CN104356710A - High-temperature-resistant and corrosion-resistant paint and preparation method thereof - Google Patents
High-temperature-resistant and corrosion-resistant paint and preparation method thereof Download PDFInfo
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- CN104356710A CN104356710A CN201410580272.3A CN201410580272A CN104356710A CN 104356710 A CN104356710 A CN 104356710A CN 201410580272 A CN201410580272 A CN 201410580272A CN 104356710 A CN104356710 A CN 104356710A
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Abstract
The invention discloses a high-temperature-resistant and corrosion-resistant paint and a preparation method thereof. The paint is formed by mixing organic silicon resin, epoxy resin E-12, benzoic acid, ethyl acetate, lemongrass extracting solution, mica powder, an antifoaming agent, a fire retardant, aluminium powder, polyacrylonitrile-based carbon fibers, a butyl cellosolve solvent, urea and trimethylolpropane triacrylate. The preparation method comprises the following steps: step 1: mixing the organic silicon resin, the epoxy resin E-12, the benzoic acid, the mica powder, the fire retardant, the aluminium powder, the polyacrylonitrile-based carbon fibers, the butyl cellosolve solvent and the urea, carrying out stirring, heating and heat preservation, carrying out heating and heat preservation again, and after natural cooling, obtaining a first mixture; step 2: adding the ethyl acetate, the lemongrass extracting solution and the trimethylolpropane triacrylate into the first mixture, heating, stirring, then adding the antifoaming agent and continuing stirring to obtain a semi-finished product; step 3: grinding the semi-finished product, regulating the PH and carrying out subpackaging to obtain the high-temperature-resistant and corrosion--resistant paint. The paint disclosed by the invention is high-temperature-resistant, corrosion-resistant, flat and bright.
Description
Technical field
The present invention relates to paint field, be specifically related to a kind of corrosion-and high-temp-resistant paint and preparation method thereof.
Background technology
Paint in daily life, is seen everywhere, and the Main Function that it plays is protection and modifies; and according to different environments for use, the kind of paint also has various, traditional paint ubiquity smell weight; easily come off; perishable, the problems such as inadequate environmental protection, can not meet the service requirements of human consumer to paint; therefore the formula improving original paint is needed; increase practicality and the weather resistance of paint, reduce its harm to environment and people, and various environment for use condition can be adapted to.
Summary of the invention
For the deficiencies in the prior art, the object of the present invention is to provide a kind of corrosion-and high-temp-resistant to paint and preparation method thereof, improve the wear life of paint, protect product.
For solving prior art problem, the technical scheme that the present invention takes is:
A corrosion-and high-temp-resistant paint, comprises the following raw material counted by weight: silicone resin 13-23 part, epoxy resin E-12 8-12 part, phenylformic acid 2-5 part, ethyl acetate 6-8 part, Herba Cymbopogonis Citrari extracting solution 5-10 part, mica powder 2-5 part, defoamer 0.2-0.6 part, fire retardant 0.3-0.6 part, aluminium powder 1-4 part, PAN-based carbon fiber 2-8 part, ethylene glycol butyl ether 5-10 part, urea 1-3 part, Viscoat 295 2-6 part.
As preferably, above-mentioned corrosion-and high-temp-resistant paint, comprises the following raw material counted by weight: silicone resin 18-20 part, epoxy resin E-12 9-11 part, phenylformic acid 3-5 part, ethyl acetate 6-8 part, Herba Cymbopogonis Citrari extracting solution 7-9 part, mica powder 3-5 part, defoamer 0.3-0.5 part, fire retardant 0.3-0.5 part, aluminium powder 2-4 part, PAN-based carbon fiber 6-8 part, ethylene glycol butyl ether 6-8 part, urea 1-3 part, Viscoat 295 3-5 part.
The preparation method of above-mentioned corrosion-and high-temp-resistant paint, comprises the following steps:
Step 1, by silicone resin, epoxy resin E-12, phenylformic acid, mica powder, fire retardant, aluminium powder, PAN-based carbon fiber, after ethylene glycol butyl ether and urea mix, stir 12-18 minute, after being incubated 10-15 minute at being heated to 150-220 DEG C, continue to be heated to 220-250 DEG C of insulation 5-10 minute, after naturally cooling, obtain mixture one;
Step 2, by ethyl acetate, Herba Cymbopogonis Citrari extracting solution and Viscoat 295 add in mixture one, heated and stirred 40-60 minute at 50-80 DEG C, then add defoamer, continue to stir 5-8 minute, obtain work in-process;
Step 3, after work in-process being ground to 200-400 order, after regulating PH to 6-8, packing obtains corrosion-and high-temp-resistant paint.
