CN101906254A - Method for extracting capsaicin ointment from dimethyl ether - Google Patents
Method for extracting capsaicin ointment from dimethyl ether Download PDFInfo
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- CN101906254A CN101906254A CN2010102372602A CN201010237260A CN101906254A CN 101906254 A CN101906254 A CN 101906254A CN 2010102372602 A CN2010102372602 A CN 2010102372602A CN 201010237260 A CN201010237260 A CN 201010237260A CN 101906254 A CN101906254 A CN 101906254A
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- Prior art keywords
- extraction
- extracting
- solvent
- ointment
- particulate material
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 239000002674 ointment Substances 0.000 title claims abstract description 22
- 238000000034 method Methods 0.000 title claims abstract description 20
- YKPUWZUDDOIDPM-SOFGYWHQSA-N capsaicin Chemical compound COC1=CC(CNC(=O)CCCC\C=C\C(C)C)=CC=C1O YKPUWZUDDOIDPM-SOFGYWHQSA-N 0.000 title claims abstract description 19
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 title claims abstract description 14
- 229960002504 capsaicin Drugs 0.000 title claims abstract description 9
- 235000017663 capsaicin Nutrition 0.000 title claims abstract description 9
- 238000000605 extraction Methods 0.000 claims abstract description 32
- 238000000926 separation method Methods 0.000 claims abstract description 21
- 239000002904 solvent Substances 0.000 claims abstract description 20
- 239000000463 material Substances 0.000 claims abstract description 19
- 239000012071 phase Substances 0.000 claims abstract description 17
- 239000007790 solid phase Substances 0.000 claims abstract description 17
- 239000007791 liquid phase Substances 0.000 claims abstract description 10
- 239000012535 impurity Substances 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims abstract description 4
- 240000008574 Capsicum frutescens Species 0.000 claims description 28
- 235000002566 Capsicum Nutrition 0.000 claims description 26
- 239000001390 capsicum minimum Substances 0.000 claims description 26
- 239000011236 particulate material Substances 0.000 claims description 18
- VYIRVAXUEZSDNC-TXDLOWMYSA-N (3R,3'S,5'R)-3,3'-dihydroxy-beta-kappa-caroten-6'-one Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC(=O)[C@]1(C)C[C@@H](O)CC1(C)C VYIRVAXUEZSDNC-TXDLOWMYSA-N 0.000 claims description 14
- VYIRVAXUEZSDNC-LOFNIBRQSA-N Capsanthyn Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CC(O)CC2(C)C VYIRVAXUEZSDNC-LOFNIBRQSA-N 0.000 claims description 14
- WRANYHFEXGNSND-LOFNIBRQSA-N capsanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CCC(O)C2(C)C WRANYHFEXGNSND-LOFNIBRQSA-N 0.000 claims description 14
- 235000018889 capsanthin Nutrition 0.000 claims description 14
- 235000012658 paprika extract Nutrition 0.000 claims description 14
- 239000001688 paprika extract Substances 0.000 claims description 14
- 235000007164 Oryza sativa Nutrition 0.000 claims description 12
- 235000009566 rice Nutrition 0.000 claims description 12
- 238000002360 preparation method Methods 0.000 claims description 9
- 238000011084 recovery Methods 0.000 claims description 9
- 230000006837 decompression Effects 0.000 claims description 8
- 238000004062 sedimentation Methods 0.000 claims description 8
- 239000000284 extract Substances 0.000 claims description 5
- 240000007594 Oryza sativa Species 0.000 claims 1
- 235000002568 Capsicum frutescens Nutrition 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 5
- 239000002245 particle Substances 0.000 abstract description 3
- 239000002893 slag Substances 0.000 abstract description 3
- 238000001914 filtration Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000000049 pigment Substances 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
- 239000012141 concentrate Substances 0.000 abstract 2
- 235000019617 piquancy Nutrition 0.000 abstract 2
- 235000012054 meals Nutrition 0.000 abstract 1
- 241000209094 Oryza Species 0.000 description 11
- 240000004160 Capsicum annuum Species 0.000 description 4
- 235000008534 Capsicum annuum var annuum Nutrition 0.000 description 2
- 235000007862 Capsicum baccatum Nutrition 0.000 description 2
- 239000001728 capsicum frutescens Substances 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 239000004278 EU approved seasoning Substances 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 230000036592 analgesia Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
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- Medicinal Preparation (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
The invention relates to an extraction method of natural pigments, in particular to an extraction method of a capsaicin ointment. The extraction method comprises the following steps of: putting particles made by mildew-free dried chili powder into an extraction container; carrying out extraction on raw particle materials by taking dimethyl ether as a solvent, carrying out solid-liquid separation after extraction, and carrying out repeated extraction 2 to 8 times on separated solid phase; and carrying out filtration or settlement on liquid phase, removing tiny impurities in the liquid phase, decompressing and separating into gas phase and concentrate, controlling the temperature of the concentrate to 20 to 50 DEG C, removing water and volatile matters under the condition that the gauge pressure is less than -0.085Mpa, and preparing the capsaicin ointment. The capsaicin ointment extracted by using the method is not limited by species of raw materials and capable of fully utilizing raw material resources, has high extraction ratio, low slag residual, light color of chili meal, low production cost and remarkable market competition advantage, and is not only suitable for chili with low piquancy degree, but also suitable for chili with high piquancy degree.
