CN104388170A - Working solution for quickly cutting water-based wire and preparation method of working solution - Google Patents
Working solution for quickly cutting water-based wire and preparation method of working solution Download PDFInfo
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- CN104388170A CN104388170A CN201410578454.7A CN201410578454A CN104388170A CN 104388170 A CN104388170 A CN 104388170A CN 201410578454 A CN201410578454 A CN 201410578454A CN 104388170 A CN104388170 A CN 104388170A
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Abstract
The invention discloses a working solution for quickly cutting a water-based wire and a preparation method of the working solution. According to the technical scheme, the working solution for quickly cutting the water-based wire is characterized by being prepared from the raw materials in percentage by mass: 5-30 percent of a lubricating antirust agent, 1-10 percent of a phosphate extreme-pressure agent, 0.5-10 percent of an explosion agent, 1-10 percent of an alcohol ether coupling agent and the balance of deionized water. The invention further discloses the preparation method of the working solution for quickly cutting the water-based wire. The working solution for quickly cutting the water-based wire is high in cutting efficiency, good in cutting quality, good in lubricating anti-rusting performance and relatively low in cost.
Description
Technical field
The present invention relates to metal wire cutting processing working fluid, be specifically related to a kind of rapid water baseline cutting working liquid and preparation method thereof.
Background technology
Wire-cut Electrical Discharge Machining is called for short Linear cut, and its ultimate principle utilizes the fine wire (copper wire or molybdenum filament) of movement as tool-electrode, carries out pulse spark electric discharge removal metal, excision forming to workpiece.Linear cut has long development history, has just occurred electrospark machining as far back as mid-term in 20th century.Along with the development of science and technology, the application of computer technology especially in recent years and the combination of line motor spark technology, the outstanding advantage of linear cutter technology especially fabrication techniques cannot replace, and therefore cutting on line obtains market application widely.
Linear cut working fluid common in the market mainly contains oil-in-water type and water-base type line cutting working liquid two class.Oil-in-water type Linear cut working fluid belongs to traditional product, oil based on many employings mineral oil, the patent of invention being 201010212696.6 as number of patent application discloses a kind of linear cutter working fluid, such Linear cut working fluid is used to there is following many deficiencies: 1, mineral oil viscosity is large, poor fluidity, cooling performance is not good, not easy cleaning, and not easily emulsification, what have is also paste, if number of patent application is the patent of invention of 03113009.7, uses very inconvenient, mineral oil is subject to resource limit, and cost is also higher; 2, oily substance is inflammable volatile, easily produces untoward reaction after human contact, and in high speed travelling wire process, have the danger of catching fire; 3, this type of Product environment pollutes large, adds and easily produces oil smoke, greasy dirt man-hour, affect the surface quality of workpiece, and the waste water produced not easily is degraded, and cost for wastewater treatment is higher.Water-base type line cutting working liquid is a kind of novel Linear cut working fluid, compared with oil-in-water type Linear cut working fluid, it is little that water-base type line cutting working liquid has pollution, without mineral oil, color is transparent, cooling and the advantage such as cleaning performance is good, but the antirust and lubricity of water-base type line cutting working liquid is slightly poor, and cutting efficiency also has much room for improvement.
Wire-cut Electrical Discharge Machining is the process of electricity, heat, power comprehensive action, the quality of the therefore direct effect string cutting of the performance of Linear cut working fluid and effect.Along with industry environmental protection require increasingly strict, Linear cut working fluid, towards efficient, environmental protection future development, is therefore developed efficient Express Order Wire cutting working liquid and is become trend.
Summary of the invention
The technical problem that the present invention solves there is provided that a kind of cutting efficiency is high, cutting quality good, lubricating and antirust performance is good and lower-cost rapid water baseline cutting working liquid.
Another technical problem that the present invention solves there is provided a kind of easy economy, environmental protection and the preparation method of rapid water baseline cutting working liquid with low cost.
