CN104321047A - Powdery solid composition for hair, powdery solid cosmetic for hair, method for manufacturing powdery solid cosmetic for hair, method for hairdressing using powdery solid cosmetic for hair - Google Patents
Powdery solid composition for hair, powdery solid cosmetic for hair, method for manufacturing powdery solid cosmetic for hair, method for hairdressing using powdery solid cosmetic for hair Download PDFInfo
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- CN104321047A CN104321047A CN201380025975.3A CN201380025975A CN104321047A CN 104321047 A CN104321047 A CN 104321047A CN 201380025975 A CN201380025975 A CN 201380025975A CN 104321047 A CN104321047 A CN 104321047A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/022—Powders; Compacted Powders
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/022—Powders; Compacted Powders
- A61K8/0225—Granulated powders
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/60—Particulates further characterized by their structure or composition
- A61K2800/65—Characterized by the composition of the particulate/core
- A61K2800/651—The particulate/core comprising inorganic material
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Abstract
The present invention provides a powdery solid cosmetic for hair of an entirely unprecedented, novel form which makes it possible to perform hairdressing easily, does not feel sticky, enables hairdressing to a desired hairstyle, and makes it possible to impart a natural texture. The powdery solid composition for hair pertaining to the present invention is a powdery solid, is used for hair, and contains: a first powder, which is at least one type of silicic acid anhydride and hydrophobized silicic acid anhydride; an oil, which is at least one type of fatty acid ester oil and silicone oil; and a second powder, which is a powder other than the first powder.
Description
Technical field
The present invention relates to Hair grooming powder solid shape compositions, possess the Hair grooming powder solid shape cosmetics of said composition and container, the manufacture method of these cosmetics and use the method for haircuting of these cosmetics.
Background technology
As the cosmetics for haircuting, there is overlay film formative resin compounding as the liquid state of function of tonic chord composition of haircuting, gel, blister or vaporific Hair grooming cosmetics (such as with reference to patent documentation 1 ~ 4).In addition, the compounding oil preparation such as wax class or hydrocarbon ils is also had as the paste of function of tonic chord composition of haircuting or wax-like Hair grooming cosmetics (for example, see patent documentation 5 ~ 6).Now, compounding have the Hair grooming cosmetics of overlay film formative resin or oil preparation just to become main flow.
But for the compounding Hair grooming cosmetics of existing overlay film formative resin or oil preparation, it can give full play to excellent function of haircuting, but also there is the problem producing sticky feeling, the problem being difficult to give natural visual impression on the contrary.Up to now, various trial has also been carried out in order to solve the above problems.
On the other hand, about the method for haircuting of use Hair grooming cosmetics, have various method of haircuting for often kind of dosage form, what generally attempt is the method using comb to implement to haircut, the method etc. of haircuting with palm or finger enforcement.
But, when using Hair grooming cosmetics, using comb to implement in the method for haircuting, although can haircut to hair entirety easily, there is the problem can not fully implementing to haircut to thin portion.In addition, when using Hair grooming cosmetics, replace comb and implement in the method for haircuting with palm or finger, although can fully implement to haircut to thin portion, if but smear cosmetics too much, sticky feeling and heavy topknot sense can be produced, thus there is the problem can not implementing easily to haircut.
So, be difficult to fully implement easily to haircut to thin portion in existing Hair grooming cosmetics.Particularly go out etc., fully to haircut easily to thin portion just more difficult, can not re-start easily and haircut.In view of such Hair grooming cosmetics and present situation thereof, expect to develop a kind of Hair grooming cosmetics, it is new-type dosage form and can implements easily to haircut.
Prior art document
Patent documentation
Patent documentation 1: Japanese Unexamined Patent Publication 9-301838 publication
Patent documentation 2: Japanese Unexamined Patent Publication 2001-335425 publication
Patent documentation 3: Japanese Unexamined Patent Publication 2000-204025 publication
Patent documentation 4: Japanese Unexamined Patent Publication 2011-251918 publication
Patent documentation 5: Japanese Unexamined Patent Publication 2009-173602 publication
Patent documentation 6: Japanese Unexamined Patent Publication 2002-114652 publication
Summary of the invention
The problem that invention will solve
Problem of the present invention is the Hair grooming powder solid shape cosmetics providing a kind of new-type dosage form, and it can impose easily and haircut, and can have no sticky feeling and haircut into desired hair style, can give natural visual impression.In addition, the invention provides the manufacture method of the Hair grooming powder solid shape cosmetics with above-mentioned Hair grooming powder solid shape cosmetics and container and Hair grooming powder solid shape cosmetics and use the method for haircuting of above-mentioned Hair grooming powder solid shape cosmetics.
For solving the scheme of problem
The present inventor continues to conduct in-depth research to develop the Hair grooming cosmetics of new-type dosage form, found that, when specific powder constituents is directly applied for hair, surprisingly, can have no sticky feeling and haircut into desired hair style, natural visual impression (natural completion status) can be given.
And then, the present inventor finds, the following problems that existing Hair grooming cosmetics have can be solved: when (1) uses comb to haircut by being made as the Hair grooming cosmetics of the powder solid shape of new-type dosage form, although can haircut to hair entirety, can not fully haircut to the problem in thin portion; (2), when haircuting with palm, finger, if smear too much, sticky feeling and heavy topknot sense can be produced, the problem thus can not haircuted easily; (3) go out etc. the problem that can not again haircut easily; Thus complete the present invention.
In order to solve above-mentioned problem, the invention provides a kind of Hair grooming powder solid shape compositions, it is powder solid shape, for hair, and containing the 1st powder body, oil preparation and the 2nd powder body, described 1st powder body is at least one in silicic acid anhydride and hydrophobization silicic acid anhydride, and described oil preparation is at least one in fatty acid ester oil and silicone oil, and described 2nd powder body is the powder body beyond above-mentioned 1st powder body.
In Hair grooming powder solid shape compositions of the present invention, preferably the oil absorption of above-mentioned 1st powder body meets 100mL/100g ~ 1000mL/100g.
In Hair grooming powder solid shape compositions of the present invention, preferably the bulk density of above-mentioned 1st powder body meets 80g/L ~ 300g/L.
In Hair grooming powder solid shape compositions of the present invention, preferably above-mentioned 2nd powder body is be selected from least one by Talcum, Muscovitum, Kaolin, sericite and barium sulfate.
In Hair grooming powder solid shape compositions of the present invention, preferably the content of above-mentioned 1st powder body is 5 quality % ~ 50 quality %, and the content of above-mentioned oil preparation is 5 quality % ~ 40 quality %, and the content of above-mentioned 2nd powder body is 30 quality % ~ 80 quality %.
The powder solid shape that Hair grooming powder solid shape compositions of the present invention obtains preferably by compression forming, it obtains by carrying out compression forming to the mix and blend thing of above-mentioned 1st powder body of mix and blend, above-mentioned oil preparation and above-mentioned 2nd powder body.