As preferably, in step 1, stirring velocity is 200-500rpm.
As preferably, after adding defoamer in step 2, stir with the speed of 100-150rpm.
As preferably, work in-process are ground to 300-400 order by step 3.
beneficial effect
The present invention's paint is by mixing corrosion-resistant and high-temperature resistant raw material, and discontinuity step heating, and make paint homogeneous, corrosion-and high-temp-resistant performance is good, and natural lemon more easily allows people accept, and is suitable as automotive lacquer or adds the material of home decoration.
Embodiment
embodiment 1
A corrosion-and high-temp-resistant paint, comprises the following raw material counted by weight: silicone resin 13 parts, epoxy resin E-12 8 parts, 2 parts, phenylformic acid, ethyl acetate 6 parts, Herba Cymbopogonis Citrari extracting solution 5 parts, mica powder 2 parts, defoamer 0.2 part, fire retardant 0.3 part, aluminium powder 1 part, PAN-based carbon fiber 2 parts, ethylene glycol butyl ether 5 parts, 1 part, urea, Viscoat 295 2 parts.
The preparation method of above-mentioned corrosion-and high-temp-resistant paint, comprises the following steps:
Step 1, by silicone resin, epoxy resin E-12, phenylformic acid, mica powder, fire retardant, aluminium powder, PAN-based carbon fiber, after ethylene glycol butyl ether and urea mix, stir 12 minutes with 200rpm, after being incubated 10 minutes at being heated to 150 DEG C, continue to be heated to 220 DEG C of insulations 5 minutes, after naturally cooling, obtain mixture one;
Step 2, by ethyl acetate, Herba Cymbopogonis Citrari extracting solution and Viscoat 295 add in mixture one, heated and stirred 40 minutes at 50 DEG C, then add defoamer, continue stirring 5 minutes, obtain work in-process with 100rpm;
Step 3, after work in-process being ground to 200 orders, after regulating PH to 6, packing obtains corrosion-and high-temp-resistant paint.
embodiment 2
A corrosion-and high-temp-resistant paint, comprises the following raw material counted by weight: silicone resin 20 parts, epoxy resin E-12 10 parts, 4 parts, phenylformic acid, ethyl acetate 7 parts, Herba Cymbopogonis Citrari extracting solution 8 parts, mica powder 3 parts, defoamer 0.4 part, fire retardant 0.5 part, aluminium powder 3 parts, PAN-based carbon fiber 6 parts, ethylene glycol butyl ether 8 parts, 2 parts, urea, Viscoat 295 4 parts.
The preparation method of above-mentioned corrosion-and high-temp-resistant paint, comprises the following steps:
Step 1, by silicone resin, epoxy resin E-12, phenylformic acid, mica powder, fire retardant, aluminium powder, PAN-based carbon fiber, after ethylene glycol butyl ether and urea mix, stir 16 minutes with 300rpm, after being incubated 13 minutes at being heated to 180 DEG C, continue to be heated to 240 DEG C of insulations 8 minutes, after naturally cooling, obtain mixture one;
Step 2, by ethyl acetate, Herba Cymbopogonis Citrari extracting solution and Viscoat 295 add in mixture one, heated and stirred 40-60 minute at 50-80 DEG C, then add defoamer, continue to stir 5-8 minute, obtain work in-process with 130rpm;
Step 3, after work in-process being ground to 300 orders, after regulating PH to 7, packing obtains corrosion-and high-temp-resistant paint.
embodiment 3
A corrosion-and high-temp-resistant paint, comprises the following raw material counted by weight: silicone resin 23 parts, epoxy resin E-12 12 parts, 5 parts, phenylformic acid, ethyl acetate 8 parts, Herba Cymbopogonis Citrari extracting solution 10 parts, mica powder 5 parts, defoamer 0.6 part, fire retardant 0.6 part, aluminium powder 4 parts, PAN-based carbon fiber 8 parts, ethylene glycol butyl ether 10 parts, 3 parts, urea, Viscoat 295 6 parts.