Technical scheme of the present invention is: a kind of rapid water baseline cutting working liquid, it is characterized in that being prepared from by the raw material of following mass percentage: lubricating and antirust agent 5%-30%, phosphoric acid ester overstocks agent 1%-10%, explosive agent 0.5%-10%, alcohol ether couplant 1%-10%, surplus is deionized water, described lubricating and antirust agent is prepared from by refining Yatall MA and hydramine, wherein the quality proportioning of refining Yatall MA and hydramine is that m(refines Yatall MA): m(hydramine)=1:0.5-3.5, hydramine is Monoethanolamine MEA BASF, a kind of or two or more arbitrarily mixture in diethanolamine and trolamine, it is fatty alcohol-ether phosphoric acid ester MOA-3P or fatty alcohol-ether phosphoric acid ester MOA-9P that described phosphoric acid ester overstocks agent, described explosive agent is Zulkovsky starch, described alcohol ether couplant is diethylene glycol ether, Diethylene Glycol propyl ether, butyl, a kind of or two or more arbitrarily mixture in tripropylene glycol methyl ether and tripropylene glycol ether.
Lubricating and antirust agent of the present invention is prepared from by following methods: first refine Yatall MA according to m(): m(hydramine) the quality proportioning of=1:0.5-3.5 takes refining Yatall MA and hydramine respectively, the refining Yatall MA taken and hydramine is mixed and heated to 50-120 DEG C of reaction 30-120min i.e. obtained lubricating and antirust agent.
Rapid water baseline cutting working liquid of the present invention, it is characterized in that being prepared from by the raw material of following mass percentage: refining Yatall MA 8%, Monoethanolamine MEA BASF 8%, trolamine 8%, fatty alcohol-ether phosphoric acid ester MOA-3P 8%, Zulkovsky starch 2%, diethylene glycol ether 2%, butyl 2% and deionized water 62%.
The preparation method of rapid water baseline cutting working liquid of the present invention, it is characterized in that comprising the following steps: (1) refines Yatall MA according to m(): m(hydramine) the quality proportioning of=1:0.5-3.5 takes refining Yatall MA and hydramine respectively, the refining Yatall MA taken and hydramine are mixed and heated to 50-120 DEG C of reaction 30-120min i.e. obtained lubricating and antirust agent, wherein hydramine is a kind of or two or more arbitrarily mixture in Monoethanolamine MEA BASF, diethanolamine and trolamine; (2) raw material is taken respectively according to following proportioning, lubricating and antirust agent 5%-30%, phosphoric acid ester overstock agent 1%-10%, explosive agent 0.5%-10%, alcohol ether couplant 1%-10%, surplus are deionized water, it is fatty alcohol-ether phosphoric acid ester MOA-3P or fatty alcohol-ether phosphoric acid ester MOA-9P that described phosphoric acid ester overstocks agent, described explosive agent is Zulkovsky starch, and described alcohol ether couplant is a kind of or two or more arbitrarily mixture in diethylene glycol ether, Diethylene Glycol propyl ether, butyl, tripropylene glycol methyl ether and tripropylene glycol ether; (3) in the deionized water taken, add explosive agent, alcohol ether couplant and phosphoric acid ester and overstock agent, mix, dissolve fully; (4) the lubricating and antirust agent taken joined in the mixing solutions that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
The preparation method of rapid water baseline cutting working liquid of the present invention, it is characterized in that comprising the following steps: (1) takes the raw material of following quality proportioning respectively, refining Yatall MA 8%, Monoethanolamine MEA BASF 8%, trolamine 8%, fatty alcohol-ether phosphoric acid ester MOA-3P 8%, Zulkovsky starch 2%, diethylene glycol ether 2%, butyl 2% and deionized water 62% are for subsequent use; (2) get refining Yatall MA and Monoethanolamine MEA BASF and trolamine to be heated to 100 DEG C and to react 45min to obtain lubricating and antirust agent for subsequent use; (3) in the deionized water taken, add Zulkovsky starch, diethylene glycol ether, butyl and fatty alcohol-ether phosphoric acid ester MOA-3P, mix, dissolve fully; (4) lubricating and antirust agent obtained for step (2) joined in the mixed solution that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
Rapid water baseline cutting working liquid of the present invention, tool has the following advantages:
1, the refining Yatall MA lubricity that the present invention is used is superior, and cleaning performance is good and have certain anti-bubble effect, wide to the subject range of hard water, and easy cleaning after product of the present invention uses, has good lubricating and antirust performance;
2, product Environmental Safety performance of the present invention is good, avoid the greasy dirt, the oil smoke problem that use oily substance to produce, improve the surface quality of workpiece, also improve Working environment simultaneously, reduce discharge and the pollution of trade effluent, saved cost, product of the present invention the experiment proved that human non-toxic, has ensured the safety of staff;
3, product of the present invention uses rear technological effect good, and not only increase process velocity fast, also improve cutting efficiency, the workpiece surface finish after processing is high, there is not blackout, burns silk problem;
4, product colour of the present invention is transparent, and avoid the lamination problem of oiliness Linear cut working fluid, stable chemical performance, the quality guaranteed period is longer.
