CN104479511A - Carboxyl-terminated bromine carbon polyester resin fire-retardant coating used in desert climate and preparation method of fire-retardant coating - Google Patents

Carboxyl-terminated bromine carbon polyester resin fire-retardant coating used in desert climate and preparation method of fire-retardant coating Download PDF

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Publication number
CN104479511A
CN104479511A CN201410741041.6A CN201410741041A CN104479511A CN 104479511 A CN104479511 A CN 104479511A CN 201410741041 A CN201410741041 A CN 201410741041A CN 104479511 A CN104479511 A CN 104479511A
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China
Prior art keywords
parts
polyester resin
retardant coating
bromine carbon
carbon polyester
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Pending
Application number
CN201410741041.6A
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Chinese (zh)
Inventor
张和庆
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TAIXING HEQING MACHINERY FITTINGS FACTORY
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TAIXING HEQING MACHINERY FITTINGS FACTORY
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Priority to CN201410741041.6A priority Critical patent/CN104479511A/en
Publication of CN104479511A publication Critical patent/CN104479511A/en
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/02—Flame or fire retardant/resistant

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Paints Or Removers (AREA)
  • Laminated Bodies (AREA)

Abstract

The invention relates to a carboxyl-terminated bromine carbon polyester resin fire-retardant coating used in desert climate and a preparation method of the fire-retardant coating. The carboxyl-terminated bromine carbon polyester resin fire-retardant coating is prepared from the following raw materials in parts by mass: 80-90 parts of carboxyl-terminated bromine carbon polyester resin, 3.5-4 parts of triethanolamine, 10-15 parts of melamine, 5-10 parts of titanium dioxide, 8-14 parts of expanded perlite, 8-12 parts of hydroxyethyl cellulose, 2-8 parts of an ionic chain extender capable of forming hydrophilic groups and having an active hydrogen and 1-10 parts of a silane coupling agent. The preparation method comprises the following steps of firstly mixing carboxyl-terminated bromine carbon polyester resin, triethanolamine, the ionic chain extender capable of forming hydrophilic groups and having activated hydrogen and the silane coupling agent, adding and mixing melamine, titanium dioxide, expanded perlite and hydroxyethyl cellulose and sequentially carrying out melt extrusion by virtue of an extruder and grinding to obtain the coating.

Description

A kind of desert climate end carboxyl bromine carbon polyester resin frie retardant coating and preparation method
Technical field
The present invention relates to a kind of frie retardant coating, is a kind of desert climate end carboxyl bromine carbon polyester resin frie retardant coating and preparation method thereof specifically.
Background technology
Polyester powder coating has good physical and mechanical properties; decoration and the protection of metallic surface can be widely used in; equipment requires that coating is prevented fires, high temperature resistant, resistance to weathering is higher under desert climate; polyester powder coating on existing market is excellent performance in fire prevention mostly only, but cannot meet the use of desert climate particular requirement.
Summary of the invention
For above-mentioned deficiency of the prior art, the invention provides a kind of easily manufactured, cost is low, fire prevention, high temperature resistant, the good a kind of desert climate end carboxyl bromine carbon polyester resin frie retardant coating of resistance to weathering and preparation method.
The technical solution used in the present invention is: a kind of desert climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 80-90 part, trolamine 3.5-4 part, trimeric cyanamide 10-15 part, titanium dioxide 5-10 part, pearlstone 8-14 part, Natvosol 8-12 part, can form ionic chainextender 2-8 part, silane coupling agent 1-10 part that hydrophilic radical has active hydrogen.
A kind of preparation method of desert climate end carboxyl bromine carbon polyester resin frie retardant coating, comprise the following steps: first by end carboxyl bromine carbon polyester resin and trolamine, can form that hydrophilic radical has the ionic chainextender of active hydrogen, silane coupling agent mixes, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol mix, finally melt extrude through forcing machine successively, pulverize and obtain coating.
The present invention adds trolamine, trimeric cyanamide, titanium dioxide, pearlstone, Natvosol in end carboxyl bromine carbon polyester resin, be equipped with and can form the ionic chainextender that hydrophilic radical has active hydrogen, fire prevention, high temperature resistant, resistance to weathering can be taken into account, Special use requirement under applicable desert climate.
Embodiment
Below in conjunction with embodiment, the invention will be further described.
Embodiment one
A kind of desert climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 80 parts, trolamine 3.5 parts, trimeric cyanamide 10 parts, titanium dioxide 5 parts, pearlstone 8 parts, Natvosol 8 parts, can form ionic chainextender 2 parts, silane coupling agent 1 part that hydrophilic radical has active hydrogen.Preparation method comprises the following steps: first by end carboxyl bromine carbon polyester resin and trolamine, can form that hydrophilic radical has the ionic chainextender of active hydrogen, silane coupling agent mixes, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol mix, finally melt extrude through forcing machine successively, pulverize and obtain coating.
Embodiment two
A kind of desert climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 90 parts, trolamine 4 parts, trimeric cyanamide 15 parts, titanium dioxide 10 parts, pearlstone 14 parts, Natvosol 12 parts, can form ionic chainextender 8 parts, silane coupling agent 10 parts that hydrophilic radical has active hydrogen.Preparation method comprises the following steps: first by end carboxyl bromine carbon polyester resin and trolamine, can form that hydrophilic radical has the ionic chainextender of active hydrogen, silane coupling agent mixes, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol mix, finally melt extrude through forcing machine successively, pulverize and obtain coating.
Embodiment three
A kind of desert climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 84 parts, trolamine 3.9 parts, trimeric cyanamide 14 parts, titanium dioxide 9 parts, pearlstone 13 parts, Natvosol 11 parts, can form ionic chainextender 6 parts, silane coupling agent 8 parts that hydrophilic radical has active hydrogen.Preparation method comprises the following steps: first by end carboxyl bromine carbon polyester resin and trolamine, can form that hydrophilic radical has the ionic chainextender of active hydrogen, silane coupling agent mixes, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol mix, finally melt extrude through forcing machine successively, pulverize and obtain coating.

