CN104366466A - Wall-broken walnut pollen as well as preparation method and application of wall-broken walnut pollen - Google Patents
Wall-broken walnut pollen as well as preparation method and application of wall-broken walnut pollen Download PDFInfo
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- CN104366466A CN104366466A CN201410550387.8A CN201410550387A CN104366466A CN 104366466 A CN104366466 A CN 104366466A CN 201410550387 A CN201410550387 A CN 201410550387A CN 104366466 A CN104366466 A CN 104366466A
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- 241000758789 Juglans Species 0.000 title claims abstract description 136
- 235000009496 Juglans regia Nutrition 0.000 title claims abstract description 136
- 235000020234 walnut Nutrition 0.000 title claims abstract description 136
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 41
- 239000000463 material Substances 0.000 claims abstract description 20
- 238000007710 freezing Methods 0.000 claims abstract description 19
- 230000008014 freezing Effects 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 30
- 239000000843 powder Substances 0.000 claims description 25
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- 238000002525 ultrasonication Methods 0.000 claims description 13
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- 238000010257 thawing Methods 0.000 claims description 5
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- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 2
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- 102000004169 proteins and genes Human genes 0.000 description 2
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- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 description 2
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- 206010020772 Hypertension Diseases 0.000 description 1
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- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 1
- 239000004472 Lysine Substances 0.000 description 1
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- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
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- 239000001814 pectin Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention relates to a walnut pollen wall breaking method, a walnut pollen tablet and a preparation method thereof. The walnut pollen wall breaking method comprises the following steps: freezing walnut pollen at the temperature of -20 DEG C for 24 hours and adding the walnut pollen into water being 60 DEG C according to a material-liquid ratio being 1 to 15; and carrying out ultrasonic treatment by an ultrasonic cell crusher under the conditions that the ultrasonic power is 720w and the ultrasonic time is 30 minutes to break walls of the walnut pollen. The walnut pollen broken by the method is adopted and a food auxiliary material accounting for a certain ratio of the walnut pollen is added; and the materials are uniformly mixed and are subjected to tabletting to obtain the walnut pollen tablets.
Description
Technical field
The present invention relates to field of food, be specifically related to walnut flower powder wall breaking method, walnut pollen tablet and preparation method thereof.
Background technology
Walnut is one of large nut in the world four, has the cultivation history of more than 2,000 year in China.In recent years, along with the increase of walnut cultivated area, the walnut total output of China more ranks first in the world.Walnut male flower is amentum, and each inflorescence can produce pollen 0.08-0.20g, and the walnut in the best fruiting period has a large amount of male flower and grows, and therefore the source of walnut pollen is very abundant.
Walnut pollen has higher nutritive value.It is reported, walnut pollen protein content is 26.59%, higher than the protein content in corn, pollen of Semen Fagopyri Esculenti.Total amino acid content is 23.70%, in China 34 in nectariferous plant, its pollen total amino acid content is occupied the forefront, wherein 8 kinds of essential amino acid total amounts are 9.61%, ratio and the E/T ratio of essential amino acid and total amino acid content are 40.55%, the amino acid ratio reached in ideal protein requires (Yu Xiuling, Deng. walnut pollen Analysis of Nutritive Composition and evaluation, forestry science and technology is developed, 2007, 21 (3): 45-47.), and lysine content enriches, therefore walnut pollen and cereal staple food can improve the nutritive value of protein greatly by amino acid complementation.Walnut pollen fat content is 5.45%, and reducing sugar content is 5.70%.In addition, walnut pollen also has the feature of high potassium, low sodium, and the content of calcium, magnesium, phosphorus is higher, and in trace element, the content of zinc, selenium belongs to higher row compared with other pollen, and in vitamin, Vc content is the highest.Wherein the feature of hyperkalemia hyponatremia to preventing and treat hypertension, kidney trouble has certain benefit, the growth of tooth, the formation of bone are played an important role.Magnesium is the indispensable element of cellular metabolism, calcium can regulate heartbeat, by blood clotting required.Zn-ef ficiency is to the facilitation of having grown of human body, and selenium element participates in the synthesis of glutathione peroxidase, has the effect suppressing peroxidization, scavenging free radicals, decompose hydroperoxide and reparation molecular damage.As can be seen here, walnut pollen has high nutritive value.