Embodiment
By the following examples foregoing of the present invention is described in further details, but this should be interpreted as that the scope of the above-mentioned theme of the present invention is only limitted to following embodiment.All technology realized based on foregoing of the present invention all belong to scope of the present invention.
Embodiment 1
(1) refining Yatall MA 8kg, Monoethanolamine MEA BASF 8kg, trolamine 8kg, fatty alcohol-ether phosphoric acid ester MOA-3P 8kg, Zulkovsky starch 2kg, diethylene glycol ether 2kg, butyl 2kg and deionized water 62kg is taken respectively; (2) get refining Yatall MA and Monoethanolamine MEA BASF and trolamine to be heated to 100 DEG C and to react 45min to obtain lubricating and antirust agent for subsequent use; (3) in the deionized water taken, add Zulkovsky starch, diethylene glycol ether, butyl and fatty alcohol-ether phosphoric acid ester MOA-3P, mix, dissolve fully; (4) lubricating and antirust agent obtained for step (2) joined in the mixed solution that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
Embodiment 2
(1) refining Yatall MA 8kg, diethanolamine 4kg, fatty alcohol-ether phosphoric acid ester MOA-9P 5kg, Zulkovsky starch 5kg, diethylene glycol ether 5kg and deionized water 73kg is taken respectively; (2) get refining Yatall MA and diethanolamine to be heated to 80 DEG C and to react 100min to obtain lubricating and antirust agent for subsequent use; (3) in the deionized water taken, add Zulkovsky starch, diethylene glycol ether and fatty alcohol-ether phosphoric acid ester MOA-9P, mix, dissolve fully; (4) lubricating and antirust agent obtained for step (2) joined in the mixed solution that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
Embodiment 3
(1) refining Yatall MA 4kg, diethanolamine 14kg, fatty alcohol-ether phosphoric acid ester MOA-3P 6kg, fatty alcohol-ether phosphoric acid ester MOA-9P 2kg, Zulkovsky starch 2kg, diethylene glycol ether 2kg, Diethylene Glycol propyl ether 2kg and deionized water 68kg is taken respectively; (2) get refining Yatall MA and diethanolamine to be heated to 60 DEG C and to react 70min to obtain lubricating and antirust agent for subsequent use; (3) in the deionized water taken, add Zulkovsky starch, diethylene glycol ether, Diethylene Glycol propyl ether, fatty alcohol-ether phosphoric acid ester MOA-3P and fatty alcohol-ether phosphoric acid ester MOA-9P, mix, dissolve fully; (4) lubricating and antirust agent obtained for step (2) joined in the mixed solution that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
Embodiment 4
(1) refining Yatall MA 3kg, Monoethanolamine MEA BASF 1kg, trolamine 1kg, fatty alcohol-ether phosphoric acid ester MOA-3P 10kg, Zulkovsky starch 0.5kg, tripropylene glycol methyl ether 10kg and deionized water 74.5kg is taken respectively; (2) get refining Yatall MA and Monoethanolamine MEA BASF and trolamine to be heated to 50 DEG C and to react 120min to obtain lubricating and antirust agent for subsequent use; (3) in the deionized water taken, add Zulkovsky starch, tripropylene glycol methyl ether and fatty alcohol-ether phosphoric acid ester MOA-3P, mix, dissolve fully; (4) lubricating and antirust agent obtained for step (2) joined in the mixed solution that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
Embodiment 5
(1) refining Yatall MA 15kg, Monoethanolamine MEA BASF 8kg, diethanolamine 3kg, trolamine 4kg, fatty alcohol-ether phosphoric acid ester MOA-9P 1kg, Zulkovsky starch 10kg, tripropylene glycol ether 1kg and deionized water 58kg is taken respectively; (2) get refining Yatall MA and Monoethanolamine MEA BASF, diethanolamine and trolamine to be heated to 120 DEG C and to react 30min to obtain lubricating and antirust agent for subsequent use; (3) in the deionized water taken, add Zulkovsky starch, tripropylene glycol ether and fatty alcohol-ether phosphoric acid ester MOA-9P, mix, dissolve fully; (4) lubricating and antirust agent obtained for step (2) joined in the mixed solution that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
Embodiment 6
