CN104371806A - Anti-rust oil containing cerium oxide and preparation method of anti-rust oil - Google Patents
Anti-rust oil containing cerium oxide and preparation method of anti-rust oil Download PDFInfo
- Publication number
- CN104371806A CN104371806A CN201410590484.XA CN201410590484A CN104371806A CN 104371806 A CN104371806 A CN 104371806A CN 201410590484 A CN201410590484 A CN 201410590484A CN 104371806 A CN104371806 A CN 104371806A
- Authority
- CN
- China
- Prior art keywords
- parts
- cerium oxide
- oil
- benzoate
- rust
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Preventing Corrosion Or Incrustation Of Metals (AREA)
Abstract
The invention discloses anti-rust oil containing cerium oxide and a preparation method of the anti-rust oil. The anti-rust oil is prepared from the following raw materials in parts by weight: 58-70 parts of organic silicone oil, 3.5-4.5 parts of barium petroleum sulfonate, 10-12 parts of cerium oxide, 20-25 parts of magnesium hydroxide, 4-6 parts of spirulina powder, 2-3 parts of benzotriazole, 1-3 parts of magnesium stearate, 4-5 parts of triethanolamine oleate, 5-7 parts of sodium dodecyl benzene sulfonate, 3-5 parts of ammonium molybdate, 2-4 parts of microcrystalline cellulose, 5-6 parts of cyclohexylamine benzoate, 3-4 parts of ammonium benzoate, 1-2 parts of sodium hexametaphosphate, 2-4 parts of antioxidant 1010, 3-5 parts of 2-methyl-4-ethylimidazole and 2-4 parts of N-methyl pyrrolidone. According to the method, defects of the prior art are overcome, the anti-rust property of the product is greatly improved, the weather tolerance can be effectively improved by adding cerium oxide rare-earth oxide into the anti-rust oil, the surface tension of an oil film can be improved, and the oil film has good spreadability on the surface of a metal base material. The anti-rust oil can be applied to anti-rust application in various fields.
Description
Technical field
The present invention relates to a kind of process for treating surface, be specifically related to a kind of containing cerium oxide slushing oil and preparation method thereof.
Background technology
Corrosion almost spreads all trades and professions, and its harm is very surprising, so slushing oil just arises at the historic moment.In machinofacture, transport, storage and normal logistics, slushing oil plays very important effect; But the development imbalances of every profession and trade, the production dispersion of processing slushing oil, the multiplex company standard of antirust grease production quality control, the kind that quality is close has different company standards.Though kind increases year by year, good and the bad difficulty point, uses confusion; No matter be in production, store, circulate or in use, have more serious corrosion phenomenon, propose more and more higher requirement to the metallic element of automobile is antirust; But at present industrial production not only lacks effective technique means for various metals alloy is antirust, and antirust valuable product.
Summary of the invention
The object of the present invention is to provide a kind of containing cerium oxide slushing oil and preparation method thereof.
The present invention adopts following technical scheme to achieve these goals:
Containing cerium oxide slushing oil, the weight part of its constitutive material is: organic silicone oil 58-70, barium mahogany sulfonate 3.5-4.5, cerium oxide 10-12, magnesium hydroxide 20-25, spirulina powder 4-6,124 Triazole 2-3, Magnesium Stearate 1-3, triethanolamine oleate 4-5, Sodium dodecylbenzene sulfonate 5-7, ammonium molybdate 3-5, Microcrystalline Cellulose 2-4, benzoate amine 5-6, Ammonium benzoate 3-4, Sodium hexametaphosphate 99 1-2, antioxidant 1010 2-4,2-methyl-4-ethyl imidazol(e) 3-5 and N-Methyl pyrrolidone 2-4.
