CN104449161A - 硅溶胶型石材防水剂生产工艺 - Google Patents

硅溶胶型石材防水剂生产工艺 Download PDF

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CN104449161A
CN104449161A CN201310440056.4A CN201310440056A CN104449161A CN 104449161 A CN104449161 A CN 104449161A CN 201310440056 A CN201310440056 A CN 201310440056A CN 104449161 A CN104449161 A CN 104449161A
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water
agent
waterproofing agent
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film
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李继升
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Qingdao Shousheng Industrial Co Ltd
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Qingdao Shousheng Industrial Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04—Homopolymers or copolymers of esters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/16—Antifouling paints; Underwater paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
    • C04B2103/60—Agents for protection against chemical, physical or biological attack
    • C04B2103/65—Water proofers or repellants
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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  • Paints Or Removers (AREA)

Abstract

本发明公开了一种硅溶胶型石材防水剂生产工艺，将石蜡粉碎成小块，加热熔融，加入复配的表面活性剂和热水，在85℃和1000r/min搅拌速度下乳化，快速冷却后再加入消泡剂和pH调节剂，搅拌均匀，即制得石蜡乳液。在搅拌下将水、硅溶胶、石蜡乳液、消泡剂、成膜助剂混合均匀，然后加入计量的纯丙乳液并搅拌均匀，最后加入消泡剂消泡，制得防水剂成品。成膜后既提高了涂膜的附着力，又可增加涂膜的韧性，大幅度提高该类涂料的性价比。粒径为纳米级的硅溶胶在高分子乳液基料中的良好分散，可以提高高分子乳胶膜的耐水性和耐沾污性，有利于提高石材防水剂的防水性能。

Description

硅溶胶型石材防水剂生产工艺
 
技术领域
本发明属于防水剂生产工艺，具体涉及一种硅溶胶型石材防水剂生产工艺。
 
背景技术
各类石材及石雕工艺品是现代装饰中的高档建材产品，但在使用过程中由于长期暴露在大气中，经受较为苛刻的恶劣环境条件，比如严寒、潮湿和酸雨等，其表面会出现不同程度的风化和锈蚀，需对其表面涂饰防水剂，以提高石材及石雕工艺品的耐候性和耐水性。恶劣大气环境对涂饰防水剂的性能要求很高，现有涂料涂膜的耐水性、耐老化性和耐沾污性还存在不足。
 
发明内容
为了克服现有技术领域存在的上述缺陷，本发明的目的在于，提供一种硅溶胶型石材防水剂生产工艺，生产的防水剂耐水性、耐老化性和耐沾污性好。
本发明提供的硅溶胶型石材防水剂生产工艺，生产工艺如下：
a.石蜡乳液的配置：将石蜡粉碎成小块，加热熔融，加入复配的表面活性剂和热水，在85℃和1000 r/min搅拌速度下乳化，快速冷却后再加入消泡剂和pH 调节剂，搅拌均匀，即制得石蜡乳液；
b.涂饰防水剂的制备：在搅拌下将水、硅溶胶、石蜡乳液、消泡剂、成膜助剂混合均匀，然后加入计量的纯丙乳液并搅拌均匀，最后加入消泡剂消泡，制得防水剂成品。
本发明提供的硅溶胶型石材防水剂生产工艺，其有益效果在于，硅溶胶分子表面具有羟基，在硅溶胶- 乳液复合涂料中，水性硅溶胶粒子分散于有机高分子乳液中，成膜后既提高了涂膜的附着力，又可增加涂膜的韧性，大幅度提高该类涂料的性价比。粒径为纳米级的硅溶胶在高分子乳液基料中的良好分散，可以提高高分子乳胶膜的耐水性和耐沾污性，有利于提高石材防水剂的防水性能。
具体实施方式
下面结合一个实施例，对本发明提供的硅溶胶型石材防水剂生产工艺进行详细的说明。
 
实施例
生产工艺如下：
a.石蜡乳液的配置：将石蜡粉碎成小块，加热熔融，加入复配的表面活性剂和热水，在85℃和1000 r/min搅拌速度下乳化，快速冷却后再加入消泡剂和pH 调节剂，搅拌均匀，即制得石蜡乳液；
b.涂饰防水剂的制备：在搅拌下将水、硅溶胶、石蜡乳液、消泡剂、成膜助剂混合均匀，然后加入计量的纯丙乳液并搅拌均匀，最后加入消泡剂消泡，制得防水剂成品。

Claims (1)

1.一种硅溶胶型石材防水剂生产工艺，其特征在于：生产工艺如下： 
a.石蜡乳液的配置：将石蜡粉碎成小块，加热熔融，加入复配的表面活性剂和热水，在85℃和1000 r/min搅拌速度下乳化，快速冷却后再加入消泡剂和pH 调节剂，搅拌均匀，即制得石蜡乳液；
b.涂饰防水剂的制备：在搅拌下将水、硅溶胶、石蜡乳液、消泡剂、成膜助剂混合均匀，然后加入计量的纯丙乳液并搅拌均匀，最后加入消泡剂消泡，制得防水剂成品。
CN201310440056.4A 2013-09-25 2013-09-25 硅溶胶型石材防水剂生产工艺 Pending CN104449161A (zh)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105199512A (zh) * 2015-10-08 2015-12-30 鹤山市顺鑫实业有限公司 一种水性疏水剂及其制备方法
CN108410275A (zh) * 2018-03-23 2018-08-17 常德市万福达环保节能建材有限公司 一种透明防污防水涂料及其制备方法
CN109943082A (zh) * 2019-04-16 2019-06-28 北京林业大学 一种含有氧化物固体颗粒的石蜡乳液防水剂及其制备方法
CN110527385A (zh) * 2019-09-12 2019-12-03 广州迪瑞夫建筑材料有限公司 一种用于水泥基地坪的抛光助剂
CN112266670A (zh) * 2020-10-28 2021-01-26 石家庄日加精细矿物制品有限公司 一种提高颗粒抗污性的涂料
CN113956729A (zh) * 2021-11-17 2022-01-21 上海阿宝实业有限公司 一种防水抗渗涂料及其制备方法

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105199512A (zh) * 2015-10-08 2015-12-30 鹤山市顺鑫实业有限公司 一种水性疏水剂及其制备方法
CN105199512B (zh) * 2015-10-08 2017-08-25 鹤山市顺鑫实业有限公司 一种水性疏水剂及其制备方法
CN108410275A (zh) * 2018-03-23 2018-08-17 常德市万福达环保节能建材有限公司 一种透明防污防水涂料及其制备方法
CN109943082A (zh) * 2019-04-16 2019-06-28 北京林业大学 一种含有氧化物固体颗粒的石蜡乳液防水剂及其制备方法
CN109943082B (zh) * 2019-04-16 2021-05-28 北京林业大学 一种含有氧化物固体颗粒的石蜡乳液防水剂及其制备方法
CN110527385A (zh) * 2019-09-12 2019-12-03 广州迪瑞夫建筑材料有限公司 一种用于水泥基地坪的抛光助剂
CN112266670A (zh) * 2020-10-28 2021-01-26 石家庄日加精细矿物制品有限公司 一种提高颗粒抗污性的涂料
CN113956729A (zh) * 2021-11-17 2022-01-21 上海阿宝实业有限公司 一种防水抗渗涂料及其制备方法

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Application publication date: 20150325