The structure of walnut flower powder has two layers of walls, outer wall is thicker, it has decorative pattern and color, has sporopollenin (being the oxidation polymer derivative of carotenoid and carotenoid ester) in the composition of composition outer wall, character is firm, has characteristic that is antiacid and antibiont decomposition; Inwall is thin, is made up of pectin and cellulose.Because outer wall construction that pollen is special prevents the release of nutriment, in order to improve the value of pollen, the broken wall of pollen is just particularly important.And after broken wall walnut pollen is made tablet, not only can retain original abundant nutrition, also there is instant, be easy to absorb, be beneficial to the features such as seasoning.But, the wall-breaking method sporoderm-broken rate of prior art center peach flower powder is lower, or destroy the nutritive value of walnut pollen, or technical matters is complicated, cost is higher, or be not suitable for extensive use, therefore this area needs that a kind of technique is simple, cost is lower, be applicable to extensive use badly, and the wall-breaking method of the walnut pollen of sporoderm-broken rate high, less destruction walnut pollen nutritive value.And broken wall walnut pollen is prepared into walnut flower powder preparation, for making full use of walnut pollen resource, enrich health food market also significant.
Summary of the invention
Inventor finds unexpectedly, and adopt the temperature difference of the present invention-ultrasonic disruption combined techniques to carry out broken wall to walnut pollen, the more independent temperature difference or ultrasonic fragmentation substantially increase sporoderm-broken rate and the nutritive value of walnut pollen, achieve unexpected technique effect.
A first aspect of the present invention provides a kind of broken wall walnut pollen, and it is characterized in that, sporoderm-broken rate is at 80%-90%.
Broken wall walnut pollen of the present invention is obtained by the temperature difference-ultrasonic disruption combined techniques, add hot water after the described temperature difference-ultrasonic disruption combined techniques is freezing under comprising the steps: that walnut pollen is placed in cryogenic conditions to thaw, then be walnut pollen broken wall in conjunction with ultrasonication effect.
In one embodiment, the described temperature difference-ultrasonic disruption combined techniques comprises the steps:
Add 60 DEG C of water with the solid-liquid ratio of 1:15 after freezing 24h under walnut pollen being placed in the cryogenic temperature of-20 DEG C and carry out thawing 1h, after thawing, adopt ultrasonic cell disruption instrument, ultrasonic power be 720w, ultrasonic time carries out ultrasonication process under being the condition of 30min, obtain the walnut pollen suspension after broken wall, after concentrated by rotary evaporation, adopt freeze-drying to carry out drying to walnut pollen suspension, obtain broken wall walnut pollen.
A second aspect of the present invention provides a kind of walnut flower powder preparation, it is characterized in that, comprises broken wall walnut pollen of the present invention; Preferably, described preparation is tablet.
In one embodiment, described tablet also comprises edible auxiliary material.
In one embodiment, described auxiliary material is selected from sweetener, acid, milk powder, adhesive, lubricant or its combination.
In one embodiment, the addition of described sweetener is 5 ~ 20% of broken wall walnut flower opaque amount, the addition of described milk powder is 5 ~ 30% of broken wall walnut flower opaque amount, the addition of described acid is 0.4 ~ 1.0% of broken wall walnut flower opaque amount, the described addition of adhesive that selects is 3 ~ 5% of broken wall walnut flower opaque amount, 4 ~ 6% of the broken wall walnut flower opaque amount that the addition of described lubricant is.
In one embodiment, described in, described sweetener is at least one in sucrose, xylitol, glucose, and described acid is at least one in citric acid, malic acid, light-coloured vinegar, and described adhesive is microcrystalline cellulose, and described lubricant is cornstarch.
