CN104434542A - Medical antibacterial adhesive and preparation method thereof - Google Patents
Medical antibacterial adhesive and preparation method thereof Download PDFInfo
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- CN104434542A CN104434542A CN201410697047.8A CN201410697047A CN104434542A CN 104434542 A CN104434542 A CN 104434542A CN 201410697047 A CN201410697047 A CN 201410697047A CN 104434542 A CN104434542 A CN 104434542A
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Abstract
The invention relates to a medical antibacterial adhesive and a preparation method thereof, and belongs to the technical field of adhesives. The medical antibacterial adhesive comprises the following constituents in parts by weight: 16 to 20 parts of epoxy resin, 2 to 10 parts of crylic acid, 4 to 10 parts of editic acid, 12 to 18 parts of polyurethane, 2 to 5 parts of polyvinyl alcohol, 2 to 8 parts of methylol cellulose, 1 to 3 parts of citric acid, 3 to 9 parts of nanometer silicon micro powder, 10 to 14 parts of titanium dioxide, and 20 to 30 parts of glycol. The medical antibacterial adhesive has good bonding property, and can rapidly realize bonding even at low temperature; the medical antibacterial adhesive has excellent antibacterial property; the preparation method is simple, convenient to carry out, and suitable for large-scale promotion and application.
Description
Technical field
The invention belongs to adhesive technical field, be specifically related to a kind of medical antibacterial adhesive and preparation method thereof.
Background technology
At present, medical adhesive has very important effect in clinical.In surgical operation, medical adhesive is used for local bond and the repairing of some Organ and tissue; The combination in skeleton, joint and location in bone surgery, and for the repairing of tooth in gear division operation.Gear division adhesive and shell adhesive can be divided into from the use object of medical adhesive and performance requirement.And above-mentioned adhesive generally should meet safe, nontoxic, without carcinogenic, teratogenesis, mutagenesis; Good bonding strength to be had in addition, and can glued joint fast with tissue under normal temperature and pressure, own aseptic and also there is good biocidal property.The words of the application segmentation of medical adhesive have soft tissue adhesive, a-cyanoacrylate adhesive, the agent of fibrin gluing, sclerous tissues's adhesive, orthopaedics with being binding agent, medical pressure-sensitive adhesive etc.
And the performance of current existing gear division adhesive is barely satisfactory, its bacteriostasis property is poor, and uses raw material not environmentally.
In sum, the deficiency solving prior art existence has become this area technical problem urgently to be resolved hurrily.
Summary of the invention
The present invention, in order to solve the deficiencies in the prior art, provides a kind of medical antibacterial adhesive and preparation method thereof, and this medical antibacterial adhesive not only has excellent bonding strength, also has good antibiotic property.
The technical solution used in the present invention is as follows:
Medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 16-20 part, acrylic acid 2-10 part, ethylenediaminetetraacetic acid 4-10 part, polyurethane 12-18 part, polyvinyl alcohol 2-5 part, hydroxy methocel 2-8 part, citric acid 1-3 part, nano silicon micronization 3-9 part, titanium dioxide 10-14 part, ethylene glycol 20-30 part.
Described medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 17-19 part, acrylic acid 4-8 part, ethylenediaminetetraacetic acid 5-9 part, polyurethane 13-17 part, polyvinyl alcohol 3-4 part, hydroxy methocel 3-7 part, citric acid 2-3 part, nano silicon micronization 4-8 part, titanium dioxide 11-13 part, ethylene glycol 22-28 part.
Described medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 17-18 part, acrylic acid 5-7 part, ethylenediaminetetraacetic acid 6-8 part, polyurethane 14-16 part, polyvinyl alcohol 3-4 part, hydroxy methocel 4-6 part, citric acid 2-3 part, nano silicon micronization 5-7 part, titanium dioxide 11-12 part, ethylene glycol 23-26 part.
Described medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 17 parts, 4 parts, acrylic acid, ethylenediaminetetraacetic acid 5 parts, polyurethane 13 parts, polyvinyl alcohol 3 parts, hydroxy methocel 3 parts, citric acid 2 parts, nano silicon micronization 4 parts, titanium dioxide 11 parts, ethylene glycol 22 parts.