Hair grooming powder solid shape cosmetics of the present invention possess above-mentioned Hair grooming powder solid shape compositions and preserve the container of above-mentioned Hair grooming powder solid shape compositions.
The manufacture method of Hair grooming powder solid shape cosmetics of the present invention possesses: by above-mentioned 1st powder body, above-mentioned oil preparation and above-mentioned 2nd powder body mix and blend, obtain the operation of mix and blend thing; 2nd operation, is directly filled in said vesse by above-mentioned mix and blend thing or is filled in the inner vessel therein be arranged in said vesse; With the 3rd operation, after filling by the compression forming of above-mentioned mix and blend thing or after filling compression forming is not carried out to above-mentioned mix and blend thing but utilize the forming method different from compression forming carry out molding.
In the manufacture method of Hair grooming powder solid shape cosmetics of the present invention, by the 3rd operation of above-mentioned mix and blend thing compression forming after above-mentioned 3rd operation is preferably and fills.
The method of haircuting of Hair grooming powder solid shape cosmetics of the present invention is used to possess: the 1st operation, utilize above-mentioned Hair grooming powder solid shape cosmetics, with finger tip or use applicator, wipe from the surface of above-mentioned Hair grooming powder solid shape compositions and get above-mentioned Hair grooming powder solid shape compositions; 2nd operation, with finger tip or use applicator, is applied on hair by wiping the above-mentioned Hair grooming powder solid shape compositions taken off; With the 3rd operation, use finger tip or palm, the above-mentioned Hair grooming powder solid shape compositions be applied on hair is rubbed on hair, implement thus to haircut.
The effect of invention
The character of Hair grooming powder solid shape compositions of the present invention is powder solid shape, the above-mentioned composition of taking in required minimum of implementing to haircut can be wiped from the surface of above-mentioned composition, and powder constituents does not disperse, above-mentioned composition can be smeared in the mode invested thinly on hair, therefore can produce following effect: can have no sticky feeling and haircut into desired hair style, natural visual impression can be given.
In addition, the Hair grooming powder solid shape cosmetics of the present invention that above-mentioned composition is saved in a reservoir also can produce following effect: also there is no need when haircuting to use comb, can implement easily to haircut.And then, because simplicity is excellent, even if therefore also can easily again haircut waiting with going out.
In addition, utilize the manufacture method of Hair grooming powder solid shape cosmetics of the present invention, the Hair grooming cosmetics of the powder solid shape of the new-type dosage form do not had completely in prior art can be provided as.In addition, the method for haircuting of Hair grooming powder solid shape cosmetics of the present invention is used can to produce following effect: can both implement easily to haircut to thin portion for from hair entirety.
Detailed description of the invention
Hair grooming powder solid shape compositions of the present invention is powder solid shape, for hair.Hair grooming powder solid shape compositions of the present invention is applied on hair.Hair grooming powder solid shape compositions of the present invention contains: the 1st powder body (being hereinafter sometimes designated as (A) composition) that (A) is at least one in silicic acid anhydride and hydrophobization silicic acid anhydride; (B) be the oil preparation (being hereinafter sometimes designated as (B) composition) of at least one in fatty acid ester oil and silicone oil; (C) be the 2nd powder body (being hereinafter sometimes designated as (C) composition) of the powder body beyond above-mentioned 1st powder body ((A) composition).Above-mentioned (A) composition and above-mentioned (C) composition are powder constituents separately.Above-mentioned (B) composition is oil preparation composition.
The character of Hair grooming powder solid shape compositions of the present invention is powder solid shape.Therefore, it is possible to suppress dispersing of each powder (powder constituents)." powder solid shape " is the character of each powder (granule) integration, is different from the character that powder body exists separately.The powder solid shape that Hair grooming powder solid shape compositions of the present invention obtains preferably by compression forming, obtains preferably by carrying out compression forming to the mix and blend thing of above-mentioned 1st powder body of mix and blend, above-mentioned oil preparation and above-mentioned 2nd powder body.Hair grooming powder solid shape compositions of the present invention is preferably the molded body of powder solid shape.
The above-mentioned silicic acid anhydride of above-mentioned (A) composition used and above-mentioned hydrophobization silicic acid anhydride are the composition of haircuting as having no sticky feeling and then can haircut again and the powder body be compounded in above-mentioned composition.Above-mentioned hydrophobization silicic acid anhydride in the present invention refers to the powder body surface of silicic acid anhydride being implemented to hydrophobization process.Above-mentioned hydrophobization silicic acid anhydride is such as the powder body utilizing the surface of following inorganic agent to silicic acid anhydride to implement hydrophobization process.
As the concrete inorganic agent for hydrophobization process, such as methyl trichlorosilane can be enumerated, dimethyldichlorosilane, trim,ethylchlorosilane, hexamethyldisiloxane, methyl trialkoxysilane, dimethyldialkylammonium oxygen base, trimethylalkyoxys iotalane, ethyl trichlorosilane, propyltrichlorosilan, hexyl trichlorosilane, chain alkyl trichlorosilane, ethyltrialkoxysilanes, propyl trialkoxy silane, hexyl trialkoxy silane, chain alkyl trialkoxy silane, methacryl silanes, fluoroalkyl silanes, the Organosilyl compounds such as perfluoroalkyl silanes, the silicone compounds etc. such as dimethyl polysiloxane (silicone oil), methyl phenyl silicone, methylhydrogenpolysi,oxane, amino modified silicone.Process for hydrophobicizing is not particularly limited, known method can be used to implement hydrophobization process.As process for hydrophobicizing, liquid phase method, vapor phase method, autoclave method etc. can be illustrated.
As concrete above-mentioned hydrophobization silicic acid anhydride, dimethyl silane oxygen base SiClx anhydride, trimethylsiloxy SiClx anhydride, octyl group siloxy SiClx anhydride, silicone oil process silicic acid anhydride, methacrylic acid monosilane oxygen base SiClx anhydride etc. can be illustrated.
As above-mentioned silicic acid anhydride and the above-mentioned hydrophobization silicic acid anhydride of above-mentioned (A) composition, also directly commercially available product can be used.As the commercially available product of above-mentioned silicic acid anhydride, such as AEROSIL 50, AEROSIL 90G, AEROSIL 130, AEROSIL 150, AEROSIL 200, AEROSIL 300, AEROSIL 380, AEROSIL 200V, AEROSIL 300V, AEROSIL 380V, AEROSIL OX50 (trade name is NIPPON AEROSIL society and manufactures) can be enumerated; SUNSPHERE H-31, SUNSPHERE H-51, SUNSPHERE H-121, SUNSPHERE H-201, SUNSPHERE H-32, SUNSPHERE H-52, SUNSPHERE H-122, SUNSPHERE H-33, SUNSPHERE H-53 (trade name is AGC SI-TECH society and manufactures); HDK-N20, HDK-T30 (trade name, is wacker asahikasei silicone co., and ltd. manufactures); Sylysia 310P, Sylysia 320, Sylysia 350, Sylysia 370, Sylysia 380, Sylysia 420, Sylysia 430, Sylysia 440, Sylysia 450, Sylysia 470 (trade name, be Fuji Silysia Chemical society manufacture) etc.