In one embodiment, described sweetener is white granulated sugar, and described acid is citric acid, and described adhesive is microcrystalline cellulose, and described lubricant is cornstarch.
A third aspect of the present invention provides the preparation method of walnut pollen tablet of the present invention, it is characterized in that, comprises the following steps: by described broken wall walnut pollen and described auxiliary materials and mixing, utilize rotary tablet press, obtains walnut pollen tablet.
Accompanying drawing explanation
Fig. 1 is walnut pollen broken wall and tablet producing technology flow chart thereof.
Fig. 2 is natural nucleus peach flower powder electromicroscopic photograph.
Fig. 3 is broken wall walnut pollen electromicroscopic photograph.
Detailed description of the invention
Add hot water after walnut flower powder wall breaking method of the present invention is freezing under comprising the steps: that walnut pollen is placed in cryogenic conditions to thaw, then make walnut pollen broken wall in conjunction with ultrasonication effect.
Broken wall walnut pollen preparation flow can schematically as follows:
Walnut pollen → removal of impurities → cryogenic freezing → high temperature thaws → and ultrasonication process → drying → sieve → broken wall walnut pollen
Wherein, in order to improve walnut rate of breaking pollen wall in the inventive method, be preferably as follows scheme: walnut pollen is freezing 12 ~ 36h under being placed in the freezing environment of-20 DEG C, then with walnut flower grain weight amount 5 ~ 25 times, temperature 40 ~ 95 DEG C hot water to walnut pollen thaw process 0.5-4h, then adopt ultrasonic cell disruptor to carry out ultrasonic process under the condition of ultrasonic power 480 ~ 960w, ultrasonic time 15 ~ 35min, after freeze drying, obtain broken wall walnut pollen.More preferably following scheme: under walnut pollen is placed in-20 DEG C of freezing conditions, freezing 24 hours, then carry out thawing 1h with the hot water that walnut flower grain weight amount 15 times, temperature are 60 DEG C, then under the condition of ultrasonic power 720w, ultrasonication time 30min, carry out ultrasonic process, after freeze drying, obtain broken wall walnut pollen.
Wherein, adopt this optimal case to carry out broken wall treatment to walnut pollen, sporoderm-broken rate can reach 88.72%.
Walnut pollen tablet of the present invention adopts said method broken wall walnut pollen to be raw material, is prepared from by adding acceptable auxiliary material in bromatology.
Walnut pollen tablet preparation flow can schematically as follows:
Raw material preparation → weighing → pulverizing → allotment → hybrid bonding → granulation → whole grain → compressing tablet → quality inspection → packaging → finished product
Wherein, according to specific needs, the tablet that different taste made by different auxiliary materials can be added.Described auxiliary material comprises sweetener, milk powder, acid, adhesive, lubricant, wherein sweetener is at least one in sucrose, xylitol, glucose, acid is at least one in citric acid, malic acid, light-coloured vinegar, and adhesive is microcrystalline cellulose, and lubricant is cornstarch.
Selected sweetener is white granulated sugar, addition is 5 ~ 20% of pollen quality, and the amount of adding milk powder is 5 ~ 30% of walnut flower opaque amount, and selected acid is citric acid, addition is 0.4 ~ 1.0% of walnut flower opaque amount, selected adhesive is microcrystalline cellulose, and addition is 3 ~ 5% of walnut flower opaque amount, and selected lubricant is cornstarch, addition is 4 ~ 6% of walnut flower opaque amount, by various main ingredient through mixing, rotary tablet press, obtains broken wall walnut pollen milk sheet.
The gatherer process of walnut pollen is:
When walnut male flower inflorescence starts individually loose powder, gathering base portion will the inflorescence of loose powder (inflorescence is by green flavescence) or just loose powder, be placed on dry indoor tiling to dry, temperature remains on 20 ~ 25 DEG C of conditions, gets final product loose powder through 2 ~ 3 days, then by pollen collecting in valve bag, obturage, for subsequent use under being placed in the cryogenic conditions of 2 ~ 5 DEG C, suitably breathe freely, in case mouldy.Through measuring every 500 grams of male inflorescences after collection, pollen 15.37 grams after drying in the shade, can be gone out.