Described medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 19 parts, 8 parts, acrylic acid, ethylenediaminetetraacetic acid 9 parts, polyurethane 17 parts, polyvinyl alcohol 4 parts, hydroxy methocel 7 parts, citric acid 3 parts, nano silicon micronization 8 parts, titanium dioxide 13 parts, ethylene glycol 28 parts.
Described medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 17 parts, 5 parts, acrylic acid, ethylenediaminetetraacetic acid 6 parts, polyurethane 14 parts, polyvinyl alcohol 3 parts, hydroxy methocel 4 parts, citric acid 2 parts, nano silicon micronization 5 parts, titanium dioxide 11 parts, ethylene glycol 23 parts.
Described medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 18 parts, 7 parts, acrylic acid, ethylenediaminetetraacetic acid 8 parts, polyurethane 16 parts, polyvinyl alcohol 4 parts, hydroxy methocel 6 parts, citric acid 3 parts, nano silicon micronization 7 parts, titanium dioxide 12 parts, ethylene glycol 26 parts.
The preparation method of described medical antibacterial adhesive, comprise the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol are mixed, stir 30-50min, after being warming up to 80-90 DEG C, add hydroxy methocel, nano silicon micronization, titanium dioxide successively again, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 40-50 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
compared with prior art, its beneficial effect is in the present invention:the first, medical adhesive of the present invention has good bond properties, also can realize fast at low temperatures glueing joint; The second, medical adhesive of the present invention has excellent antibiotic property; 3rd, preparation method of the present invention is simple, and it is convenient to implement, and is suitable for applying on a large scale.
Detailed description of the invention
Below in conjunction with detailed description of the invention, set forth the present invention further.
embodiment 1
Medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 16 parts, 2 parts, acrylic acid, ethylenediaminetetraacetic acid 4 parts, polyurethane 12 parts, polyvinyl alcohol 2 parts, hydroxy methocel 2 parts, citric acid 1 part, nano silicon micronization 3 parts, titanium dioxide 10 parts, ethylene glycol 20 parts.
The preparation method of described medical antibacterial adhesive, comprise the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol are mixed, stir 30min, after being warming up to 80 DEG C, add hydroxy methocel, nano silicon micronization, titanium dioxide successively again, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 40 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
embodiment 2
Medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 20 parts, 10 parts, acrylic acid, ethylenediaminetetraacetic acid 10 parts, polyurethane 18 parts, polyvinyl alcohol 5 parts, hydroxy methocel 8 parts, citric acid 3 parts, nano silicon micronization 9 parts, titanium dioxide 14 parts, ethylene glycol 30 parts.
The preparation method of described medical antibacterial adhesive, comprise the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol are mixed, stir 50min, after being warming up to 90 DEG C, add hydroxy methocel, nano silicon micronization, titanium dioxide successively again, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 50 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
embodiment 3
Medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 17 parts, 4 parts, acrylic acid, ethylenediaminetetraacetic acid 5 parts, polyurethane 13 parts, polyvinyl alcohol 3 parts, hydroxy methocel 3 parts, citric acid 2 parts, nano silicon micronization 4 parts, titanium dioxide 11 parts, ethylene glycol 22 parts.
The preparation method of described medical antibacterial adhesive, comprise the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol are mixed, stir 40min, after being warming up to 85 DEG C, add hydroxy methocel, nano silicon micronization, titanium dioxide successively again, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 45 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
embodiment 4
Medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 19 parts, 8 parts, acrylic acid, ethylenediaminetetraacetic acid 9 parts, polyurethane 17 parts, polyvinyl alcohol 4 parts, hydroxy methocel 7 parts, citric acid 3 parts, nano silicon micronization 8 parts, titanium dioxide 13 parts, ethylene glycol 28 parts.
