A true CN104449261A (en) 2015-03-25

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106118483A (en) * 2016-07-18 2016-11-16 张和庆 Under a kind of low temperature environment, clutch surface sheet stock is with soaking coating processed

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1380370A (en) * 2002-03-25 2002-11-20 葛明槽 Fire-resistant powder coating material and its production process
CN101255310A (en) * 2007-09-11 2008-09-03 兰州理工大学 Powder fire-proof paint containing bromine-carbon polyester and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1380370A (en) * 2002-03-25 2002-11-20 葛明槽 Fire-resistant powder coating material and its production process
CN101255310A (en) * 2007-09-11 2008-09-03 兰州理工大学 Powder fire-proof paint containing bromine-carbon polyester and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106118483A (en) * 2016-07-18 2016-11-16 张和庆 Under a kind of low temperature environment, clutch surface sheet stock is with soaking coating processed

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Application publication date: 20150325

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