Containing cerium oxide slushing oil, the weight part of its constitutive material is: organic silicone oil 65, barium mahogany sulfonate 4, cerium oxide 11, magnesium hydroxide 22, spirulina powder 5,124 Triazole 2.5, Magnesium Stearate 2, triethanolamine oleate 4.5, Sodium dodecylbenzene sulfonate 6, ammonium molybdate 4, Microcrystalline Cellulose 3, benzoate amine 5.5, Ammonium benzoate 3.5, Sodium hexametaphosphate 99 1.5, antioxidant 1010 3,2-methyl-4-ethyl imidazol(e) 4 and N-Methyl pyrrolidone 3.
Preparation method containing cerium oxide slushing oil, comprises the following steps:
(1) measure organic silicone oil by the weight part of constitutive material, add heated and stirred in reactor, to adding Magnesium Stearate, Sodium dodecylbenzene sulfonate, ammonium molybdate and Sodium hexametaphosphate 99 during 150-160 DEG C, stirring reaction 15-20min;
(2) cerium oxide, magnesium hydroxide and spirulina powder is taken by weight, grind rear mixing respectively, then add appropriate dehydrated alcohol, sinter 40-50 minute after mixing at temperature 600-700 DEG C, after sintering, recycling dehydrated alcohol is that medium milling pulping is for subsequent use;
(4) add the slurry for subsequent use of barium mahogany sulfonate, Microcrystalline Cellulose, benzoate amine, Ammonium benzoate and step (2) in step (1), be warming up to 180-200 DEG C, continue to stir, react after 40-50 minute, be cooled to 40-50 DEG C;
(5) in step (4), add other constitutive material by the weight part of constitutive material, after continuing to stir 4-5h filtration, get product.
Beneficial effect of the present invention:
Instant invention overcomes the deficiencies in the prior art, greatly improve the rust-preventing characteristic of product, adding cerium oxide rare earth oxide at slushing oil effectively can improve weathering resistance, improves the surface tension of oil film, good in the spreadability of metallic substrate surface, the present invention goes in the antirust application of each row.
Embodiment
Embodiment 1: containing cerium oxide slushing oil, the weight part (kg) of its constitutive material is: organic silicone oil 65, barium mahogany sulfonate 4, cerium oxide 11, magnesium hydroxide 22, spirulina powder 5,124 Triazole 2.5, Magnesium Stearate 2, triethanolamine oleate 4.5, Sodium dodecylbenzene sulfonate 6, ammonium molybdate 4, Microcrystalline Cellulose 3, benzoate amine 5.5, Ammonium benzoate 3.5, Sodium hexametaphosphate 99 1.5, antioxidant 1010 3,2-methyl-4-ethyl imidazol(e) 4 and N-Methyl pyrrolidone 3.
Preparation method containing cerium oxide slushing oil, comprises the following steps:
(1) measure organic silicone oil by the weight part of constitutive material, add heated and stirred in reactor, add Magnesium Stearate, Sodium dodecylbenzene sulfonate, ammonium molybdate and Sodium hexametaphosphate 99 to when 155 DEG C, stirring reaction 20min;
(2) take cerium oxide, magnesium hydroxide and spirulina powder by weight, grind rear mixing respectively, then add appropriate dehydrated alcohol, sinter 45 minutes after mixing at temperature 650 DEG C, after sintering, recycling dehydrated alcohol is that medium milling pulping is for subsequent use;
(4) add the slurry for subsequent use of barium mahogany sulfonate, Microcrystalline Cellulose, benzoate amine, Ammonium benzoate and step (2) in step (1), be warming up to 190 DEG C, continue to stir, react after 45 minutes, be cooled to 40-50 DEG C;
(5) in step (4), add other constitutive material by the weight part of constitutive material, after continuing to stir 4-5h filtration, get product.
The over-all properties of slushing oil prepared by above-described embodiment 1 is as follows: sticking power/level≤2 grade; 2, neutral salt spray corrosion test (h) >=92; 3, humid heat test (h) > 1100; 4, oil film time of drying (min) 14-15; 5, coating thickness (μm) < 4.1.