The preparation method of described medical antibacterial adhesive, comprise the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol are mixed, stir 35min, after being warming up to 82 DEG C, add hydroxy methocel, nano silicon micronization, titanium dioxide successively again, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 42 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
embodiment 5
Medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 17 parts, 5 parts, acrylic acid, ethylenediaminetetraacetic acid 6 parts, polyurethane 14 parts, polyvinyl alcohol 3 parts, hydroxy methocel 4 parts, citric acid 2 parts, nano silicon micronization 5 parts, titanium dioxide 11 parts, ethylene glycol 23 parts.
The preparation method of described medical antibacterial adhesive, comprise the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol are mixed, stir 45min, after being warming up to 84 DEG C, add hydroxy methocel, nano silicon micronization, titanium dioxide successively again, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 46 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
embodiment 6
Medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 18 parts, 7 parts, acrylic acid, ethylenediaminetetraacetic acid 8 parts, polyurethane 16 parts, polyvinyl alcohol 4 parts, hydroxy methocel 6 parts, citric acid 3 parts, nano silicon micronization 7 parts, titanium dioxide 12 parts, ethylene glycol 26 parts.
The preparation method of described medical antibacterial adhesive, comprise the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol are mixed, stir 48min, after being warming up to 86 DEG C, add hydroxy methocel, nano silicon micronization, titanium dioxide successively again, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 48 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
reference examples 1
Medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 17 parts, 4 parts, acrylic acid, ethylenediaminetetraacetic acid 5 parts, polyurethane 13 parts, polyvinyl alcohol 3 parts, hydroxy methocel 3 parts, citric acid 2 parts, titanium dioxide 11 parts, ethylene glycol 22 parts.
The preparation method of described medical antibacterial adhesive, comprises the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol is mixed, stir 40min, after being warming up to 85 DEG C, then add hydroxy methocel, titanium dioxide successively, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 45 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
reference examples 2
Medical antibacterial adhesive, comprises the following component according to weight parts: epoxy resin 17 parts, 4 parts, acrylic acid, ethylenediaminetetraacetic acid 5 parts, polyurethane 13 parts, polyvinyl alcohol 3 parts, citric acid 2 parts, titanium dioxide 11 parts, ethylene glycol 22 parts.
The preparation method of described medical antibacterial adhesive, comprises the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol is mixed, and stirs 40min, after being warming up to 85 DEG C, then adds titanium dioxide, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 45 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
performance Detection:
The embodiment of the present invention 1 to 6 gained finished product, reference examples 1 to 2 gained finished product are carried out performance test, and result is as follows:
Table 1 performance test data
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Reference examples 1 | Reference examples 2 | |
| To staphylococcus aureus suppression ratio, % | 99.1 | 99.5 | 99.9 | 99.8 | 99.2 | 99.8 | 20 | 30 |
| To escherichia coli suppression ratio, % | 99 | 99.5 | 99.9 | 99.8 | 99.5 | 99.6 | 28 | 30 |
| Caking property | Excellent | Excellent | Excellent | Excellent | Excellent | Excellent | Difference | Difference |
As can be seen from the table, the present invention has excellent performance, and wherein the performance of embodiment 3 is best, and gained finished product of the present invention also has good toughness in addition.
Claims (8)
1. medical antibacterial adhesive, it is characterized in that, comprise the following component according to weight parts: epoxy resin 16-20 part, acrylic acid 2-10 part, ethylenediaminetetraacetic acid 4-10 part, polyurethane 12-18 part, polyvinyl alcohol 2-5 part, hydroxy methocel 2-8 part, citric acid 1-3 part, nano silicon micronization 3-9 part, titanium dioxide 10-14 part, ethylene glycol 20-30 part.
2. medical antibacterial adhesive according to claim 1, it is characterized in that, comprise the following component according to weight parts: epoxy resin 17-19 part, acrylic acid 4-8 part, ethylenediaminetetraacetic acid 5-9 part, polyurethane 13-17 part, polyvinyl alcohol 3-4 part, hydroxy methocel 3-7 part, citric acid 2-3 part, nano silicon micronization 4-8 part, titanium dioxide 11-13 part, ethylene glycol 22-28 part.
