CN104403348B - 一种高水洗牢度和升华牢度的紫色分散染料及其制备方法 - Google Patents
一种高水洗牢度和升华牢度的紫色分散染料及其制备方法 Download PDFInfo
- Publication number
- CN104403348B CN104403348B CN201410660350.0A CN201410660350A CN104403348B CN 104403348 B CN104403348 B CN 104403348B CN 201410660350 A CN201410660350 A CN 201410660350A CN 104403348 B CN104403348 B CN 104403348B
- Authority
- CN
- China
- Prior art keywords
- disperse dyes
- washing fastness
- formula
- ethyl
- high washing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000986 disperse dye Substances 0.000 title claims abstract description 37
- 238000005406 washing Methods 0.000 title claims abstract description 30
- 238000000859 sublimation Methods 0.000 title claims abstract description 25
- 230000008022 sublimation Effects 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000000975 dye Substances 0.000 claims abstract description 34
- 238000000034 method Methods 0.000 claims abstract description 15
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims abstract description 12
- -1 pi-allyl Chemical group 0.000 claims abstract description 10
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 8
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims abstract description 5
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims abstract description 4
- FHIVAFMUCKRCQO-UHFFFAOYSA-N diazinon Chemical compound CCOP(=S)(OCC)OC1=CC(C)=NC(C(C)C)=N1 FHIVAFMUCKRCQO-UHFFFAOYSA-N 0.000 claims description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid group Chemical group S(O)(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 10
- 150000001875 compounds Chemical class 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- 239000000243 solution Substances 0.000 claims description 7
- 239000003153 chemical reaction reagent Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 238000005859 coupling reaction Methods 0.000 claims description 5
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 claims description 5
- UHOVQNZJYSORNB-UHFFFAOYSA-N monobenzene Natural products C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 5
- RXQNKKRGJJRMKD-UHFFFAOYSA-N 5-bromo-2-methylaniline Chemical compound CC1=CC=C(Br)C=C1N RXQNKKRGJJRMKD-UHFFFAOYSA-N 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 4
- 230000008859 change Effects 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 3
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 claims description 2
- 239000012954 diazonium Substances 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-O diazynium Chemical compound [NH+]#N IJGRMHOSHXDMSA-UHFFFAOYSA-O 0.000 claims description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 1
- 239000005864 Sulphur Substances 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 239000004744 fabric Substances 0.000 abstract description 11
- 238000004043 dyeing Methods 0.000 abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 7
- 239000000047 product Substances 0.000 abstract description 5
- 238000011161 development Methods 0.000 abstract description 3
- 238000011160 research Methods 0.000 abstract description 3
- 208000005623 Carcinogenesis Diseases 0.000 abstract description 2
- 150000001450 anions Chemical class 0.000 abstract description 2
- 230000036952 cancer formation Effects 0.000 abstract description 2
- 231100000504 carcinogenesis Toxicity 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 125000004185 ester group Chemical group 0.000 abstract description 2
- 239000000413 hydrolysate Substances 0.000 abstract description 2
- 230000007062 hydrolysis Effects 0.000 abstract description 2
- 238000006460 hydrolysis reaction Methods 0.000 abstract description 2
- 230000000774 hypoallergenic effect Effects 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 125000005543 phthalimide group Chemical group 0.000 abstract description 2
- 239000002699 waste material Substances 0.000 abstract description 2
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 238000003786 synthesis reaction Methods 0.000 abstract 1
- 239000000835 fiber Substances 0.000 description 13
- 238000003756 stirring Methods 0.000 description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 230000002209 hydrophobic effect Effects 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 239000007859 condensation product Substances 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 229920000728 polyester Polymers 0.000 description 3
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 3
- 229920001732 Lignosulfonate Polymers 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- 229920004933 Terylene® Polymers 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 description 2
- 238000004044 disperse dyeing Methods 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000002657 fibrous material Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- NHNUFAASKXPOQA-UHFFFAOYSA-N (3-acetamido-2-hydroxyphenyl)arsonic acid Chemical compound C(C)(=O)NC=1C(=C(C=CC1)[As](O)(=O)O)O NHNUFAASKXPOQA-UHFFFAOYSA-N 0.000 description 1