(1) refining Yatall MA 10kg, Monoethanolamine MEA BASF 8kg, diethanolamine 8kg, trolamine 4kg, fatty alcohol-ether phosphoric acid ester MOA-3P 8kg, Zulkovsky starch 2kg, diethylene glycol ether 2kg, butyl 2kg, tripropylene glycol methyl ether 4kg and deionized water 52kg; Get refining Yatall MA and Monoethanolamine MEA BASF, diethanolamine and trolamine to be heated to 90 DEG C and to react 60min to obtain lubricating and antirust agent for subsequent use; (3) in the deionized water taken, add Zulkovsky starch, diethylene glycol ether, butyl, tripropylene glycol methyl ether and fatty alcohol-ether phosphoric acid ester MOA-3P, mix, dissolve fully; (4) lubricating and antirust agent obtained for step (2) joined in the mixed solution that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
The rapid water baseline cutting working liquid that embodiment of the present invention 1-6 is obtained, tool has the following advantages:
1, refining Yatall MA lubricity used is superior, and cleaning performance is good and have certain anti-bubble effect, wide to the subject range of hard water, and easy cleaning after product uses, has good lubricating and antirust performance;
2, product Environmental Safety performance is good, avoid the greasy dirt, the oil smoke problem that use oily substance to produce, improve the surface quality of workpiece, also improve Working environment simultaneously, reduce discharge and the pollution of trade effluent, saved cost, product of the present invention the experiment proved that human non-toxic, has ensured the safety of staff;
3, product uses rear technological effect good, and not only increase process velocity fast, also improve cutting efficiency, the workpiece surface finish after processing is high, there is not blackout, burns silk problem;
4, product colour is transparent, and avoid the lamination problem of oiliness Linear cut working fluid, stable chemical performance, the quality guaranteed period is longer.
More than show and describe ultimate principle of the present invention, principal character and advantage, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these changes and improvements all fall into claimed scope of the present invention.
Claims (5)
1. a rapid water baseline cutting working liquid, it is characterized in that being prepared from by the raw material of following mass percentage: lubricating and antirust agent 5%-30%, phosphoric acid ester overstocks agent 1%-10%, explosive agent 0.5%-10%, alcohol ether couplant 1%-10%, surplus is deionized water, described lubricating and antirust agent is prepared from by refining Yatall MA and hydramine, wherein the quality proportioning of refining Yatall MA and hydramine is that m(refines Yatall MA): m(hydramine)=1:0.5-3.5, hydramine is Monoethanolamine MEA BASF, a kind of or two or more arbitrarily mixture in diethanolamine and trolamine, it is fatty alcohol-ether phosphoric acid ester MOA-3P or fatty alcohol-ether phosphoric acid ester MOA-9P that described phosphoric acid ester overstocks agent, described explosive agent is Zulkovsky starch, described alcohol ether couplant is diethylene glycol ether, Diethylene Glycol propyl ether, butyl, a kind of or two or more arbitrarily mixture in tripropylene glycol methyl ether and tripropylene glycol ether.
2. rapid water baseline cutting working liquid according to claim 1, it is characterized in that described lubricating and antirust agent is prepared from by following methods: first refine Yatall MA according to m(): m(hydramine) the quality proportioning of=1:0.5-3.5 takes refining Yatall MA and hydramine respectively, the refining Yatall MA taken and hydramine is mixed and heated to 50-120 DEG C of reaction 30-120min i.e. obtained lubricating and antirust agent.
3. rapid water baseline cutting working liquid according to claim 1, it is characterized in that being prepared from by the raw material of following mass percentage: refining Yatall MA 8%, Monoethanolamine MEA BASF 8%, trolamine 8%, fatty alcohol-ether phosphoric acid ester MOA-3P 8%, Zulkovsky starch 2%, diethylene glycol ether 2%, butyl 2% and deionized water 62%.