The preparation method of above-mentioned corrosion-and high-temp-resistant paint, comprises the following steps:
Step 1, by silicone resin, epoxy resin E-12, phenylformic acid, mica powder, fire retardant, aluminium powder, PAN-based carbon fiber, after ethylene glycol butyl ether and urea mix, stir 18 minutes with 500rpm, after being incubated 15 minutes at being heated to 220 DEG C, continue to be heated to 250 DEG C of insulations 10 minutes, after naturally cooling, obtain mixture one;
Step 2, by ethyl acetate, Herba Cymbopogonis Citrari extracting solution and Viscoat 295 add in mixture one, heated and stirred 60 minutes at 80 DEG C, then add defoamer, continue stirring 8 minutes, obtain work in-process with 150rpm;
Step 3, after work in-process being ground to 400 orders, after regulating PH to 8, packing obtains corrosion-and high-temp-resistant paint.
embodiment 4
A corrosion-and high-temp-resistant paint, comprises the following raw material counted by weight: silicone resin 23 parts, epoxy resin E-12 12 parts, 5 parts, phenylformic acid, ethyl acetate 8 parts, Herba Cymbopogonis Citrari extracting solution 10 parts, mica powder 5 parts, defoamer 0.6 part, fire retardant 0.6 part, aluminium powder 4 parts, PAN-based carbon fiber 8 parts, ethylene glycol butyl ether 10 parts, 3 parts, urea, Viscoat 295 6 parts.
The preparation method of above-mentioned corrosion-and high-temp-resistant paint, comprises the following steps:
Step 1, by silicone resin, epoxy resin E-12, phenylformic acid, mica powder, fire retardant, aluminium powder, PAN-based carbon fiber, after ethylene glycol butyl ether and urea mix, stir 18 minutes with 500rpm, after being incubated 15 minutes at being heated to 220 DEG C, continue to be heated to 250 DEG C of insulations 10 minutes, after naturally cooling, obtain mixture one;
Step 2, by ethyl acetate, Herba Cymbopogonis Citrari extracting solution and Viscoat 295 add in mixture one, heated and stirred 60 minutes at 80 DEG C, then add defoamer, continue stirring 8 minutes, obtain work in-process with 150rpm;
Step 3, after work in-process being ground to 400 orders, after regulating PH to 6, packing obtains corrosion-and high-temp-resistant paint.
performance test
Detected with existing paint by the present invention's paint, the data obtained is as shown in the table:
As can be known from the above table, the present invention paints high temperature resistant, good corrosion resistance, and natural lemon taste is popular.
Claims (6)
1. a corrosion-and high-temp-resistant paint, is characterized in that, comprise the following raw material counted by weight: silicone resin 13-23 part, epoxy resin E-12 8-12 part, phenylformic acid 2-5 part, ethyl acetate 6-8 part, Herba Cymbopogonis Citrari extracting solution 5-10 part, mica powder 2-5 part, defoamer 0.2-0.6 part, fire retardant 0.3-0.6 part, aluminium powder 1-4 part, PAN-based carbon fiber 2-8 part, ethylene glycol butyl ether 5-10 part, urea 1-3 part, Viscoat 295 2-6 part.
2. corrosion-and high-temp-resistant paint according to claim 1, is characterized in that, comprise the following raw material counted by weight: silicone resin 18-20 part, epoxy resin E-12 9-11 part, phenylformic acid 3-5 part, ethyl acetate 6-8 part, Herba Cymbopogonis Citrari extracting solution 7-9 part, mica powder 3-5 part, defoamer 0.3-0.5 part, fire retardant 0.3-0.5 part, aluminium powder 2-4 part, PAN-based carbon fiber 6-8 part, ethylene glycol butyl ether 6-8 part, urea 1-3 part, Viscoat 295 3-5 part.
3. the preparation method of corrosion-and high-temp-resistant paint according to claim 1, is characterized in that, comprise the following steps:
Step 1, by silicone resin, epoxy resin E-12, phenylformic acid, mica powder, fire retardant, aluminium powder, PAN-based carbon fiber, after ethylene glycol butyl ether and urea mix, stir 12-18 minute, after being incubated 10-15 minute at being heated to 150-220 DEG C, continue to be heated to 220-250 DEG C of insulation 5-10 minute, after naturally cooling, obtain mixture one;
Step 2, by ethyl acetate, Herba Cymbopogonis Citrari extracting solution and Viscoat 295 add in mixture one, heated and stirred 40-60 minute at 50-80 DEG C, then add defoamer, continue to stir 5-8 minute, obtain work in-process;
Step 3, after work in-process being ground to 200-400 order, after regulating PH to 6-8, packing obtains corrosion-and high-temp-resistant paint.
4. the preparation method of corrosion-and high-temp-resistant paint according to claim 3, is characterized in that: in step 1, stirring velocity is 200-500rpm.