- IQXJCCZJOIKIAD-UHFFFAOYSA-N 1-(2-methoxyethoxy)hexadecane Chemical compound CCCCCCCCCCCCCCCCOCCOC IQXJCCZJOIKIAD-UHFFFAOYSA-N 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- WLLGXSLBOPFWQV-UHFFFAOYSA-N MGK 264 Chemical compound C1=CC2CC1C1C2C(=O)N(CC(CC)CCCC)C1=O WLLGXSLBOPFWQV-UHFFFAOYSA-N 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- KKEYFWRCBNTPAC-UHFFFAOYSA-N benzene-dicarboxylic acid Natural products OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 229950009789 cetomacrogol 1000 Drugs 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 125000002587 enol group Chemical class 0.000 description 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 125000003010 ionic group Chemical group 0.000 description 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Natural products OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
- IIACRCGMVDHOTQ-UHFFFAOYSA-N sulfamic acid Chemical compound NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 150000003504 terephthalic acids Chemical class 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Landscapes
- Coloring (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410660350.0A CN104403348B (zh) | 2014-11-18 | 2014-11-18 | 一种高水洗牢度和升华牢度的紫色分散染料及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410660350.0A CN104403348B (zh) | 2014-11-18 | 2014-11-18 | 一种高水洗牢度和升华牢度的紫色分散染料及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104403348A CN104403348A (zh) | 2015-03-11 |
CN104403348B true CN104403348B (zh) | 2016-09-07 |
Family
ID=52641022
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201410660350.0A Active CN104403348B (zh) | 2014-11-18 | 2014-11-18 | 一种高水洗牢度和升华牢度的紫色分散染料及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN104403348B (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105647224A (zh) * | 2016-01-28 | 2016-06-08 | 俞杏英 | 一种邻苯二甲酰亚胺-偶氮分散染料单体化合物及其制备方法和应用 |
CN107722663A (zh) * | 2017-10-10 | 2018-02-23 | 浙江万丰化工有限公司 | 一种偶氮染料化合物及其制备方法和应用 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2002068539A1 (en) * | 2001-02-07 | 2002-09-06 | Ciba Specialty Chemicals Holding Inc. | Phthalimidyl azo dyes, process for the preparation thereof and the use thereof |
AU2003276247A1 (en) * | 2002-11-11 | 2004-06-03 | Ciba Specialty Chemicals Holding Inc. | Phthalimidyl-azo dyes, process for their preparation and their use |
US9376570B2 (en) * | 2012-07-27 | 2016-06-28 | Huntsman International Llc | Disperse azo dyes, a process for the preparation thereof and the use thereof |
-
2014
- 2014-11-18 CN CN201410660350.0A patent/CN104403348B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN104403348A (zh) | 2015-03-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101649129B (zh) | 一种适用于碱性染色的分散染料组合物 | |
KR101346852B1 (ko) | 고 습윤견뢰도의 흑색 및 네이비블루 분산염료 조성물 | |
CN103525122B (zh) | 一种分散染料组合物及其制品和应用 | |
CN102782210B (zh) | 偶氮分散染料 | |
KR20060118533A (ko) | 분산 염료 | |
CN106118119B (zh) | 耐强碱中温型分散紫染料、其复配混合物及其制备方法 | |
CN104448892B (zh) | 一种高水洗牢度和升华牢度的宝蓝分散染料及其制备方法 | |
CN104403348B (zh) | 一种高水洗牢度和升华牢度的紫色分散染料及其制备方法 | |
CN104448893B (zh) | 一种高水洗牢度和升华牢度的红色分散染料及其制备方法 | |
CN104448894B (zh) | 高水洗牢度和升华牢度的分散绿光蓝染料及其制备方法 | |
CN104592782B (zh) | 适于酸-碱性浴中染色的偶氮型分散染料、制备及应用 | |
KR101801993B1 (ko) | 분산염료 | |
CN109535769B (zh) | 一种分散红染料组合物和染料制品 | |
CN105733290A (zh) | 一种高耐汗牢度橙色分散染料单体化合物及其制备方法和应用 | |
CN110229541A (zh) | 一种组合偶氮分散染料及制备方法 | |
CN102443280A (zh) | 一种分散蓝色至黑色染料组合物 | |
CN105860570B (zh) | 一种卤代苯并噻唑-偶氮分散染料单体化合物及其制备方法和应用 | |
CN101778908A (zh) | 分散染料、它们的制备及应用 | |
JPH0841364A (ja) | 水不溶性赤色モノアゾ染料、その製造方法及びこれを用いて染色又は捺染する方法 | |
CN111117290B (zh) | 一种分散红染料组合物及染料制品 | |
JPH1077583A (ja) | 分散染料組成物を用いるポリエステル系新合繊の染色又は捺染方法 | |
CN105542508B (zh) | 一种分散染料单体化合物及其制备方法和应用 | |
CN105623309A (zh) | 一种高上染率分散染料组合物及其制备方法和应用 | |
BRPI0609651A2 (pt) | corantes dispersos azuis de cor estável com relação à luz em temperaturas elevadas | |
BRPI0815000B1 (pt) | Corantes dispersos de 1,3-tiazolila, seu processo de preparação, seu uso, e tinta para impressão digital em materiais têxteis pelo processo de jato de tinta |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20180504 Address after: 311200 Linjiang Industrial Park, Xiaoshan, Hangzhou, Zhejiang, No. 1919, No. five road. Patentee after: Hangzhou Fulai'ente Finechemical Co., Ltd. Address before: 311228 Linjiang Industrial Park, Xiaoshan District, Hangzhou, Zhejiang, No. 1919, No. five road. Patentee before: Li Baichun |
|
TR01 | Transfer of patent right | ||
CP03 | Change of name, title or address |
Address after: 310000 no.1919, Jingwu Road, Linjiang Industrial Park, Xiaoshan District, Hangzhou City, Zhejiang Province Patentee after: Hangzhou Fulai anthracite Co., Ltd Address before: 311200, Linjiang Industrial Park, Zhejiang, Hangzhou Province, No. five, No. 1919, Xiaoshan Patentee before: Hangzhou Fulai'ente Finechemical Co., Ltd. |
|
CP03 | Change of name, title or address |