4. the preparation method of a rapid water baseline cutting working liquid according to claim 1, it is characterized in that comprising the following steps: (1) refines Yatall MA according to m(): m(hydramine) the quality proportioning of=1:0.5-3.5 takes refining Yatall MA and hydramine respectively, the refining Yatall MA taken and hydramine are mixed and heated to 50-120 DEG C of reaction 30-120min i.e. obtained lubricating and antirust agent, wherein hydramine is a kind of or two or more arbitrarily mixture in Monoethanolamine MEA BASF, diethanolamine and trolamine; (2) raw material is taken respectively according to following proportioning, lubricating and antirust agent 5%-30%, phosphoric acid ester overstock agent 1%-10%, explosive agent 0.5%-10%, alcohol ether couplant 1%-10%, surplus are deionized water, it is fatty alcohol-ether phosphoric acid ester MOA-3P or fatty alcohol-ether phosphoric acid ester MOA-9P that described phosphoric acid ester overstocks agent, described explosive agent is Zulkovsky starch, and described alcohol ether couplant is a kind of or two or more arbitrarily mixture in diethylene glycol ether, Diethylene Glycol propyl ether, butyl, tripropylene glycol methyl ether and tripropylene glycol ether; (3) in the deionized water taken, add explosive agent, alcohol ether couplant and phosphoric acid ester and overstock agent, mix, dissolve fully; (4) the lubricating and antirust agent taken joined in the mixing solutions that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
5. the preparation method of rapid water baseline cutting working liquid according to claim 4, it is characterized in that comprising the following steps: (1) takes the raw material of following quality proportioning respectively, refining Yatall MA 8%, Monoethanolamine MEA BASF 8%, trolamine 8%, fatty alcohol-ether phosphoric acid ester MOA-3P 8%, Zulkovsky starch 2%, diethylene glycol ether 2%, butyl 2% and deionized water 62% are for subsequent use; (2) get refining Yatall MA and Monoethanolamine MEA BASF and trolamine to be heated to 100 DEG C and to react 45min to obtain lubricating and antirust agent for subsequent use; (3) in the deionized water taken, add Zulkovsky starch, diethylene glycol ether, butyl and fatty alcohol-ether phosphoric acid ester MOA-3P, mix, dissolve fully; (4) lubricating and antirust agent obtained for step (2) joined in the mixed solution that step (3) formed, dissolve fully, be cooled to room temperature, measuring pH value is the rapid water baseline cutting working liquid that 8-9.5 is namely obtained qualified.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104818101A (en) * | 2015-03-19 | 2015-08-05 | 柳州市永益机械制造有限公司 | Preparation method for wire electrical discharge machining working fluid |
| CN106381200A (en) * | 2016-08-17 | 2017-02-08 | 吴江华威特种油有限公司 | Rust-preventative oil used for iron casting parts and a preparing method thereof |
| CN108467682A (en) * | 2018-05-25 | 2018-08-31 | 高阳 | A kind of preparation method of dark color leather shoes maintenance oil |
| CN109722332A (en) * | 2017-10-31 | 2019-05-07 | 宜兴市华青润滑材料科技有限公司 | A kind of highly enriched aqueous composition of Wire EDM |
| CN112980558A (en) * | 2021-03-01 | 2021-06-18 | 南宁珀源能源材料有限公司 | Sapphire cutting fluid and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103740452A (en) * | 2013-12-20 | 2014-04-23 | 开封恒锐新金刚石制品有限公司 | Environment-friendly cooling liquid for diamond wire cutting and preparation method thereof |
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2014
- 2014-10-27 CN CN201410578454.7A patent/CN104388170B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103740452A (en) * | 2013-12-20 | 2014-04-23 | 开封恒锐新金刚石制品有限公司 | Environment-friendly cooling liquid for diamond wire cutting and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104818101A (en) * | 2015-03-19 | 2015-08-05 | 柳州市永益机械制造有限公司 | Preparation method for wire electrical discharge machining working fluid |
| CN106381200A (en) * | 2016-08-17 | 2017-02-08 | 吴江华威特种油有限公司 | Rust-preventative oil used for iron casting parts and a preparing method thereof |
| CN109722332A (en) * | 2017-10-31 | 2019-05-07 | 宜兴市华青润滑材料科技有限公司 | A kind of highly enriched aqueous composition of Wire EDM |
| CN108467682A (en) * | 2018-05-25 | 2018-08-31 | 高阳 | A kind of preparation method of dark color leather shoes maintenance oil |
| CN112980558A (en) * | 2021-03-01 | 2021-06-18 | 南宁珀源能源材料有限公司 | Sapphire cutting fluid and preparation method thereof |
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| CN104388170B (en) | 2017-07-25 |
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