Description
Technical field
The present invention relates to a kind of extraction method of natural pigments, relate in particular to the extracting method of capsanthin ointment.
Background technology
Red pepper is a kind of common agricultural-food, wherein contains capsicine (pungent element), natural red colouring matter etc.Low pungent element is as seasonings, and height pungent element has analgesia, anti-inflammatory, germicidal action; Capsanthin is natural haematochrome, can be used for medicine or superior cosmetics industry, and is without any side effects.At present, the method for extraction capsanthin ointment mainly contains from red pepper: normal hexane extraction method (CN1082570A); Alcohol solvent extraction method (CN1053803A) etc., owing to select the difference of raw material of hot pepper or use solvent for use, mix ingredients and the quantity extracted are also inequality, big capsicum dregs of rice blackening of resulting capsicum dregs of rice water content or peppery haematochrome extract not exclusively, yield is lower, and cost is higher.
Summary of the invention
The object of the present invention is to provide a kind of extracting method of capsanthin ointment, as the solvent extraction capsicum, improve capsanthin ointment yield, make the residual reduction greatly of capsicum dregs of rice slag, reduce cost with dme.
The method of extracting capsaicin ointment from dimethyl ether may further comprise the steps:
(1) preparation capsicum particulate material: cause after the chilli that nothing is gone mouldy is ground into 20～60 purpose powder
Particulate material, put in the extraction vessel;
(2) extract: with the dme is that solvent extracts particulate material, and the weight ratio of particulate material and solvent is 1: 0.8～6, and extracting temperature is 10～45 ℃, and extraction time is 10～60min; Carry out solid-liquid separation after extracting end, isolating solid phase is repeated to extract 2～8 times by the said extracted processing condition, the solid phase after extracting is the capsicum dregs of rice;
(3) reclaim solvent: (2) isolating liquid phase is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied the recovery solvent;
(4) product separation: (3) isolating enriched material controlled temperature at 20～50 ℃, under the condition of gauge pressure less than-0.085Mpa, is removed moisture and volatile matter content, obtain the capsanthin ointment.
Use method of the present invention to extract the capsanthin ointment, not limited by raw material variety, can make full use of raw material resources, the extraction yield height, slag is residual low, the lighter color of the capsicum dregs of rice, the capsicum that not only is fit to hang down the pungent degree, be more suitable for the capsicum of high pungent degree, production cost is low, and market competition advantage is obvious.
