CN104448901A - Method for extracting capsanthin ointment - Google Patents
Method for extracting capsanthin ointment Download PDFInfo
- Publication number
- CN104448901A CN104448901A CN201310431185.7A CN201310431185A CN104448901A CN 104448901 A CN104448901 A CN 104448901A CN 201310431185 A CN201310431185 A CN 201310431185A CN 104448901 A CN104448901 A CN 104448901A
- Authority
- CN
- China
- Prior art keywords
- extraction
- extracting
- capsicum
- particulate material
- capsanthin ointment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
Abstract
The invention relates to a method for extracting a natural pigment, and concretely relates to a method for extracting a capsanthin ointment. The method comprises the following steps: processing dry paprika powder with no molds to form particles with the diameter phi of 2-6mm, and adding the particles into an extraction container; extracting the particle raw material with dimethyl ether as a solvent, carrying out solid-liquid separation after the extraction, and repeatedly extracting the separated solid phase 1-10 times; and filtering or settling the obtained liquid phase to remove fine impurities in the liquid phase, carrying out reduced pressure separation to obtain a gas phase and a concentrate, and removing water and volatile matters from the concentrate at a temperature of 20-50DEG C under a gauge pressure of below -0.085MPa to prepare the capsanthin ointment. The method allows the capsanthin ointment to be extracted without raw material kind restriction, has the advantages of full utilization of the raw material resource, high extraction rate, low residue residual and light color of capsicum meal, is suitable for capsicum with low pungency degree, and is more suitable for capsicum with high pungency degree. The method has a low production cost obvious market competition advantage.
Description
Technical field
The present invention relates to a kind of extracting method of natural pigment, relate in particular to the extracting method of capsanthin ointment.
Background technology
Red pepper is a kind of common agricultural-food, wherein containing capsicine (pungent element), natural red colouring matter etc.Low pungent element is as seasonings, and height pungent element has analgesia, anti-inflammatory, germicidal action; Capsanthin is natural haematochrome, can be used for medicine or superior cosmetics industry, without any side effects.At present, the method extracting capsanthin ointment from red pepper mainly contains: normal hexane extraction method (CN1082570A); Ethonal extraction method (CN1053803A) etc., owing to selecting the difference of raw material of hot pepper or use solvent, the mix ingredients extracted is not identical with quantity yet, the large chili meal blackening of the chili meal water content obtained or peppery haematochrome extract not exclusively, yield is lower, and cost is higher.
Summary of the invention
The object of the present invention is to provide a kind of extracting method of capsanthin ointment, with dme as solvent extraction capsicum, improve capsanthin ointment yield, make that chili meal slag is residual to be reduced greatly, reduce costs.
Extract a method for capsanthin ointment, comprise the following steps:
(1) prepare capsicum particulate material: the particulate material caused after the chilli that nothing is gone mouldy is ground into the powder of 20 ~ 60 order φ 2 ~ 6mm, put in extraction vessel;
(2) extract: be that solvent extracts particulate material with dme, the weight ratio of particulate material and solvent is 1: 0.8 ~ 6, and Extracting temperature is 10 ~ 45 DEG C, and extraction time is 10 ~ 60min; Carry out solid-liquid separation after extraction terminates, repeat extraction 2 ~ 8 times to the solid phase be separated by said extracted processing condition, the solid phase after extracting is chili meal;
(3) recycling design: the liquid phase that (2) are separated is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied recycling design;
(4) product separation: the enriched material control temperature (3) be separated is at 20 ~ 50 DEG C, and gauge pressure removes moisture and volatile matter content under being less than the condition of-0.085Mpa, obtains capsanthin ointment.
Use method of the present invention to extract capsanthin ointment, do not limit by raw material variety, can make full use of raw material resources, extraction yield is high, slag is residual low, the lighter color of chili meal, is not only applicable to the capsicum of low pungent degree, be more suitable for the capsicum of high pungent degree, production cost is low, and market competition advantage is obvious.