In addition, as the commercially available product of above-mentioned hydrophobization silicic acid anhydride, such as AEROSIL R972, AEROSIL R974, AEROSIL R9200 (trade name, dimethyl silane oxygen base SiClx anhydride are NIPPON AEROSIL society and manufacture) can be enumerated; HDK H15, HDK H18, HDK H2O, HDK H30 (trade name, dimethyl silane oxygen base SiClx anhydride, is wacker asahikasei silicone co., and ltd. manufactures); AEROSIL RX200, AEROSIL R8200, AEROSIL RX300, AEROSIL R812, AEROSIL R812S (trade name, trimethylsiloxy SiClx anhydride are NIPPON AEROSIL society and manufacture); VM-2270Aerogel Fine particles (TorayDow Corning society manufactures for trade name, trimethylsiloxy SiClx anhydride); HDK H2000 (wacker asahikasei silicone co., ltd. manufacture for trade name, trimethylsiloxy SiClx anhydride); AEROSIL R805 (NIPPON AEROSIL society manufactures for trade name, octyl group siloxy SiClx anhydride); AEROSIL R202, AEROSIL RY200, AEROSIL RY200S, AEROSIL RY300 (trade name, silicone oil process silicic acid anhydride are NIPPON AEROSIL society and manufacture); SUNSPHERE H-51-ET, SUNSPHERE H-52-ET, SUNSPHERE H-121-ET (trade name, silicone oil process silicic acid anhydride are AGC SI-TECH society and manufacture); AEROSIL R711, AEROSIL R7200 (trade name, methacrylic acid monosilane oxygen base SiClx anhydride are NIPPON AEROSIL society and manufacture) etc.
Above-mentioned silicic acid anhydride and the above-mentioned hydrophobization silicic acid anhydride of above-mentioned (A) composition can be used alone one, also two or more proper combination can be used.In the present invention, from the aspect giving full play to the power of haircuting and the aspect consideration that can also haircut again, as above-mentioned (A) composition, preferably use the composition meeting aftermentioned oil absorption (mL/100g).
As oil absorption more specifically, the oil absorption of the above-mentioned silicic acid anhydride of every 100g or above-mentioned hydrophobization silicic acid anhydride (above-mentioned (A) composition contained by above-mentioned composition) is preferably more than 100mL/100g, is more preferably more than 150mL/100g, more preferably more than 200mL/100g, is preferably below 1000mL/100g, is more preferably below 800mL/100g, more preferably below 700mL/100g.The scope ranging preferably from 100 ~ 1000mL/100g of the oil absorption of the above-mentioned silicic acid anhydride of every 100g or above-mentioned hydrophobization silicic acid anhydride, be more preferably the scope of scope, the more preferably 200 ~ 700mL/100g of 150 ~ 800mL/100g.It should be noted that, oil absorption (mL/100g) is the value measured according to the method recorded in JISK5101.
As the commercially available product of above-mentioned (A) composition of the scope of satisfied suitable oil absorption, can enumerate such as AEROSIL 200, AEROSIL 300, AEROSIL 380, AEROSIL 200V, AEROSIL 300V, AEROSIL 380V (trade name, silicic acid anhydride, be NIPPON AEROSIL society manufacture); SUNSPHERE H-32, SUNSPHERE H-52, SUNSPHERE H-122, SUNSPHERE H-33, SUNSPHERE H-53 (trade name is AGC SI-TECH society and manufactures); HDK-N20, HDK-T30 (trade name, silicic acid anhydride, is wacker asahikasei silicone co., and ltd. manufactures); Sylysia 310P, Sylysia 320, Sylysia 350, Sylysia 370, Sylysia 380, Sylysia 420, Sylysia 430, Sylysia 440, Sylysia 450, Sylysia 470 (trade name, silicic acid anhydride, be Fuji Silysia Chemical society manufacture), AEROSIL R972, AEROSIL R974, AEROSIL R9200 (trade name, dimethyl silane oxygen base SiClx anhydride, is NIPPON AEROSIL society and manufactures); HDK H15, HDK H18, HDK H2O, HDK H30 (trade name, dimethyl silane oxygen base SiClx anhydride, is wacker asahikasei silicone co., and ltd. manufactures); AEROSIL RX200, AEROSIL R8200, AEROSIL RX300, AEROSIL R812, AEROSIL R812S (trade name, trimethylsiloxy SiClx anhydride are NIPPON AEROSIL society and manufacture); VM-2270Aerogel Fine particles (TorayDow Corning society manufactures for trade name, trimethylsiloxy SiClx anhydride); HDK H2O00 (wacker asahikasei silicone co., ltd. manufacture for trade name, trimethylsiloxy SiClx anhydride); AEROSIL R805 (NIPPON AEROSIL society manufactures for trade name, octyl group siloxy SiClx anhydride); AEROSIL R202, AEROSIL RY200, AEROSIL RY200S, AEROSIL RY300 (trade name, silicone oil process silicic acid anhydride are NIPPON AEROSIL society and manufacture); SUNSPHERE H-51-ET, SUNSPHERE H-52-ET, SUNSPHERE H-121-ET (trade name, silicone oil process silicic acid anhydride are AGC SI-TECH society and manufacture); AEROSIL R711, AEROSIL R7200 (trade name, methacrylic acid monosilane oxygen base SiClx anhydride are NIPPON AEROSIL society and manufacture) etc.
In addition, in the present invention, do not disperse from the viewpoint of powder constituents, can wipe take in required minimum of implementing to haircut from the surface of powder solid shape, as above-mentioned (A) composition, preferably use meets the composition of aftermentioned bulk density (g/L).
As bulk density more specifically, be preferably more than 80g/L, be more preferably more than 90g/L, be preferably below 300g/L, be more preferably below 250g/L, more preferably below 200g/L.More specifically bulk density the scope ranging preferably from 80 ~ 300g/L, be more preferably the scope of scope, the more preferably 90 ~ 200g/L of 80 ~ 250g/L.It should be noted that, bulk density (g/L) is with within 30 seconds, to be filled in graduated cylinder and to leave standstill the value making for 5 minutes to measure the volume of above-mentioned (A) composition during its stabilisation with this state by above-mentioned (A) composition of constant weight.