The assay method of rate of breaking pollen wall is:
Accurately take containing equivalent broken wall walnut pollen samples and natural nucleus peach flower powder, make unit for uniform suspension, capillary is used to draw identical amount film-making, use biology microscope sem observation sample, advance position observation 9 visuals field, record complete pollen grain number, each sample repeats film-making 3, and computing formula is as follows:
Rate of breaking pollen wall=(after 1-broken wall before remaining complete walnut flower powder number/broken wall complete walnut flower powder number) × 100%
Key instrument equipment:
Electronic balance: FA type, Shanghai Precision Scientific Apparatus Co., Ltd;
Electric-heated thermostatic water bath: HWSY type, mayor of Beijing bearing instruments and meters Co., Ltd;
Ultrasonic cell disruptor: JY98-IIIDN, Ningbo Xin Yi ultrasonic device Co., Ltd;
Constant Temp. Oven: 101 type Beijing Ke Weiyongxin experimental instrument and equipment factories;
Vacuum freeze drier: LGJ-100F, Beijing development in science and technology Co., Ltd of Song Yuan Huaxing;
Microscope: CH20-BIM, the graceful bio tech ltd of Hypon on Olympus;
SEM: Hitachi SEM-2500, Japan;
Rotary tablet machine: ZPSX10 type, Shanghai is along auspicious pharmaceutical machine Co., Ltd.
Below in conjunction with embodiment, the specific embodiment of the present invention is further described, does not therefore limit the present invention among described scope of embodiments.
Experimental technique described in following embodiment, if no special instructions, is conventional method; Described reagent and material, if no special instructions, all can obtain from commercial channels.
Embodiment 1
The preparation of walnut pollen broken wall and tablet thereof:
(1) take 200g walnut pollen be placed in the freezing environment of-20 DEG C under freezing 12h.(2) with 1000g temperature 40 DEG C water (being incubated with water-bath) to walnut pollen thaw process 0.5h.(3) ultrasonic cell disruptor is then adopted to carry out ultrasonication process under the condition of ultrasonic power 480w, ultrasonic time 15min.(4) obtain broken wall walnut pollen after freeze drying, its sporoderm-broken rate is 80.10%.(5) take 100g broken wall walnut pollen, add 20g white granulated sugar, the milk powder of 30g, 1g citric acid, 3g microcrystalline cellulose, mixing.(6) material of mixing is placed in baking oven carries out drying.(7) carry out after drying pulverizing, sieving, make material have good mobility.(8) before compressing tablet, 4g cornstarch is added as lubricant, mixing.(9) rotary tablet machine is used to carry out compressing tablet.(10) tablet is packed, being up to the standards is broken wall walnut pollen tablet.
Embodiment 2
The preparation of walnut pollen broken wall and tablet thereof:
(1) take 100g walnut pollen be placed in the freezing environment of-20 DEG C under freezing 24h.(2) with 1500g temperature 60 DEG C water (being incubated with water-bath) to walnut pollen thaw process 1h.(3) ultrasonic cell disruptor is then adopted to carry out ultrasonication process under the condition of ultrasonic power 720w, ultrasonic time 30min.(4) obtain broken wall walnut pollen after freeze drying, its sporoderm-broken rate is 88.72%.(5) take 50g broken wall walnut pollen, add 2.5g white granulated sugar, the milk powder of 10g, 0.2g citric acid, 2g microcrystalline cellulose, mixing.(6) material of mixing is placed in baking oven carries out drying.(7) carry out after drying pulverizing, sieving, make material have good mobility.(8) before compressing tablet, 2.5g cornstarch is added as lubricant, mixing.(9) rotary tablet machine is used to carry out compressing tablet.(10) tablet is packed, being up to the standards is broken wall walnut pollen tablet.