Embodiment
Specify below and realize technical process of the present invention and implementation:
(1), technical process
Step 1, preparation capsicum particulate material: cause after the chilli that nothing is gone mouldy with machine is ground into 20～60 purpose powder
Particle;
Step 2, extraction: will put in the extraction container through weighing according to the capsicum particulate material of step 1 preparation, be solvent with the dme, the capsicum particulate material is extracted, and wherein, the weight ratio of particulate material and solvent is 1: 0.8～6, extracting temperature is 10～45 ℃, and extraction time is 10～60min; Carry out solid-liquid separation after extracting end, isolating solid phase is repeated to extract 2～8 times by above-mentioned processing condition, the solid phase after extracting is the capsicum dregs of rice;
Step 3, recovery solvent: to filtering or sedimentation from the isolating liquid phase of step 2, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied the recovery solvent;
Step 4, product separation: to from the isolating enriched material of step 3, controlled temperature is at 20～50 ℃, and enriched material is removed moisture and volatile matter content under the condition of gauge pressure less than-0.085Mpa, just obtained the capsanthin ointment.
Described operating process all is to finish under the processing condition of complete closed.
(2), implementation
Further specify method of the present invention with embodiment below:
Embodiment 1: get the capsicum particulate material 100kg according to step 1 preparation in the above-mentioned technical process, place extraction container, add the 80kg dme, extracting temperature is 45 ℃, and extraction time is 60min; Carry out solid-liquid separation after extracting end, isolating solid phase is repeated to extract 2～8 times by above-mentioned processing condition, the solid phase after multiple extraction is the capsicum dregs of rice; Liquid phase is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied the recovery solvent; The enriched material controlled temperature at 20～50 ℃, is removed moisture and volatile matter content under the condition of gauge pressure less than-0.085Mpa, just obtained the capsanthin ointment.
Embodiment 2: get the capsicum particulate material 100kg according to step 1 preparation in the above-mentioned technical process, place extraction container, add the 600kg dme, extracting temperature is 10 ℃, and extraction time is 10min; Carry out solid-liquid separation after extracting end, isolating solid phase is repeated to extract 2 times by above-mentioned processing condition, the solid phase after extracting is the capsicum dregs of rice; Liquid phase is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied the recovery solvent; The enriched material controlled temperature at 20～50 ℃, is removed moisture and volatile matter content under the condition of gauge pressure less than-0.085MPa, just obtained the capsanthin ointment.
Embodiment 3: get the capsicum particulate material 100kg according to step 1 preparation in the above-mentioned technical process, place extraction container, add the 300kg dme, extracting temperature is 30 ℃, and extraction time is 30min; Carry out solid-liquid separation after extracting end, isolating solid phase is repeated to extract 4 times by above-mentioned processing condition, the solid phase after extracting is the capsicum dregs of rice; Liquid phase is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied the recovery solvent; The enriched material controlled temperature at 20～50 ℃, is removed moisture and volatile matter content under the condition of gauge pressure less than-0.085MPa, just obtained the capsanthin ointment.
Embodiment 4: get the capsicum particulate material 100kg according to step 1 preparation in the above-mentioned technical process, place extraction container, add the 100kg dme, extracting temperature is 35 ℃, and extraction time is 40min; Carry out solid-liquid separation after extracting end, isolating solid phase is repeated to extract 5 times by above-mentioned processing condition, the solid phase after extracting is the capsicum dregs of rice; Liquid phase is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied the recovery solvent; The enriched material controlled temperature at 20～50 ℃, is removed moisture and volatile matter content under the condition of gauge pressure less than-0.085MPa, just obtained the capsanthin ointment.
Embodiment 5: get the capsicum particulate material 100kg according to step 1 preparation in the above-mentioned technical process, place extraction container, add the 200kg dme, extracting temperature is 45 ℃, and extraction time is 50min; Carry out solid-liquid separation after extracting end, isolating solid phase is repeated to extract 5 times by above-mentioned processing condition, the solid phase after extracting is the capsicum dregs of rice; Liquid phase is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied the recovery solvent; The enriched material controlled temperature at 20～50 ℃, is removed moisture and volatile matter content under the condition of gauge pressure less than-0.085MPa, just obtained the capsanthin ointment.