5. the preparation method of corrosion-and high-temp-resistant paint according to claim 3, is characterized in that: after adding defoamer in step 2, stirs with the speed of 100-150rpm.
6. the preparation method of corrosion-and high-temp-resistant paint according to claim 3, is characterized in that: step 3, work in-process is ground to 300-400 order.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410580272.3A CN104356710A (en) | 2014-10-27 | 2014-10-27 | High-temperature-resistant and corrosion-resistant paint and preparation method thereof |
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| CN201410580272.3A CN104356710A (en) | 2014-10-27 | 2014-10-27 | High-temperature-resistant and corrosion-resistant paint and preparation method thereof |
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| CN104356710A true CN104356710A (en) | 2015-02-18 |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104877406A (en) * | 2015-05-20 | 2015-09-02 | 苏州市贝克生物科技有限公司 | High-temperature-resistant transparent anticorrosive paint and preparation method thereof |
| CN104877407A (en) * | 2015-05-20 | 2015-09-02 | 苏州市贝克生物科技有限公司 | Anti-radiation wear-proof paint and preparation method thereof |
| CN105038484A (en) * | 2015-08-05 | 2015-11-11 | 南通新昱化工有限公司 | Icing-preventing and impact-resisting coating |
| CN105149567A (en) * | 2015-08-28 | 2015-12-16 | 苏州莱特复合材料有限公司 | Preparing method for powder metallurgy preservatives |
| CN106047084A (en) * | 2016-08-14 | 2016-10-26 | 安庆市沁之源电器有限公司 | Electric fan anti-scraping coating and preparation method thereof |
| CN106995638A (en) * | 2017-06-17 | 2017-08-01 | 合肥市晨雷思建筑材料科技有限公司 | A kind of Wood floor oil paint and preparation method thereof |
| CN107641417A (en) * | 2017-08-02 | 2018-01-30 | 江苏丰海新能源淡化海水发展有限公司 | A kind of Marine Paints of corrosion-and high-temp-resistant and preparation method thereof |
| CN110835752A (en) * | 2018-08-19 | 2020-02-25 | 天长市京发铝业有限公司 | Method for improving high-temperature oxidation resistance of aluminum alloy |
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| CN102051117A (en) * | 2009-11-03 | 2011-05-11 | 孙向勇 | High temperature resistant anticorrosive paint and preparation method thereof |
| CN102464939A (en) * | 2010-11-18 | 2012-05-23 | 贵州航天风华精密设备有限公司 | High-temperature-resistant heat-proof paint and preparation and use methods thereof |
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| CN102051117A (en) * | 2009-11-03 | 2011-05-11 | 孙向勇 | High temperature resistant anticorrosive paint and preparation method thereof |
| CN102464939A (en) * | 2010-11-18 | 2012-05-23 | 贵州航天风华精密设备有限公司 | High-temperature-resistant heat-proof paint and preparation and use methods thereof |
| CN103484014A (en) * | 2013-06-26 | 2014-01-01 | 南京市荣达树脂有限公司 | Preparation method of organic silicon high-temperature resistant resin coating |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104877406A (en) * | 2015-05-20 | 2015-09-02 | 苏州市贝克生物科技有限公司 | High-temperature-resistant transparent anticorrosive paint and preparation method thereof |
| CN104877407A (en) * | 2015-05-20 | 2015-09-02 | 苏州市贝克生物科技有限公司 | Anti-radiation wear-proof paint and preparation method thereof |
| CN105038484A (en) * | 2015-08-05 | 2015-11-11 | 南通新昱化工有限公司 | Icing-preventing and impact-resisting coating |
| CN105149567A (en) * | 2015-08-28 | 2015-12-16 | 苏州莱特复合材料有限公司 | Preparing method for powder metallurgy preservatives |
| CN106047084A (en) * | 2016-08-14 | 2016-10-26 | 安庆市沁之源电器有限公司 | Electric fan anti-scraping coating and preparation method thereof |
| CN106995638A (en) * | 2017-06-17 | 2017-08-01 | 合肥市晨雷思建筑材料科技有限公司 | A kind of Wood floor oil paint and preparation method thereof |
| CN107641417A (en) * | 2017-08-02 | 2018-01-30 | 江苏丰海新能源淡化海水发展有限公司 | A kind of Marine Paints of corrosion-and high-temp-resistant and preparation method thereof |
| CN110835752A (en) * | 2018-08-19 | 2020-02-25 | 天长市京发铝业有限公司 | Method for improving high-temperature oxidation resistance of aluminum alloy |
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Application publication date: 20150218 |