Embodiment 3
The preparation of walnut pollen broken wall and tablet thereof:
(1) take 200g walnut pollen be placed in the freezing environment of-20 DEG C under freezing 30h.(2) with 4000g temperature 80 DEG C water (being incubated with water-bath) to walnut pollen thaw process 2h.(3) ultrasonic cell disruptor is then adopted to carry out ultrasonication process under the condition of ultrasonic power 900w, ultrasonic time 25min.(4) obtain broken wall walnut pollen after freeze drying, its sporoderm-broken rate is 83.45%.(5) take 100g broken wall walnut pollen, add 10g white granulated sugar, 10g milk powder, 0.6g citric acid, 5g microcrystalline cellulose, mixing.(6) material of mixing is placed in baking oven carries out drying.(7) carry out after drying pulverizing, sieving, make material have good mobility.(8) before compressing tablet, 6g cornstarch is added as lubricant, mixing.(9) rotary tablet machine is used to carry out compressing tablet.(10) tablet is packed, being up to the standards is broken wall walnut pollen tablet.
Embodiment 4
The preparation of walnut pollen broken wall and tablet thereof:
(1) take 100g walnut pollen be placed in the freezing environment of-20 DEG C under freezing 36h.(2) with 2500g temperature 95 DEG C water (being incubated with water-bath) to walnut pollen thaw process 4h.(3) ultrasonic cell disruptor is then adopted to carry out ultrasonication process under the condition of ultrasonic power 960w, ultrasonic time 35min.(4) obtain broken wall walnut pollen after freeze drying, its sporoderm-broken rate is 84.50%.(5) take 50g broken wall walnut pollen, add 7.5g white granulated sugar, the milk powder of 2.5g, 0.4g citric acid, 2.5g microcrystalline cellulose, mixing.(6) material of mixing is placed in baking oven carries out drying.(7) carry out after drying pulverizing, sieving, make material have good mobility.(8) before compressing tablet, 3g cornstarch is added as lubricant, mixing.(9) rotary tablet machine is used to carry out compressing tablet.(10) tablet is packed, being up to the standards is broken wall walnut pollen tablet.
Embodiment 5
Determine the impact of different wall-breaking method on walnut rate of breaking pollen wall and nutritional labeling extracted amount, see the following form.
The different wall-breaking method of table 1 is on the impact of walnut rate of breaking pollen wall and nutritional labeling extracted amount
From table 1, the temperature difference-ultrasonication combined techniques with adopt temperature differential method or sonioation method broken wall separately, greatly can improve sporoderm-broken rate, after broken wall, total reducing sugar, fat, water soluble vitamin, leachable Zn content are significantly increased, and become multiple to increase, become positive correlation with sporoderm-broken rate.Visible, the temperature difference-ultrasonication combined techniques does not obtain higher sporoderm-broken rate, and leachable nutrient composition content is improved greatly.
Nutrient component determining method:
Total sugar content measures: adopt improvement Fehling Regent method.
Fat content: the pollen through different disposal taking equal in quality, adopts extracted with diethyl ether, and sea can measure fat content by SOX500 Milko-Tester.
Water-soluble zinc measures: the sample taking a certain amount of different disposal, in volumetric flask, uses pure water constant volume, and spend the night after vibration 15min, then centrifuging and taking supernatant, uses atomic absorption spectroscopy determination.
Vitamin B6, vitamin E and C: adopt high performance liquid chromatography.
Claims (10)
1. a broken wall walnut pollen, is characterized in that, sporoderm-broken rate is at 80%-90%.
2. broken wall walnut pollen according to claim 1, it is characterized in that, described broken wall walnut pollen is obtained by the temperature difference-ultrasonic disruption combined techniques, add hot water after the described temperature difference-ultrasonic disruption combined techniques is freezing under comprising the steps: that walnut pollen is placed in cryogenic conditions to thaw, then make walnut pollen broken wall in conjunction with ultrasonication effect.