As the commercially available product of above-mentioned (A) composition of the scope of satisfied suitable bulk density, such as AEROSIL 200V, AEROSIL 300V, AEROSIL 380V (trade name can be enumerated, silicic acid anhydride, be NIPPON AEROSIL society and manufacture), SUNSPHERE H-32, SUNSPHERE H-52, SUNSPHERE H-122, SUNSPHERE H-33, SUNSPHERE H-53 (trade name, be AGC SI-TECH society manufacture); Sylysia 310P, Sylysia 320, Sylysia 350, Sylysia 370, Sylysia 380, Sylysia 420, Sylysia 430, Sylysia 440, Sylysia 450, Sylysia 470 (trade name, silicic acid anhydride, be Fuji Silysia Chemical society manufacture), AEROSIL R9200 (trade name, dimethyl silane oxygen base SiClx anhydride, NIPPON AEROSIL society manufactures); AEROSIL R8200 (NIPPON AEROSIL society manufactures for trade name, trimethylsiloxy SiClx anhydride); SUNSPHERE H-51-ET, SUNSPHERE H-52-ET, SUNSPHERE H-121-ET (trade name, silicone oil process silicic acid anhydride are AGC SI-TECH society and manufacture); AEROSIL R7200 (NIPPON AEROSIL society manufactures for trade name, methacrylic acid monosilane oxygen base SiClx anhydride) etc.
In the present invention, from the viewpoint of playing effect of the present invention to greatest extent, as above-mentioned (A) composition, most preferably use the composition meeting the scope of above-mentioned oil absorption and both scopes of bulk density.As the commercially available product of most preferred above-mentioned (A) composition, such as AEROSIL 200V, AEROSIL 300V, AEROSIL 380V (trade name can be enumerated, silicic acid anhydride, be NIPPON AEROSIL society manufacture), AEROSIL R9200 (trade name, dimethyl silane oxygen base SiClx anhydride, NIPPON AEROSIL society manufactures); AEROSIL R8200 (trade name, trimethylsiloxy SiClx anhydride, NIPPON AEROSIL society manufacture), AEROSIL R7200 (trade name, methacrylic acid monosilane oxygen base SiClx anhydride, NIPPON AEROSIL society manufacture) etc.
The content of above-mentioned (A) composition is not particularly limited, suitable adjustment can be carried out to it so that the effect desired by fully giving.Usually, carry out from the viewpoint of having no sticky feeling further haircuting, can also haircut again, in above-mentioned composition 100 quality %, the content of above-mentioned (A) composition is preferably more than 5 quality %, is more preferably more than 10 quality %, more preferably more than 15 quality %, is preferably below 50 quality %, is more preferably below 40 quality %; In above-mentioned composition 100 quality %, be preferably 5 quality % ~ 50 quality %, be more preferably 10 quality % ~ 40 quality %, more preferably 15 quality % ~ 40 quality %.The content of above-mentioned (A) composition can be less than 5 quality %, but when the content of above-mentioned (A) composition is less than 5 quality %, has the tendency that haircuting property reduces.
Above-mentioned fatty acid ester oil and the above-mentioned silicone oil of above-mentioned (B) composition used are the compositions be compounded into as the composition making powder solid shape in above-mentioned composition.
As concrete above-mentioned fatty acid ester oil used, such as ethyl oleate can be enumerated, isopropyl myristate, isopropyl palmitate, butyl stearate, tetradecylic acid myristin, tetradecylic acid cetyl ester, cetyl palmitate, stearyl stearate, decyl oleate, oleyl oleate, tetradecylic acid octyldodecyl, octyldodecyl oleate, isostearic acid ethyl ester, isocetyl stearate base ester, IPIS, isostearic acid isocetyl ester, 2 ethyl hexanoic acid cetyl ester, 2 ethyl hexanoic acid cetearyl alcohol ester, two capric acid DOPCP, neopentyl glycol two (thylhexoic acid) ester, plant sterol/octyl dodecanol lauroyl glutamate ester, glyceryl isostearate, three 2 ethyl hexanoic acid glyceride, tricaprylin, three different tripalmitins, three glyceryl isostearates, three 2 ethyl hexanoic acid trihydroxymethylpropanyl esters, three isostearic acid trihydroxymethylpropanyl esters, four 2 ethyl hexanoic acid pentaerythritol esters, Cetyl octanoate, sad isocetyl ester, sad different stearyl ester, the different stearyl ester of decanedioic acid, isostearic acid octyldodecyl, dimethyl-octa acid octyldodecyl, Tetradecyl lactate, lactic acid cetyl ester, the different stearyl ester of malic acid two, oleic acid sorbitan etc.
As concrete above-mentioned silicone oil used, such as methyl polysiloxane can be enumerated, average degree of polymerization be 650 ~ 7000 height gather the chain silicone such as methyl polysiloxane, octamethyltrisiloxane, decamethyl tetrasiloxane, methyl phenyl silicone, methylhydrogenpolysi,oxane, dimethiconol; The cyclic silicone such as octamethylpolysiloxane, octamethylcy-clotetrasiloxane, decamethylcyclopentaandoxane, ten diformazan basic ring six siloxanes; The amino modified silicone such as aminopropylmethylsiloxane dimethylsiloxane copolymer, aminoethylaminopropyl siloxanes dimethylsiloxane copolymer, aminoethylaminopropyl methylsiloxane dimethylsiloxane copolymer; Carboxy-modified silicone, fatty acid modified silicone, alcohol modified silicone, aliphatic alcohol modified silicone, epoxide modified silicone, fluorine richness silicone, alkyl-modified silicone etc.
Above-mentioned (B) composition can be used alone one, also two or more proper combination can be used.In the present invention, haircut into desired hair style from the viewpoint of having no sticky feeling further, more natural visual impression can be given, preferably share above-mentioned fatty acid ester oil and above-mentioned silicone oil.Above-mentioned (B) composition (above-mentioned oil preparation) preferably comprises above-mentioned fatty acid ester oil and above-mentioned silicone oil.
The content of above-mentioned (B) composition is not particularly limited, suitable adjustment can be carried out to it so that the effect desired by fully giving.Usually, haircut into desired hair style from the viewpoint of having no sticky feeling further, more natural visual impression can be given, in above-mentioned composition 100 quality %, the content of above-mentioned (B) composition is preferably more than 5 quality %, is more preferably more than 8 quality %, is preferably below 40 quality %, is more preferably below 30 quality %, more preferably below 25 quality %; In above-mentioned composition 100 quality %, be preferably 5 quality % ~ 40 quality %, be more preferably 5 quality % ~ 30 quality %, more preferably 8 quality % ~ 25 quality %.
Above-mentioned (C) used is as long as composition is the powder body beyond above-mentioned (A) composition.Powder body as above-mentioned (C) composition is the powder body different with hydrophobization silicic acid anhydride from silicic acid anhydride.As above-mentioned (C) composition, the inorganic particle beyond such as above-mentioned (A) composition and organic powder can be enumerated.In addition, as the shape of above-mentioned (C) composition used, such as spherical, tabular, needle-like, amorphous etc. can be enumerated.The shape of above-mentioned powder body can be arbitrary shape, is not particularly limited.