3. medical antibacterial adhesive according to claim 1, it is characterized in that, comprise the following component according to weight parts: epoxy resin 17-18 part, acrylic acid 5-7 part, ethylenediaminetetraacetic acid 6-8 part, polyurethane 14-16 part, polyvinyl alcohol 3-4 part, hydroxy methocel 4-6 part, citric acid 2-3 part, nano silicon micronization 5-7 part, titanium dioxide 11-12 part, ethylene glycol 23-26 part.
4. medical antibacterial adhesive according to claim 1, it is characterized in that, comprise the following component according to weight parts: epoxy resin 17 parts, 4 parts, acrylic acid, ethylenediaminetetraacetic acid 5 parts, polyurethane 13 parts, polyvinyl alcohol 3 parts, hydroxy methocel 3 parts, citric acid 2 parts, nano silicon micronization 4 parts, titanium dioxide 11 parts, ethylene glycol 22 parts.
5. medical antibacterial adhesive according to claim 1, it is characterized in that, comprise the following component according to weight parts: epoxy resin 19 parts, 8 parts, acrylic acid, ethylenediaminetetraacetic acid 9 parts, polyurethane 17 parts, polyvinyl alcohol 4 parts, hydroxy methocel 7 parts, citric acid 3 parts, nano silicon micronization 8 parts, titanium dioxide 13 parts, ethylene glycol 28 parts.
6. medical antibacterial adhesive according to claim 1, it is characterized in that, comprise the following component according to weight parts: epoxy resin 17 parts, 5 parts, acrylic acid, ethylenediaminetetraacetic acid 6 parts, polyurethane 14 parts, polyvinyl alcohol 3 parts, hydroxy methocel 4 parts, citric acid 2 parts, nano silicon micronization 5 parts, titanium dioxide 11 parts, ethylene glycol 23 parts.
7. medical antibacterial adhesive according to claim 1, it is characterized in that, comprise the following component according to weight parts: epoxy resin 18 parts, 7 parts, acrylic acid, ethylenediaminetetraacetic acid 8 parts, polyurethane 16 parts, polyvinyl alcohol 4 parts, hydroxy methocel 6 parts, citric acid 3 parts, nano silicon micronization 7 parts, titanium dioxide 12 parts, ethylene glycol 26 parts.
8. the preparation method of medical antibacterial adhesive according to claim 1, it is characterized in that, comprise the steps: step one: according to weight proportion, epoxy resin, acrylic acid, polyurethane and polyvinyl alcohol are mixed, stir 30-50min, after being warming up to 80-90 DEG C, then add hydroxy methocel, nano silicon micronization, titanium dioxide successively, stir; Step 2: add ethylenediaminetetraacetic acid and citric acid again, at 40-50 DEG C, constant temperature stirs; Step 3: drip ethylene glycol again, stirs and obtains described medical antibacterial adhesive.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410697047.8A CN104434542A (en) | 2014-11-27 | 2014-11-27 | Medical antibacterial adhesive and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410697047.8A CN104434542A (en) | 2014-11-27 | 2014-11-27 | Medical antibacterial adhesive and preparation method thereof |
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| CN104434542A true CN104434542A (en) | 2015-03-25 |
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Cited By (11)
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| CN104873403A (en) * | 2015-05-21 | 2015-09-02 | 苏州市贝克生物科技有限公司 | Orthodontic adhesive and preparation method thereof |
| CN105368263A (en) * | 2015-12-21 | 2016-03-02 | 常熟市雷号医疗器械有限公司 | Medical suction head |
| CN105617442A (en) * | 2016-03-01 | 2016-06-01 | 苏州市贝克生物科技有限公司 | Adhesive for adhesive bandage and preparation method of adhesive |