3. broken wall walnut pollen according to claim 2, is characterized in that, the described temperature difference-ultrasonic disruption combined techniques comprises the steps:
Add 40 ~ 95 DEG C of water with the solid-liquid ratio of 1:5 ~ 1:25 after freezing 12 ~ 36h under walnut pollen being placed in the cryogenic temperature of-40 ~-20 DEG C and carry out thawing 0.5 ~ 4h, after thawing, adopt ultrasonic cell disruption instrument, ultrasonic power be 480 ~ 960w, ultrasonic time carries out ultrasonication process under being the condition of 15 ~ 35min, obtain the walnut pollen suspension after broken wall, after concentrated by rotary evaporation, adopt freeze-drying to carry out drying to walnut pollen suspension, obtain broken wall walnut pollen.
4. a walnut flower powder preparation, is characterized in that, comprises the broken wall walnut pollen according to any one of claims 1 to 3; Preferably, described preparation is tablet.
5. walnut pollen tablet according to claim 4, is characterized in that, also comprise edible auxiliary material.
6. walnut pollen tablet according to claim 5, is characterized in that, described auxiliary material is selected from sweetener, acid, milk powder, adhesive, lubricant or its combination.
7. walnut pollen tablet according to claim 6, it is characterized in that, the addition of described sweetener is 5 ~ 20% of broken wall walnut flower opaque amount, the addition of described milk powder is 5 ~ 30% of broken wall walnut flower opaque amount, the addition of described acid is 0.4 ~ 1.0% of broken wall walnut flower opaque amount, the described addition of adhesive that selects is 3 ~ 5% of broken wall walnut flower opaque amount, 4 ~ 6% of the broken wall walnut flower opaque amount that the addition of described lubricant is.
8. the walnut pollen tablet according to claim 6 or 7, it is characterized in that, described sweetener is at least one in sucrose, xylitol, glucose, described acid is at least one in citric acid, malic acid, light-coloured vinegar, described adhesive is microcrystalline cellulose, and described lubricant is cornstarch.
9. the walnut pollen tablet stated according to Claim 8, is characterized in that: described sweetener is white granulated sugar, and described acid is citric acid, and described adhesive is microcrystalline cellulose, and described lubricant is cornstarch.
10. the preparation method of the walnut pollen tablet according to claim 5-9, is characterized in that, comprise the following steps: by described broken wall walnut pollen and described auxiliary materials and mixing, utilize rotary tablet press, obtains walnut pollen tablet.
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| CN104957456A (en) * | 2015-06-09 | 2015-10-07 | 西北大学 | Fagopyrum esculentum pollen composite instant particle and processing method thereof |
| CN106861865A (en) * | 2017-04-19 | 2017-06-20 | 长葛市怀瑞蜂产品有限公司 | A kind of means for breaking walls of pollen |
| CN106984414A (en) * | 2017-03-24 | 2017-07-28 | 甘肃省医学科学研究院 | The wall-breaking method of peony pollen |
| CN107397162A (en) * | 2017-05-19 | 2017-11-28 | 贾丽娜 | The edible exploitation of walnut male flower |
| CN109329698A (en) * | 2018-09-26 | 2019-02-15 | 浙江圣博康药业有限公司 | A kind of preparation method that anti-inflammation and sterilization preserved egg is scattered |
| CN115251224A (en) * | 2022-04-29 | 2022-11-01 | 南京中医药大学 | Preparation method of bee pollen protein |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104957456A (en) * | 2015-06-09 | 2015-10-07 | 西北大学 | Fagopyrum esculentum pollen composite instant particle and processing method thereof |
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| CN106861865A (en) * | 2017-04-19 | 2017-06-20 | 长葛市怀瑞蜂产品有限公司 | A kind of means for breaking walls of pollen |
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| CN109329698A (en) * | 2018-09-26 | 2019-02-15 | 浙江圣博康药业有限公司 | A kind of preparation method that anti-inflammation and sterilization preserved egg is scattered |
| CN115251224A (en) * | 2022-04-29 | 2022-11-01 | 南京中医药大学 | Preparation method of bee pollen protein |
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