Claims (3)
1. the method for extracting capsaicin ointment from dimethyl ether is characterized in that:
(1) preparation capsicum particulate material: cause after the chilli that nothing is gone mouldy is ground into 20～60 purpose powder
Particulate material, put in the extraction vessel;
(2) extract: with the dme is that solvent extracts particulate material, and the weight ratio of particulate material and solvent is 1: 0.8～6, and extracting temperature is 10～45 ℃, and extraction time is 10～60min; Carry out solid-liquid separation after extracting end, isolating solid phase is repeated to extract 2～8 times by the said extracted processing condition, the solid phase after extracting is the capsicum dregs of rice;
(3) reclaim solvent: (2) isolating liquid phase is filtered or sedimentation, remove fine impurities wherein, decompression separation is gas phase and enriched material, and gas phase is compressed and liquefied the recovery solvent;
(4) product separation: (3) isolating enriched material controlled temperature at 20～50 ℃, under the condition of gauge pressure less than-0.085Mpa, is removed moisture and volatile matter content, obtain the capsanthin ointment.
2. the method for extracting capsaicin ointment from dimethyl ether according to claim 1, it is characterized in that: the weight ratio of described capsicum particulate material and solvent is 1: 0.8～3, extracting temperature is 20～45 ℃, and extraction time is 20～50min, and repeating extraction time is 3～5 times.
3. the method for extracting capsaicin ointment from dimethyl ether according to claim 1 is characterized in that: the temperature of described product separation control enriched material is 20～50 ℃, under the condition of gauge pressure less than-0.085Mpa, removes moisture and volatile matter content.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102372602A CN101906254A (en) | 2010-07-20 | 2010-07-20 | Method for extracting capsaicin ointment from dimethyl ether |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102372602A CN101906254A (en) | 2010-07-20 | 2010-07-20 | Method for extracting capsaicin ointment from dimethyl ether |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101906254A true CN101906254A (en) | 2010-12-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010102372602A Pending CN101906254A (en) | 2010-07-20 | 2010-07-20 | Method for extracting capsaicin ointment from dimethyl ether |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102326669A (en) * | 2011-08-26 | 2012-01-25 | 朱新亮 | Process for preparing white fish meal by dehydrating and degreasing at low temperature at one time |
| CN104479861A (en) * | 2014-12-15 | 2015-04-01 | 端木凡林 | Method for extracting liposoluble substances |
| CN106752067A (en) * | 2016-11-11 | 2017-05-31 | 安阳市晶华油脂工程有限公司 | A kind of method for extracting capsicum red pigment resin |
| CN110713733A (en) * | 2019-10-29 | 2020-01-21 | 四川常青调正食品有限责任公司 | Process for separating capsanthin from hot pepper |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1911902A (en) * | 2006-08-04 | 2007-02-14 | 苏州洪升油脂化工机械有限公司 | Extraction technology of capsanthin and capsicine |
| CN101712812A (en) * | 2009-10-15 | 2010-05-26 | 云南瑞升烟草技术（集团）有限公司 | Method and device for extracting fat-soluble natural pigment |
-
2010
- 2010-07-20 CN CN2010102372602A patent/CN101906254A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1911902A (en) * | 2006-08-04 | 2007-02-14 | 苏州洪升油脂化工机械有限公司 | Extraction technology of capsanthin and capsicine |
| CN101712812A (en) * | 2009-10-15 | 2010-05-26 | 云南瑞升烟草技术（集团）有限公司 | Method and device for extracting fat-soluble natural pigment |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102326669A (en) * | 2011-08-26 | 2012-01-25 | 朱新亮 | Process for preparing white fish meal by dehydrating and degreasing at low temperature at one time |
| CN102326669B (en) * | 2011-08-26 | 2013-05-08 | 朱新亮 | Process for preparing white fish meal by dehydrating and degreasing at low temperature at one time |
| CN104479861A (en) * | 2014-12-15 | 2015-04-01 | 端木凡林 | Method for extracting liposoluble substances |
| CN106752067A (en) * | 2016-11-11 | 2017-05-31 | 安阳市晶华油脂工程有限公司 | A kind of method for extracting capsicum red pigment resin |
| CN106752067B (en) * | 2016-11-11 | 2018-11-27 | 安阳市晶华油脂工程有限公司 | A method of extracting capsicum red pigment resin |
| CN110713733A (en) * | 2019-10-29 | 2020-01-21 | 四川常青调正食品有限责任公司 | Process for separating capsanthin from hot pepper |
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Application publication date: 20101208 |