As concrete above-mentioned inorganic particle, as long as be beyond above-mentioned (A) composition, such as calcium silicates can be enumerated, magnesium silicate, aluminium silicate, synthetic aluminium silicate, natural aluminium silicate, Magnesiumaluminumsilicate, Talcum, Muscovitum, Kaolin, mica titanium, sericite, bentonite, calcium carbonate, magnesium carbonate, calcium sulfate, barium sulfate, magnesium sulfate, zinc oxide, titanium dioxide, aluminium oxide, zirconium oxide, magnesium oxide, ferrum oxide, iron oxide yellow, Black Rouge, iron oxide-titania sinter, iron oxide red is coated to Muscovitum, iron oxide red is coated to mica titanium, titanium dioxide is coated to silicic acid anhydride, chromium oxide, stannum oxide, aluminium oxide, Bismuth Oxychloride, ultramarine, Prussian blue, smithsonite, borosilicic acid, white carbon black, cobalt titanate, soft calcium, soft magnesium, heavy calcium, heavy magnesium, aluminum end, boron nitride, hydroxyapatite, borosilicic acid (Ca/Na), zeolite etc.
In addition, in the present invention, as above-mentioned (C) composition, also can use and utilize silicic acid anhydride that the surface-coated silicic acid anhydride of the powder body such as Talcum, Muscovitum, Kaolin, titanium dioxide, aluminium oxide, zinc oxide, cerium oxide is coated to powder body etc.
As concrete above-mentioned organic powder, the nylon powders such as such as nylon 6, nylon 12, nylon66 fiber can be enumerated; The polyolefin powder such as polyethylene, polypropylene; The polyacrylate powder such as polymethyl methacrylate; The silicone resin powder such as polymethylsilsesquioxane, dimethylpolysiloxanepolymer polymer; The fluororesin powders such as politef; Polystyrene powder, polyurethane powder, poly-epoxy powder, polyethylene terephthalate, PTT, Merlon, celluloid, cellulose, crystalline cellulose, acetylcellulose, chitin, chitosan, polysaccharide, protein powder, lauroyl lysine, vinylite, carbamide resin, (PET/ polyolefin) laminate, (PET/Al/ epoxy resin) laminate etc.
Above-mentioned (C) composition can be used alone one, also two or more proper combination can be used.In the present invention, haircut into desired hair style from the viewpoint of having no sticky feeling further, more natural visual impression can be given, as above-mentioned (C) composition, preferably use Talcum, Muscovitum, Kaolin, sericite and barium sulfate.
The content of above-mentioned (C) composition is not particularly limited, suitable adjustment can be carried out to it so that the effect desired by fully giving.Usually, from the viewpoint of making better powder solid shape, in above-mentioned composition 100 quality %, the content of above-mentioned (C) composition is preferably more than 30 quality %, is more preferably more than 35 quality %, more preferably more than 40 quality %, is preferably below 80 quality %, is more preferably below 75 quality %, more preferably below 70 quality %; In above-mentioned composition 100 quality %, be preferably 30 quality % ~ 80 quality %, be more preferably 35 quality % ~ 75 quality %, more preferably 40 quality % ~ 70 quality %.
Except mentioned component, in the scope not damaging effect of the present invention, composition that can be used in the usual cosmetics of mixture in Hair grooming powder solid shape compositions of the present invention.Such as, the oil preparation beyond above-mentioned (B) compositions such as any mixture oils and fats, wax class, hydrocarbon ils, higher fatty acids, higher alcohol can be suitable for according to object; Anionic property overlay film forms polymer, cationic overlay film forms polymer, both sexes overlay film forms polymer, nonionic overlay film forms the overlay films such as polymer and forms polymer; The surfactants such as non-ionic surface active agent, anion surfactant, cationic surfactant, amphoteric surfactant; Polyhydric alcohol, tackifying macromolecule, wetting agent, antioxidant, UV absorbent, chelating agen, anticorrosion and bactericidal agent, vitamins, animals and plants extract, spice etc.
As concrete above-mentioned oils and fats, can exemplify: Oleum Helianthi, American Avocado Tree oil, Oleum Gossypii semen, soybean oil, olive oil, macadimia nut oil, Oleum Arachidis hypogaeae semen, Semen Maydis oil, Oleum Brassicae campestris, Oleum sesami, safflower oil, Testa oryzae oil, Oleum Ricini, Jojoba oil, Camellia oil, ermine wet goods liquid fat; Oleum Cocois, Petiolus Trachycarpi oil, palm kernel oil, cocoa butter, fixed oil, hydrogenated castor wet goods solid grease etc.
As concrete above-mentioned wax class, can exemplify: Brazil wax, candelilla wax, Cera Flava, rice bran wax, montan wax, shellac wax, spermaceti, Jojoba wax, lanoline, liquid lanolin, reduction lanoline, hard lanoline etc.
As concrete above-mentioned hydrocarbon ils, can exemplify: ceresin, paraffin, liquid paraffin, liquid isoparaffin, hard paraffin, microwax, Fischer-Tropsch wax, polyethylene end, Tissuemat E, vaseline, squalane etc.
As concrete above-mentioned higher fatty acids, can exemplify: lauric acid, tetradecylic acid, Palmic acid, stearic acid, oleic acid, behenic acid, 9-undecylenic acid, isostearic acid, linoleic acid, linolenic acid, 12-hydroxy stearic acid etc.
As concrete above-mentioned higher alcohol, can exemplify: lauryl alcohol, myristyl alcohol, cetyl alcohol, stearyl alcohol, oleyl alcohol, lanolin alcohol, docosanol, cetearyl alcohol, isooctadecanol etc.
Polymer is formed as concrete above-mentioned anionic property overlay film, can exemplify: (methyl) alkyl acrylate copolymer, (methyl) acrylic acid/(methyl) alkyl acrylate copolymer, acrylic resin alkanolamine, methyl vinyl ether/maleate copolymer, vinyl acetate/crotonic acid copolymers, vinyl acetate/butenoic acid/neodecanoic acid ethylenic copolymer, vinyl acetate/butenoic acid/vinyl propionate copolymer, vinyl acetate/butyl maleate/isobornyl acrylate copolymer, acrylic acid/alkyl acrylate/alkyl acrylamide copolymer, polyvinyl pyrrolidone/acrylate/(methyl) acrylic copolymer, (styrene/acrylic Arrcostab) copolymer, (styrene/acrylamide) copolymer, urethane-acrylic copolymer, kayexalate etc.It should be noted that, in this description, " (methyl) acrylic acid " refers to both " acrylic acid " and " methacrylic acid ".