Claims (3)
1., containing a cerium oxide slushing oil, it is characterized in that the weight part of its constitutive material is: organic silicone oil 58-70, barium mahogany sulfonate 3.5-4.5, cerium oxide 10-12, magnesium hydroxide 20-25, spirulina powder 4-6,124 Triazole 2-3, Magnesium Stearate 1-3, triethanolamine oleate 4-5, Sodium dodecylbenzene sulfonate 5-7, ammonium molybdate 3-5, Microcrystalline Cellulose 2-4, benzoate amine 5-6, Ammonium benzoate 3-4, Sodium hexametaphosphate 99 1-2, antioxidant 1010 2-4,2-methyl-4-ethyl imidazol(e) 3-5 and N-Methyl pyrrolidone 2-4.
2. according to claim 1 containing cerium oxide slushing oil, it is characterized in that the weight part of its constitutive material is: organic silicone oil 65, barium mahogany sulfonate 4, cerium oxide 11, magnesium hydroxide 22, spirulina powder 5,124 Triazole 2.5, Magnesium Stearate 2, triethanolamine oleate 4.5, Sodium dodecylbenzene sulfonate 6, ammonium molybdate 4, Microcrystalline Cellulose 3, benzoate amine 5.5, Ammonium benzoate 3.5, Sodium hexametaphosphate 99 1.5, antioxidant 1010 3,2-methyl-4-ethyl imidazol(e) 4 and N-Methyl pyrrolidone 3.
3. the preparation method containing cerium oxide slushing oil as claimed in claim 1, is characterized in that comprising the following steps:
(1) measure organic silicone oil by the weight part of constitutive material, add heated and stirred in reactor, to adding Magnesium Stearate, Sodium dodecylbenzene sulfonate, ammonium molybdate and Sodium hexametaphosphate 99 during 150-160 DEG C, stirring reaction 15-20min;
(2) cerium oxide, magnesium hydroxide and spirulina powder is taken by weight, grind rear mixing respectively, then add appropriate dehydrated alcohol, sinter 40-50 minute after mixing at temperature 600-700 DEG C, after sintering, recycling dehydrated alcohol is that medium milling pulping is for subsequent use;
(4) add the slurry for subsequent use of barium mahogany sulfonate, Microcrystalline Cellulose, benzoate amine, Ammonium benzoate and step (2) in step (1), be warming up to 180-200 DEG C, continue to stir, react after 40-50 minute, be cooled to 40-50 DEG C;
(5) in step (4), add other constitutive material by the weight part of constitutive material, after continuing to stir 4-5h filtration, get product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410590484.XA CN104371806A (en) | 2014-10-29 | 2014-10-29 | Anti-rust oil containing cerium oxide and preparation method of anti-rust oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410590484.XA CN104371806A (en) | 2014-10-29 | 2014-10-29 | Anti-rust oil containing cerium oxide and preparation method of anti-rust oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104371806A true CN104371806A (en) | 2015-02-25 |
Family
ID=52551004
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410590484.XA Pending CN104371806A (en) | 2014-10-29 | 2014-10-29 | Anti-rust oil containing cerium oxide and preparation method of anti-rust oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104371806A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106318572A (en) * | 2016-08-10 | 2017-01-11 | 东至县洋湖镇希望皮具厂 | Leather product zipper lubricating oil |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103352217A (en) * | 2013-06-21 | 2013-10-16 | 安徽省六安市朝晖机械制造有限公司 | Surface bluing anti-rust treatment process for workpiece |
| CN103966005A (en) * | 2014-03-28 | 2014-08-06 | 安徽九华金润铜业有限公司 | Drawing fluid for rapidly drawing copper wire |
| CN104004567A (en) * | 2014-04-25 | 2014-08-27 | 蚌埠市鸿安精密机械有限公司 | Antirust oil containing rare earth compound |
-
2014
- 2014-10-29 CN CN201410590484.XA patent/CN104371806A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103352217A (en) * | 2013-06-21 | 2013-10-16 | 安徽省六安市朝晖机械制造有限公司 | Surface bluing anti-rust treatment process for workpiece |