| CN105749324A (en) * | 2016-03-08 | 2016-07-13 | 苏州市贝克生物科技有限公司 | Adhesive applicable to bandage and preparation method of adhesive applicable to bandage |
| CN106110375A (en) * | 2016-06-27 | 2016-11-16 | 林春梅 | A kind of medical adhesive and preparation method thereof |
| US10233380B1 (en) * | 2017-09-11 | 2019-03-19 | Saudi Arabian Oil Company | Well treatment fluid having an acidic nanoparticle based dispersion and a polyamine |
| US10316238B2 (en) | 2017-09-11 | 2019-06-11 | Saudi Arabian Oil Company | Nanosilica dispersion for thermally insulating packer fluid |
| US10577526B2 (en) | 2017-09-11 | 2020-03-03 | Saudi Arabian Oil Company | Loss circulation material composition having an acidic nanoparticle based dispersion and polyamine |
| US10683452B2 (en) | 2017-09-11 | 2020-06-16 | Saudi Arabian Oil Company | Nanosilica dispersion for thermally insulating packer fluid |
| US11279865B2 (en) | 2017-09-11 | 2022-03-22 | Saudi Arabian Oil Company | Well treatment fluid having an acidic nanoparticle based dispersion, an epoxy resin, and a polyamine |
| CN115852734A (en) * | 2022-12-23 | 2023-03-28 | 九牧厨卫股份有限公司 | Melamine adhesive and preparation method and application thereof |
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| CN104873403A (en) * | 2015-05-21 | 2015-09-02 | 苏州市贝克生物科技有限公司 | Orthodontic adhesive and preparation method thereof |
| CN104873403B (en) * | 2015-05-21 | 2018-04-27 | 王梦梦 | A kind of mouth cavity orthodontic adhesive and preparation method thereof |
| CN105368263A (en) * | 2015-12-21 | 2016-03-02 | 常熟市雷号医疗器械有限公司 | Medical suction head |
| CN105617442A (en) * | 2016-03-01 | 2016-06-01 | 苏州市贝克生物科技有限公司 | Adhesive for adhesive bandage and preparation method of adhesive |
| CN105617442B (en) * | 2016-03-01 | 2019-02-19 | 苏州市贝克生物科技有限公司 | Adhesive bandage adhesive and preparation method thereof |
| CN105749324A (en) * | 2016-03-08 | 2016-07-13 | 苏州市贝克生物科技有限公司 | Adhesive applicable to bandage and preparation method of adhesive applicable to bandage |
| CN106110375A (en) * | 2016-06-27 | 2016-11-16 | 林春梅 | A kind of medical adhesive and preparation method thereof |
| US10316238B2 (en) | 2017-09-11 | 2019-06-11 | Saudi Arabian Oil Company | Nanosilica dispersion for thermally insulating packer fluid |
| US10233380B1 (en) * | 2017-09-11 | 2019-03-19 | Saudi Arabian Oil Company | Well treatment fluid having an acidic nanoparticle based dispersion and a polyamine |
| US10577526B2 (en) | 2017-09-11 | 2020-03-03 | Saudi Arabian Oil Company | Loss circulation material composition having an acidic nanoparticle based dispersion and polyamine |
| US10683452B2 (en) | 2017-09-11 | 2020-06-16 | Saudi Arabian Oil Company | Nanosilica dispersion for thermally insulating packer fluid |
| US10731069B2 (en) | 2017-09-11 | 2020-08-04 | Saudi Arabian Oil Company | Well treatment fluid having an acidic nanoparticle based dispersion and a polyamine |
| US11034881B2 (en) | 2017-09-11 | 2021-06-15 | Saudi Arabian Oil Company | Nanosilica dispersion for thermally insulating packer fluid |
| US11279865B2 (en) | 2017-09-11 | 2022-03-22 | Saudi Arabian Oil Company | Well treatment fluid having an acidic nanoparticle based dispersion, an epoxy resin, and a polyamine |
| US11370955B2 (en) | 2017-09-11 | 2022-06-28 | Saudi Arabian Oil Company | Nanosilica dispersion for thermally insulating packer fluid |
| CN115852734A (en) * | 2022-12-23 | 2023-03-28 | 九牧厨卫股份有限公司 | Melamine adhesive and preparation method and application thereof |
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