Polymer is formed as concrete above-mentioned cationic overlay film, can exemplify: vinyl pyrrolidone N, N-dimethylaminoethyl methacrylic acid copolymer dithyl sulfate salt, chlorination О-[2-hydroxyl-3-(trimethyl ammonium) propyl group] hydroxyethyl-cellulose, vinyl imidazole terchoride/vinylpyrrolidone copolymer, hydroxyethyl-cellulose/dimethyl diallyl ammonium chloride, polyvinyl pyrrolidone/alkyl amido acrylate/vinyl caprolactam copolymer, chloromethane vinyl imidazolelvinyl base pyrrolidinone copolymer, (vinyl pyrrolidone/dimethylamino-propyl Methacrylamide/lauryl dimethyl amine propyl methacrylamide) copolymer etc.
Polymer is formed as concrete above-mentioned both sexes overlay film, can exemplify: N-methacryloxyethyl-N, N-Dimethyl Ammonium-α-N-methyl carboxybetaine methacrylate copolymer, N, N-dimethyl-N-(2-methacryloxyethyl) amine=N-oxide methacrylate copolymer, Hydroxypropyl acrylate/butylaminoethyl/acrylic acid octyl group amide copolymer, the monochloro acetic acid both sexes compound of methacrylic acid dialkylamino ethyl/methacrylate copolymer, (isobutene ./diethyl amino propyl maleimide/maleic acid) copolymer etc.
Form polymer as concrete above-mentioned nonionic overlay film, can exemplify: polyvinyl pyrrolidone, vinyl pyrrolidone/vinyl acetate copolymer, vinyl pyrrolidone/Methacrylamide/Nvinylimidazole copolymers, vinyl methyl ether ethyl maleate copolymer, polyvinyl alcohol, Vinylcaprolactam homopolymer etc.
Hair grooming powder solid shape compositions of the present invention can be haircuted to hair owing to playing, can be given natural visual impression such effect with having no sticky feeling, and thus can be suitable for haircuting, can be suitable as use of haircuting.
In addition, Hair grooming powder solid shape cosmetics of the present invention possess above-mentioned Hair grooming powder solid shape compositions and preserve the container of this Hair grooming powder solid shape compositions.By providing with the state of Hair grooming powder solid shape cosmetics of the present invention, when haircuting also without the need to using comb, can implement easily to haircut.
The said vesse that above-mentioned Hair grooming powder solid shape cosmetics use is not particularly limited, the container selecting the form can preserving above-mentioned Hair grooming powder solid shape compositions can be suitable for.As said vesse, specifically, can exemplify the tank container of desirable lower cover, desirable lower cover box type container, be formed and renovate (See Open き Cover) tank container, be formed with the box type container, bar type container etc. renovated.
In the present invention, excellent from not only simplicity, and wait with going out also can easily again haircut in consider, preferably the desirable lower cover of use box type container or be formed with the box type container renovated.
It should be noted that, about Hair grooming powder solid shape cosmetics of the present invention, can be filled directly for above-mentioned Hair grooming powder solid shape compositions any form be filled in the form of container or above-mentioned Hair grooming powder solid shape compositions in the form of the inner vessel therein be arranged in container.Above-mentioned inner vessel therein is preferably arranged in said vesse in the mode can taken out, can load.In addition, the shape of above-mentioned Hair grooming powder solid shape composition molding is not particularly limited, as long as be the shape corresponding to the container of use or the shape of inner vessel therein.
As the material of the container that above-mentioned cosmetics use, be not particularly limited, such as PET resin, AS resin, ABS resin, polycarbonate resin etc. can be enumerated.In addition, being also not particularly limited the material of above-mentioned inner vessel therein, can be any material in metal and resin-made.
Hair grooming powder solid shape cosmetics of the present invention can be manufactured by known method.As concrete manufacture method, following method can be enumerated: such as, by the manufacture method of above-mentioned Hair grooming powder solid shape compositions (mix and blend thing) compression forming; Or, compression forming is not carried out to above-mentioned Hair grooming powder solid shape compositions (mix and blend thing), but utilizes the forming method different from compression forming to carry out the manufacture method of molding; Etc..
The manufacture method of compression forming can be any means in dry method and wet method.In addition, as the manufacture method of carrying out compression forming, specifically, the manufacture method possessing following operation can be exemplified: the 1st operation, by above-mentioned (A) composition (above-mentioned 1st powder body), above-mentioned (B) composition (above-mentioned oil preparation) and above-mentioned (C) composition (above-mentioned 2nd powder body) mix and blend, obtain mix and blend thing; 2nd operation, is directly filled in said vesse by above-mentioned mix and blend thing or is filled in the inner vessel therein be arranged in said vesse; With the 3rd operation, by the compression forming of above-mentioned mix and blend thing after filling.
The mixing and blending machine used in above-mentioned 1st operation is not particularly limited, the mixing and blending machine that above-mentioned (A) composition, above-mentioned (B) composition and above-mentioned (C) uniform composition can mix by suitable selection.As above-mentioned mixing and blending machine, Henschel mixer, blender blender, V-type blender, ribbon mixer, Nauta mixer (NAUTA MIXER), super mixer etc. can be exemplified.
In the present invention, the above-mentioned mix and blend thing obtained directly can be filled in said vesse or above-mentioned inner vessel therein in above-mentioned 1st operation.Uniformity when filling from the viewpoint of raising, hammer crusher can be used, sell the pulverizers such as excellent pulverizer, aerosol apparatus to pulverize above-mentioned mix and blend thing, fill again after the ground product of gained is sieved.In addition, in above-mentioned 2nd operation, uniformity when filling from the viewpoint of further raising, vibration can be imposed and fill above-mentioned mix and blend thing.
In above-mentioned 3rd operation, compression forming time institute applied pressure is not particularly limited, can according to the suitable adjustment of the mode of the powder solid shape becoming desired hardness.During compression forming, applied pressure is preferably more than 0.01MPa, is more preferably more than 0.05MPa, is preferably below 4MPa, is more preferably below 3MPa.
When carrying out compression forming by dry method, use above-mentioned manufacture method.When carrying out compression forming by wet method, preferably the above-mentioned mix and blend thing obtained in above-mentioned 1st operation and volatile solvent are carried out slurried.In addition, also can use hammer crusher, sell the pulverizers such as excellent pulverizer, aerosol apparatus to pulverize above-mentioned mix and blend thing, carry out slurried after the ground product of gained is sieved again.
As long as the solvent that the above-mentioned mix and blend thing of above-mentioned (A) composition, above-mentioned (B) composition and above-mentioned (C) composition can be made to become pulp-like for slurried above-mentioned volatile solvent is just not particularly limited.As above-mentioned volatile solvent, can enumerate such as: water, ethanol, isopropyl alcohol, n-butyl alcohol, isoparaffin, light isoparaffins, octamethylcy-clotetrasiloxane, decamethylcyclopentaandoxane, ten diformazan basic ring six siloxanes, octamethyltrisiloxane, tetradecamethylhexasiloxane, low viscosity methyl polysiloxane etc.Above-mentioned volatile solvent can be used alone one, also can use two or more by proper combination.
