CN104400674A - High-strength ceramic bonding agent and preparation method thereof - Google Patents

High-strength ceramic bonding agent and preparation method thereof Download PDF

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Publication number
CN104400674A
CN104400674A CN201410823644.0A CN201410823644A CN104400674A CN 104400674 A CN104400674 A CN 104400674A CN 201410823644 A CN201410823644 A CN 201410823644A CN 104400674 A CN104400674 A CN 104400674A
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CN
China
Prior art keywords
parts
bonding agent
ceramic bonding
preparation
strength ceramic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410823644.0A
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Chinese (zh)
Inventor
高杏祖
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CHANGSHU HAIYU GRINDING WHEEL Co Ltd
Original Assignee
CHANGSHU HAIYU GRINDING WHEEL Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CHANGSHU HAIYU GRINDING WHEEL Co Ltd filed Critical CHANGSHU HAIYU GRINDING WHEEL Co Ltd
Priority to CN201410823644.0A priority Critical patent/CN104400674A/en
Publication of CN104400674A publication Critical patent/CN104400674A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D3/00Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents
    • B24D3/02Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent
    • B24D3/04Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent and being essentially inorganic
    • B24D3/14Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent and being essentially inorganic ceramic, i.e. vitrified bondings
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/10Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/14Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • C04B35/6261Milling
    • C04B35/62615High energy or reactive ball milling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Ceramic Products (AREA)

Abstract

The invention discloses a high-strength ceramic bonding agent and a preparation method thereof. The high-strength ceramic bonding agent is prepared from the following substances in parts by weight: 37-44 parts of SiO2, 26-38 parts of B2O3, 23-28 parts of Al2O3, 6-9 parts of TiO2, 5-10 parts of Li2NO3, 15-22 parts of K2CO3, 1-7 parts of Zn and 2-6 parts of Sn. The preparation method of the high-strength ceramic bonding agent comprises the following steps: sufficiently mixing all the raw materials in a ball mill, adding water into the raw materials for performing ball-milling for 6-8 hours, then, standing for 3-4 hours, pouring out water, drying at 95-105 DEG C, and performing ball-milling and screening so as to obtain the ceramic bonding agent. The ceramic bonding agent prepared by the preparation method has the characteristics of low refractoriness and high strength.

Description

A kind of high-strength ceramic bonding agent and preparation method thereof
Technical field
The invention belongs to vitrified bond technical field, be specifically related to vitrified bond of a kind of high strength and preparation method thereof.
Background technology
Because vitrified bond has Heat stability is good, the advantages such as rigidity is higher, the porosity is controlled, ceramic binder cubic boron nitride grinding tool is possessed, and intensity is higher, self-sharpening is good, be easy to the advantages such as finishing.The structural elements such as abrasive particle, bonding agent and pore determine jointly can the performance of grinding tool.And vitrified bonded grinding wheel slightly depend primarily on the intensity of vitrified bond itself and the bond strength between bonding agent and abrasive grain.The composition of bonding agent is the key factor affecting vitrified bond intensity and bonding agent and abrasive grain interface bond strength.Along with the progress of science and technology, vitrified bond of the prior art can not meet the demand of commercial Application, therefore, needs the vitrified bond providing a kind of low melting point high strength.
Summary of the invention
Technical problem: the technical issues that need to address of the present invention are to provide a kind of high-strength ceramic bonding agent and preparation method thereof.
Technical scheme: the invention discloses a kind of high-strength ceramic bonding agent, this vitrified bond is made up of the material of following weight fraction: SiO 237 ~ 44 parts, B 2o 326 ~ 38 parts, Al 2o 323 ~ 28 parts, TiO 26 ~ 9 parts, Li 2nO 35 ~ 10 parts, K 2cO 315 ~ 22 parts, Zn 1 ~ 7 part, Sn 2 ~ 6 parts.
Wherein, this vitrified bond is made up of the material of following weight fraction: SiO 240 parts, B 2o 330 parts, Al 2o 325 parts, TiO 28 parts, Li 2nO 38 parts, K 2cO 320 parts, Zn 5 parts, Sn 4 parts.
The preparation method of this high-strength ceramic bonding agent is as follows: fully mixed in ball mill by all raw materials, is adding water, ball milling 6 ~ 8h, then leave standstill 3 ~ 4h, poured out by water, dry under 95 ~ 105 DEG C of conditions, then ball milling, sieving prepares vitrified bond.
Wherein, the particle diameter of described vitrified bond is 26 ~ 30 μm.Wherein, the particle diameter of described vitrified bond is 26 ~ 30 μm.
Beneficial effect: vitrified bond provided by the invention has the advantages that refractoriness is low, good fluidity, thermal coefficient of expansion are high.
Detailed description of the invention
Embodiment 1:
A kind of high-strength ceramic bonding agent, forms SiO by the material of following weight fraction 237 parts, B 2o 326 parts, Al 2o 323 parts, TiO 26 parts, Li 2nO 35 parts, K 2cO 315 parts, Zn 1 part, Sn 2 parts.
Above-mentioned substance is fully mixed in high energy ball mill, all raw materials are fully mixed in ball mill, adding water, ball milling 5h, then leave standstill 2h, water is poured out, dries under 90 DEG C of conditions, then ball milling, sieving prepares vitrified bond.
Embodiment 2:
A kind of high-strength ceramic bonding agent, is made up of the material of following weight fraction: SiO 240 parts, B 2o 330 parts, Al 2o 325 parts, TiO 28 parts, Li 2nO 38 parts, K 2cO 320 parts, Zn 5 parts, Sn 4 parts.
All raw materials are fully mixed in ball mill, is adding water, ball milling 8h, then leave standstill 2h, water is poured out, dries under 90 DEG C of conditions, then ball milling, sieving prepares vitrified bond.
Embodiment 3:
A kind of high-strength ceramic bonding agent, is made up of the material of following weight fraction: SiO 244 parts, B 2o 338 parts, Al 2o 328 parts, TiO 29 parts, Li 2nO 310 parts, K 2cO 322 parts, Zn 7 parts, Sn 6.
All raw materials are fully mixed in ball mill, is adding water, ball milling 10h, then leave standstill 1h, water is poured out, dries under 100 DEG C of conditions, then ball milling, sieving prepares vitrified bond.