| CN103966005A (en) * | 2014-03-28 | 2014-08-06 | 安徽九华金润铜业有限公司 | Drawing fluid for rapidly drawing copper wire |
| CN104004567A (en) * | 2014-04-25 | 2014-08-27 | 蚌埠市鸿安精密机械有限公司 | Antirust oil containing rare earth compound |
Non-Patent Citations (3)
| Title |
|---|
| 刘程 李江华 刘博 孙丽艳: "《表面活性剂应用手册》", 30 September 2004, 化学工业出版社 * |
| 张大全: "《气相缓蚀剂及其应用》", 30 April 2007, 化学工业出版社 * |
| 王毓民: "《润滑材料与润滑技术》", 31 January 2005, 化学工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106318572A (en) * | 2016-08-10 | 2017-01-11 | 东至县洋湖镇希望皮具厂 | Leather product zipper lubricating oil |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR101613952B1 (en) | Water soluble composition for waterproof coating | |
| CN103254978B (en) | Anti-rust oil and preparation method thereof | |
| CN104177895A (en) | Graphene or graphite oxide-based anticorrosive coating and preparation method thereof | |
| CN107653045A (en) | Antirust oil and preparation method thereof | |
| CN104312657A (en) | Anti-rust oil for auto parts and preparation method thereof | |
| CN103087572A (en) | Surface silanization protection treatment agent for hard aluminum alloy and preparation method thereof | |
| CN103882451B (en) | A kind of water base normal temperature rust-removing and antirusting agent and preparation method thereof | |
| CN103820788B (en) | A kind of antirust agent containing modified mullite powder | |
| CN103555104A (en) | High molecular material special for corrosion prevention of steel and iron, and preparation method and application process thereof | |
| CN104371806A (en) | Anti-rust oil containing cerium oxide and preparation method of anti-rust oil | |
| CN103254796A (en) | Anti-rust oil for automobile parts and preparation method thereof | |
| CN103254795A (en) | Damp and heat highly-resistant antirust oil and preparation method thereof | |
| CN103254979B (en) | Multi-base-oil anti-rust oil and preparation method thereof | |
| CN105907208A (en) | Water-based metal anticorrosion thermal insulation compound paint and preparation method thereof | |
| JP6764521B2 (en) | Aqueous high temperature heat resistant titanium steel antibonding coating and its use | |
| CN104911578A (en) | Green environment-friendly aqueous rust inhibitor and preparation method thereof | |
| CN105647631A (en) | A lubricating fluid for high-speed fine wire drawing of copper wires and a preparing method thereof | |
| CN107057572A (en) | A kind of antirusting paint of automobile chassis and preparation method thereof | |
| CN103497805A (en) | Rust preventive oil and preparation method thereof | |
| CN102993817A (en) | Metal rust inhibitor containing peregal O | |
| CN103232814A (en) | Dehydration anti-rust oil and preparation method thereof | |
| CN103484200A (en) | Soft film anti-rust oil | |
| CN103254785A (en) | Long-acting anti-rust oil and preparation method thereof | |
| CN103087569A (en) | Surface silanization protection treatment agent for stainless steel plates and preparation method thereof | |
| CN101698543B (en) | Closed circulating water corrosion inhibitor, preparation method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160525 Address after: Luyang District of Hefei City Shouchun road 230001 Anhui province No. 356 merchants International Building room 1407 Applicant after: HEFEI ZHENGTUO DECORATION MATERIALS CO., LTD. Address before: 230011 Luyang Industrial Park, Fuyang North Road, Luyang District, Anhui, Hefei Applicant before: Hefei Huayang Construction Machinery Co.,Ltd. |
|
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150225 |
|
| RJ01 | Rejection of invention patent application after publication |