In order to above-mentioned mix and blend thing be made pulp-like by using above-mentioned volatile solvent, preferably relative to above-mentioned mix and blend thing 100 mass parts, use above-mentioned volatile solvent 10 mass parts ~ 150 mass parts, as long as be the slurry formed according to above-mentioned mass ratio, then can be more prone to be shaped to various shape.
In addition, when carrying out compression forming by wet method, from the viewpoint of the above-mentioned volatile solvent of removing, preferably carry out vacuum attraction drying when compression forming, more preferably use the means such as natural drying, heat drying, warm braw drying to carry out drying thereafter further.
On the other hand, as the manufacture method of not carrying out compression forming, the manufacture method possessing following operation can be exemplified: the 1st operation, by above-mentioned (A) composition, above-mentioned (B) composition and above-mentioned (C) composition mix and blend (above-mentioned powder constituents and above-mentioned oil preparation composition being uniformly mixed), obtain the mix and blend thing as above-mentioned Hair grooming powder solid shape compositions; 2nd operation, is directly filled in said vesse by the above-mentioned mix and blend thing obtained in above-mentioned 1st operation or is filled in the inner vessel therein be arranged in said vesse; With the 3rd operation, do not carry out compression forming after filling but utilize the forming method different from compression forming to carry out molding.
When not carrying out compression forming, as the concrete example of above-mentioned 3rd operation, following operation can be exemplified: use the means such as natural drying, heat drying, warm braw drying to carry out drying, thus by the operation of above-mentioned mix and blend thing molding; Or, by being cured by the operation of above-mentioned mix and blend thing molding.It should be noted that, when above-mentioned mix and blend thing is solidified, can adopt after filling by the method making it solidify after above-mentioned mix and blend thing heating for dissolving or by carry out after above-mentioned mix and blend thing heating for dissolving filling then make it solidify method in any means.
Use the method for haircuting of Hair grooming powder solid shape cosmetics of the present invention to possess following operation: the 1st operation, with finger tip or use applicator, wipe from the surface of above-mentioned Hair grooming powder solid shape compositions and get above-mentioned Hair grooming powder solid shape compositions; 2nd operation, with finger tip or use applicator, is applied on hair by wiping the above-mentioned Hair grooming powder solid shape compositions taken off; With the 3rd operation, with finger tip or palm, the above-mentioned Hair grooming powder solid shape compositions be applied on hair is rubbed on hair, implement thus to haircut.
In method of haircuting of the present invention, maximum feature is, wipes to get said composition to implement haircut from the surface of above-mentioned Hair grooming powder solid shape compositions.As wiping the means of getting above-mentioned composition, being not particularly limited, preferably wiping with finger tip or use applicator and getting above-mentioned composition.By with finger tip, easily above-mentioned composition is smeared to thin portion, can fully haircut to thin portion.In addition, by using above-mentioned applicator, easily smearing above-mentioned composition on the whole at hair, can haircut to hair entirety.
As long as the above-mentioned applicator used can be got said composition from the surface wiping of above-mentioned Hair grooming powder solid shape compositions and just be not particularly limited.As above-mentioned applicator, can enumerate such as: hairbrush, the special powder puff of powder solid dosage form etc.
Of the present inventionly haircut in method, smear rear finger tip or palm is implemented to haircut in the mode of being rubbed on hair by the above-mentioned composition be applied on hair, thereby, it is possible to haircut into desired hair style.By above-mentioned method of haircuting, can implement easily to haircut to thin portion for from hair entirety.
Hair grooming powder solid shape compositions of the present invention and possess said composition and can have no sticky feeling with the Hair grooming powder solid shape cosmetics of container and haircut into the hair style of expectation, natural visual impression can be given, provide new-type dosage form, therefore, be compositions and the cosmetics can replacing existing Hair grooming cosmetics.
Embodiment
Based on embodiment, the present invention will be described in more detail below.The present invention is not limited to these embodiments.It should be noted that, unless otherwise specified, blend amount represents with " quality % ".
(preparation of sample)
According to the composition that table 1 is recorded, prepared each hair grooming compositions of embodiment 1 ~ 10 and comparative example 1 ~ 5 by following method for making, and carry out following evaluation.Result is remembered in the lump in table 1 ~ 3.It should be noted that, evaluate be all 23 DEG C, implement under the certain condition of the constant temperature and humidity of humidity 60%.It should be noted that, in embodiment 1 ~ 10 and comparative example 1 ~ 2, obtain Hair grooming powder solid shape compositions.In comparative example 3 ~ 5, the non-integration of each powder body, obtaining is not the Powdered hair grooming compositions of powder solid shape.
(method for making)
After the powder constituents recorded in table 1 ~ 3 being mixed with Henschel mixer, add oil preparation, carry out mix and blend further, obtain mix and blend thing.Next, mix and blend thing is filled in the inner vessel therein be arranged in box type container, carries out compression forming.In addition, about the compositions not containing oil preparation, with Henschel mixer by after powder constituents mix and blend, be filled in the inner vessel therein be arranged in box type container, carry out compression forming.
(test example 1: the evaluation of dispersing of powder constituents)
20 officials can evaluate professional and get hair grooming compositions in the mode of stroking from the surface wiping of obtained hair grooming compositions with finger tip, carry out sense evaluation according to following metewand to " dispersing of powder constituents " now.
The metewand > dispersed of < powder constituents
Zero (well): have more than 16 answers " without the dispersing of powder constituents, can wipe and get compositions " in 20.
△ (slightly good): have 10 ~ 15 answers " without the dispersing of powder constituents, can wipe and get compositions " in 20.
× (bad): have less than 9 answers " without the dispersing of powder constituents, can wipe and get compositions " in 20.
(test example 2: the evaluation of sticky feeling and haircuting property)
20 officials having carried out the evaluation of test example 1 can evaluate professional use obtain hair grooming compositions, implement to haircut to wig (course body model (レ ッ ス Application マ ネ キ Application): Yukari Japan society manufactures) by following method of haircuting, about " haircuting property " when haircuting, carry out sense evaluation according to following metewand.
(method of haircuting)
Get above-mentioned hair grooming compositions in the mode of stroking from the surface wiping of obtained hair grooming compositions with finger tip, and be applied on above-mentioned wig.Next, implement to haircut in the mode that above-mentioned hair grooming compositions is rubbed on hair with finger tip or palm.
The metewand > of haircuting property of <
Zero (well): have more than 16 answers " not have sticky feeling, desired hair style can be haircuted into " in 20.
△ (slightly good): have 10 ~ 15 answers " not have sticky feeling, desired hair style can be haircuted into " in 20.