Claims (4)

1. a high-strength ceramic bonding agent, is characterized in that, this vitrified bond is made up of the material of following weight fraction: SiO 237 ~ 44 parts, B 2o 326 ~ 38 parts, Al 2o 323 ~ 28 parts, TiO 26 ~ 9 parts, Li 2nO 35 ~ 10 parts, K 2cO 315 ~ 22 parts, Zn 1 ~ 7 part, Sn 2 ~ 6 parts.
2. high-strength ceramic bonding agent according to claim 1, is characterized in that, this vitrified bond is made up of the material of following weight fraction: SiO 240 parts, B 2o 330 parts, Al 2o 325 parts, TiO 28 parts, Li 2nO 38 parts, K 2cO 320 parts, Zn 5 parts, Sn 4 parts.
3. the preparation method of high-strength ceramic bonding agent according to claim 1, is characterized in that, is fully mixed by all raw materials in ball mill, add water, ball milling 6 ~ 8h, then leave standstill 3 ~ 4h, water is poured out, dries under 95 ~ 105 DEG C of conditions, then ball milling, sieving prepares vitrified bond.
4. the preparation method of high-strength ceramic bonding agent according to claim 3, is characterized in that, the particle diameter of described vitrified bond is 26 ~ 30 μm.
CN201410823644.0A 2014-12-26 2014-12-26 High-strength ceramic bonding agent and preparation method thereof Pending CN104400674A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410823644.0A CN104400674A (en) 2014-12-26 2014-12-26 High-strength ceramic bonding agent and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410823644.0A CN104400674A (en) 2014-12-26 2014-12-26 High-strength ceramic bonding agent and preparation method thereof

Publications (1)

Publication Number Publication Date
CN104400674A true CN104400674A (en) 2015-03-11

Family

ID=52638373

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410823644.0A Pending CN104400674A (en) 2014-12-26 2014-12-26 High-strength ceramic bonding agent and preparation method thereof

Country Status (1)

Country Link
CN (1) CN104400674A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59156974A (en) * 1983-02-23 1984-09-06 日本特殊陶業株式会社 Method of bonding ceramics and silicon
CN103273431A (en) * 2013-06-13 2013-09-04 江苏亚宝车业有限公司 Ceramic binder
CN103522207A (en) * 2013-09-29 2014-01-22 河南华茂新材料科技开发有限公司 Ceramic bonding agent containing rare-earth metal
CN103624696A (en) * 2013-12-16 2014-03-12 珠海市钜鑫科技开发有限公司 Ceramic bond, preparation method thereof and manufacturing method of ceramic bond grinding tool
CN103753410A (en) * 2014-01-08 2014-04-30 袁德禄 Low-temperature metal ceramic blinder grinding wheel and production method thereof
CN103781595A (en) * 2011-09-07 2014-05-07 3M创新有限公司 Bonded abrasive article

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59156974A (en) * 1983-02-23 1984-09-06 日本特殊陶業株式会社 Method of bonding ceramics and silicon
CN103781595A (en) * 2011-09-07 2014-05-07 3M创新有限公司 Bonded abrasive article
CN103273431A (en) * 2013-06-13 2013-09-04 江苏亚宝车业有限公司 Ceramic binder
CN103522207A (en) * 2013-09-29 2014-01-22 河南华茂新材料科技开发有限公司 Ceramic bonding agent containing rare-earth metal
CN103624696A (en) * 2013-12-16 2014-03-12 珠海市钜鑫科技开发有限公司 Ceramic bond, preparation method thereof and manufacturing method of ceramic bond grinding tool
CN103753410A (en) * 2014-01-08 2014-04-30 袁德禄 Low-temperature metal ceramic blinder grinding wheel and production method thereof

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Application publication date: 20150311