4, embodiment
Illustrate below and realize technical process of the present invention and implementation:
(1), technical process
Step 1, preparation capsicum particulate material: the particle caused after the chilli that nothing is gone mouldy being ground into the powder of 20 ~ 60 order φ 2 ~ 6mm with machine;
Step 2, extraction: by the capsicum particulate material prepared according to step 1, put in extraction container through weighing, take dme as solvent, capsicum particulate material is extracted, wherein, the weight ratio of particulate material and solvent is 1: 0.8 ~ 6, and Extracting temperature is 10 ~ 45 DEG C, and extraction time is 10 ~ 60min; Carry out solid-liquid separation after extraction terminates, repeat extraction 1 ~ 10 time to the solid phase be separated by above-mentioned processing condition, the solid phase after extracting is chili meal;
Step 3, recycling design: the liquid phase be separated from step 2 is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied recycling design;
Step 4, product separation: to the enriched material be separated from step 3, control temperature, at 20 ~ 50 DEG C, removes moisture and volatile matter content enriched material is less than the condition of-0.085Mpa in gauge pressure under, just obtains capsanthin ointment.
Described operating process all completes under complete totally enclosed processing condition.
(2), implementation
Method of the present invention is further illustrated below by embodiment:
Embodiment 1: get the capsicum particulate material 100kg prepared according to step 1 in above-mentioned technical process, be placed in extraction container, add 80kg dme, Extracting temperature is 45 DEG C, and extraction time is 60min; Carry out solid-liquid separation after extraction terminates, repeat extraction 2 ~ 8 times to the solid phase be separated by above-mentioned processing condition, the solid phase after repeatedly extracting is chili meal; Filter or sedimentation liquid phase, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied recycling design;
By enriched material control temperature at 20 ~ 50 DEG C, gauge pressure removes moisture and volatile matter content under being less than the condition of-0.085Mpa, just obtains capsanthin ointment.
Embodiment 2: get the capsicum particulate material 100kg prepared according to step 1 in above-mentioned technical process, be placed in extraction container, add 600kg dme, Extracting temperature is 10 DEG C, and extraction time is 10min; Carry out solid-liquid separation after extraction terminates, repeat extraction 2 times to the solid phase be separated by above-mentioned processing condition, the solid phase after extracting is chili meal; Filter or sedimentation liquid phase, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied recycling design; By enriched material control temperature at 20 ~ 50 DEG C, gauge pressure removes moisture and volatile matter content under being less than the condition of-0.085MPa, just obtains capsanthin ointment.
Embodiment 3: get the capsicum particulate material 100kg prepared according to step 1 in above-mentioned technical process, be placed in extraction container, add 300kg dme, Extracting temperature is 30 DEG C, and extraction time is 30min; Carry out solid-liquid separation after extraction terminates, repeat extraction 4 times to the solid phase be separated by above-mentioned processing condition, the solid phase after extracting is chili meal; Filter or sedimentation liquid phase, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied recycling design; By enriched material control temperature at 20 ~ 50 DEG C, gauge pressure removes moisture and volatile matter content under being less than the condition of-0.085MPa, just obtains capsanthin ointment.
Embodiment 4: get the capsicum particulate material 100kg prepared according to step 1 in above-mentioned technical process, be placed in extraction container, add 100kg dme, Extracting temperature is 35 DEG C, and extraction time is 40min; Carry out solid-liquid separation after extraction terminates, repeat extraction 5 times to the solid phase be separated by above-mentioned processing condition, the solid phase after extracting is chili meal; Filter or sedimentation liquid phase, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied recycling design; By enriched material control temperature at 20 ~ 50 DEG C, gauge pressure removes moisture and volatile matter content under being less than the condition of-0.085MPa, just obtains capsanthin ointment.
Embodiment 5: get the capsicum particulate material 100kg prepared according to step 1 in above-mentioned technical process, be placed in extraction container, add 200kg dme, Extracting temperature is 45 DEG C, and extraction time is 50min; Carry out solid-liquid separation after extraction terminates, repeat extraction 5 times to the solid phase be separated by above-mentioned processing condition, the solid phase after extracting is chili meal; Filter or sedimentation liquid phase, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied recycling design; By enriched material control temperature at 20 ~ 50 DEG C, gauge pressure removes moisture and volatile matter content under being less than the condition of-0.085MPa, just obtains capsanthin ointment.
Claims (3)
1. extract a method for capsanthin ointment, it is characterized in that:
(1) prepare capsicum particulate material: the particulate material caused after the chilli that nothing is gone mouldy is ground into 20 ~ 60 object φ 2 ~ 6mm powder, put in extraction vessel;
(2) extract: be that solvent extracts particulate material with dme, the weight ratio of particulate material and solvent is 1: 0.8 ~ 6, and Extracting temperature is 10 ~ 45 DEG C, and extraction time is 10 ~ 60min; Carry out solid-liquid separation after extraction terminates, repeat extraction 1 ~ 10 time to the solid phase be separated by said extracted processing condition, the solid phase after extracting is chili meal;
(3) recycling design: the liquid phase that (2) are separated is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied recycling design;
(4) product separation: the enriched material control temperature (3) be separated is at 20 ~ 50 DEG C, and gauge pressure removes moisture and volatile matter content under being less than the condition of-0.085Mpa, obtains capsanthin ointment.