Claims (4)

1. a desert climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 80-90 part, trolamine 3.5-4 part, trimeric cyanamide 10-15 part, titanium dioxide 5-10 part, pearlstone 8-14 part, Natvosol 8-12 part, can form ionic chainextender 2-8 part, silane coupling agent 1-10 part that hydrophilic radical has active hydrogen.
2. a desert climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 80-84 part, trolamine 3.5-4 part, trimeric cyanamide 10-15 part, titanium dioxide 5-10 part, pearlstone 8-14 part, Natvosol 8-12 part, can form ionic chainextender 2-8 part, silane coupling agent 1-10 part that hydrophilic radical has active hydrogen.
3. a desert climate end carboxyl bromine carbon polyester resin frie retardant coating, is made up of in mass ratio following raw materials according: end carboxyl bromine carbon polyester resin 84 parts, trolamine 3.9 parts, trimeric cyanamide 14 parts, titanium dioxide 9 parts, pearlstone 13 parts, Natvosol 11 parts, can form ionic chainextender 6 parts, silane coupling agent 8 parts that hydrophilic radical has active hydrogen.
4. the preparation method of a desert climate end carboxyl bromine carbon polyester resin frie retardant coating, comprise the following steps: first by end carboxyl bromine carbon polyester resin and trolamine, can form that hydrophilic radical has the ionic chainextender of active hydrogen, silane coupling agent mixes, add trimeric cyanamide again, titanium dioxide, pearlstone, Natvosol mix, finally melt extrude through forcing machine successively, pulverize and obtain coating.
CN201410741041.6A 2014-12-09 2014-12-09 Carboxyl-terminated bromine carbon polyester resin fire-retardant coating used in desert climate and preparation method of fire-retardant coating Pending CN104479511A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410741041.6A CN104479511A (en) 2014-12-09 2014-12-09 Carboxyl-terminated bromine carbon polyester resin fire-retardant coating used in desert climate and preparation method of fire-retardant coating

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410741041.6A CN104479511A (en) 2014-12-09 2014-12-09 Carboxyl-terminated bromine carbon polyester resin fire-retardant coating used in desert climate and preparation method of fire-retardant coating

Publications (1)

Publication Number Publication Date
CN104479511A true CN104479511A (en) 2015-04-01

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Application Number Title Priority Date Filing Date
CN201410741041.6A Pending CN104479511A (en) 2014-12-09 2014-12-09 Carboxyl-terminated bromine carbon polyester resin fire-retardant coating used in desert climate and preparation method of fire-retardant coating

Country Status (1)

Country Link
CN (1) CN104479511A (en)

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