2. according to the method for the extraction capsanthin ointment described in claim 1, it is characterized in that: the weight ratio of described capsicum particulate material and solvent is 1: 0.8 ~ 3, Extracting temperature is 20 ~ 45 DEG C, and extraction time is 20 ~ 50min, and repeating extraction time is 3 ~ 5 times.
3. according to the method for the extraction capsanthin ointment described in claim 1, it is characterized in that: the temperature that described product separation controls enriched material is 20 ~ 50 DEG C, and gauge pressure removes moisture and volatile matter content under being less than the condition of-0.085Mpa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310431185.7A CN104448901A (en) | 2013-09-22 | 2013-09-22 | Method for extracting capsanthin ointment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310431185.7A CN104448901A (en) | 2013-09-22 | 2013-09-22 | Method for extracting capsanthin ointment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104448901A true CN104448901A (en) | 2015-03-25 |
Family
ID=52895686
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310431185.7A Pending CN104448901A (en) | 2013-09-22 | 2013-09-22 | Method for extracting capsanthin ointment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104448901A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110713733A (en) * | 2019-10-29 | 2020-01-21 | 四川常青调正食品有限责任公司 | Process for separating capsanthin from hot pepper |
| CN113930161A (en) * | 2021-10-29 | 2022-01-14 | 晨光生物科技集团股份有限公司 | Pepper oleoresin and preparation method and application thereof |
-
2013
- 2013-09-22 CN CN201310431185.7A patent/CN104448901A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110713733A (en) * | 2019-10-29 | 2020-01-21 | 四川常青调正食品有限责任公司 | Process for separating capsanthin from hot pepper |
| CN113930161A (en) * | 2021-10-29 | 2022-01-14 | 晨光生物科技集团股份有限公司 | Pepper oleoresin and preparation method and application thereof |
| CN113930161B (en) * | 2021-10-29 | 2023-03-07 | 晨光生物科技集团股份有限公司 | Pepper oleoresin and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102408320B (en) | Method for extracting and separating curcumin and curcuma oil from carcuma longa | |
| CN102250195B (en) | Method for producing xanthoceraside | |
| CN102911095A (en) | Method for supercritical CO2 extraction of effective ingredients of Haematococcus pluvialis spore powder | |
| CN103494862B (en) | Method for extracting olive polyphenol from olive processing waste liquor | |
| CN103211219B (en) | Health food for relieving physical fatigue and preparation method thereof | |
| CN102965198A (en) | Method for extracting and processing lavender essential oil | |
| CN103896901A (en) | Method for extracting purified anthocyanin from purple sweet potatoes | |
| CN102311660B (en) | Production method of gardenia yellow pigment | |
| CN101906254A (en) | Method for extracting capsaicin ointment from dimethyl ether | |
| CN110105257A (en) | A kind of synchronous industrial method for extracting lutein and quercetagetin | |
| CN102660137A (en) | Method for high-efficiency preparation of natural pigment of Ziziphus jujuba Mill. | |
| CN102964866A (en) | Method for extracting perilla color from perilla leaves | |
| CN101696327B (en) | Method for removing phospholipid from capsanthin by using low-molecular-weight fatty acid as entrainer | |
| CN106417783A (en) | Preparation methods of Fu tea instant tea powder and double-layer compound Fu tea instant tea tablets | |
| CN104448901A (en) | Method for extracting capsanthin ointment | |
| CN105777699A (en) | Preparation method of black rice anthocyanin without pesticide residue | |
| CN101831198B (en) | Preparation method of capsanthin | |
| CN111848362A (en) | Method for preparing high-purity cannabidiol by combining ultrasonic extraction with dynamic axial compression column system | |
| CN101628857B (en) | Production technique for extracting resveratrol from giant knotweed | |
| CN113430053A (en) | Fresh pepper oleoresin separation and purification process | |
| CN105131841B (en) | A kind of extracting method of capsicum oleoresin | |
| CN102659792A (en) | Method for extracting chlorophyll from clovers | |
| CN102604421A (en) | Gardenia yellow pigment extracting process | |
| CN105295426A (en) | Capsanthin ointment extraction method | |
| CN103695179A (en) | Production process method of cinnamon volatile oil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150325 |