× (bad): have less than 9 answers " not have sticky feeling, desired hair style can be haircuted into " in 20.
(test example 3: the evaluation of visual impression)
20 officials having carried out the evaluation of above-mentioned test example 1,2 can evaluate professional and carry out visual valuation according to following metewand to " visual impression of hair " after after the evaluation of above-mentioned test example 2 10 minutes.
The metewand > of the visual impression of < hair
Zero (well): have more than 16 answers " without floating powder, to have natural visual impression " in 20.
△ (slightly good): have 10 ~ 15 answers " without floating powder, to have natural visual impression " in 20.
× (bad): have less than 9 answers " without floating powder, to have natural visual impression " in 20.
[table 1]
(※ 1) AEROSIL 300 (manufacture of NIPPON AEROSIL society)
(※ 2) AEROSIL 200V (manufacture of NIPPON AEROSIL society)
(※ 3) Sylysia 310P (manufacture of Fuji Silysia Chemical society)
(※ 4) AEROSIL R8200 (manufacture of NIPPON AEROSIL society)
(※ 5) AEROSIL RX300 (manufacture of NIPPON AEROSIL society)
[table 2]
(※ 1) AEROSIL 300 (manufacture of NIPPON AEROSIL society)
(※ 2) AEROSIL 200V (manufacture of NIPPON AEROSIL society)
(※ 3) Sylysia 310P (manufacture of Fuji Silysia Chemical society)
(※ 4) AEROSIL R8200 (manufacture of NIPPON AEROSIL society)
(※ 5) AEROSIL RX300 (manufacture of NIPPON AEROSIL society)
[table 3]
(※ 1) AEROSIL 300 (manufacture of NIPPON AEROSIL society)
(※ 2) AEROSIL 200V (manufacture of NIPPON AEROSIL society)
(※ 3) Sylysia 310P (manufacture of Fuji Silysia Chemical society)
(※ 4) AEROSIL R8200 (manufacture of NIPPON AEROSIL society)
(※ 5) AEROSIL RX300 (manufacture of NIPPON AEROSIL society)
From the result shown in table 1 ~ 3, for the Hair grooming powder solid shape compositions of embodiment 1 ~ 10, powder constituents does not disperse, the Hair grooming powder solid shape compositions of taking in required minimum of implementing to haircut can be wiped from the surface of Hair grooming powder solid shape compositions, can have no sticky feeling and haircut into desired hair style, further, without floating powder, there is natural visual impression after haircuting.
On the other hand, known: for not containing the Hair grooming powder solid shape compositions as the comparative example 1 ~ 2 of above-mentioned (A) composition of neccessary composition in the present invention, desired hair style cannot to be haircuted into, cannot function of haircuting be played completely.In addition, for not containing the Powdered hair grooming compositions as the comparative example 3 ~ 4 of above-mentioned (B) composition of neccessary composition in the present invention, known: because character is Powdered, thus not only powder constituents disperses, and be difficult to haircut into desired hair style, visual impression is also poor.In addition, for the Powdered hair grooming compositions do not contained as the comparative example 5 of above-mentioned (C) composition of neccessary composition in the present invention, known: although can have no sticky feeling and haircut into desired hair style, but visual impression is poor, and due to character be Powdered, thus powder constituents disperses.
Below, Hair grooming powder solid shape compositions of the present invention is shown and there are the Hair grooming powder solid shape cosmetics of said composition and container.It should be noted that, content is quality %.
[table 4]
With Henschel mixer by after the powder constituents mixing in mentioned component, add the oil preparation composition in mentioned component, further mix and blend.Next, mix and blend thing is filled in the inner vessel therein be arranged in box type container, carries out compression forming.
[table 5]
With Henschel mixer by after the powder constituents mixing in mentioned component, add the oil preparation composition in mentioned component, further mix and blend.Next, mix and blend thing is filled in the inner vessel therein be arranged in box type container, carries out compression forming.
Claims (10)
1. a Hair grooming powder solid shape compositions, it is powder solid shape, for hair, and contains:
1st powder body, described 1st powder body is at least one in silicic acid anhydride and hydrophobization silicic acid anhydride;
Oil preparation, described oil preparation is at least one in fatty acid ester oil and silicone oil; With
2nd powder body, described 2nd powder body is the powder body beyond above-mentioned 1st powder body.
2. Hair grooming powder solid shape compositions as claimed in claim 1, wherein, the oil absorption of described 1st powder body meets 100mL/100g ~ 1000mL/100g.
3. Hair grooming powder solid shape compositions as claimed in claim 1 or 2, wherein, the bulk density of described 1st powder body meets 80g/L ~ 300g/L.
4. the Hair grooming powder solid shape compositions as described in any one of claims 1 to 3, wherein, described 2nd powder body is be selected from least one by Talcum, Muscovitum, Kaolin, sericite and barium sulfate.
5. the Hair grooming powder solid shape compositions as described in any one of Claims 1 to 4, wherein, the content of described 1st powder body is 5 quality % ~ 50 quality %, and the content of described oil preparation is 5 quality % ~ 40 quality %, and the content of described 2nd powder body is 30 quality % ~ 80 quality %.
6. the Hair grooming powder solid shape compositions as described in any one of Claims 1 to 5, it is the powder solid shape obtained by compression forming, and it is by carrying out mix and blend to described 1st powder body, described oil preparation and described 2nd powder body and obtain mix and blend thing and carry out compression forming to this mix and blend thing and obtain.
7. Hair grooming powder solid shape cosmetics, it possesses the Hair grooming powder solid shape compositions described in any one of claim 1 ~ 6 and preserves the container of said composition.
8. the manufacture method of Hair grooming powder solid shape cosmetics, its for possess Claims 1 to 5 any one described in Hair grooming powder solid shape compositions and preserve the manufacture method of Hair grooming powder solid shape cosmetics of container of described Hair grooming powder solid shape compositions, described Hair grooming powder solid shape compositions is used for haircuting to hair
This manufacture method possesses:
By described 1st powder body, described oil preparation and described 2nd powder body mix and blend, obtain the operation of mix and blend thing;
2nd operation, is directly filled in described container by described mix and blend thing or is filled in the inner vessel therein be arranged in described container; With
3rd operation, after filling by the compression forming of described mix and blend thing or after filling compression forming is not carried out to described mix and blend thing but utilize the forming method different from compression forming carry out molding.
9. the manufacture method of Hair grooming powder solid shape cosmetics as claimed in claim 8, wherein, described 3rd operation is by the 3rd operation of described mix and blend thing compression forming after filling.
10. use a method of haircuting for Hair grooming powder solid shape cosmetics, it is for using the method for haircuting of the Hair grooming powder solid shape cosmetics described in claim 7, and this method of haircuting possesses:
1st operation, with finger tip or use applicator, wipes from the surface of described Hair grooming powder solid shape compositions and gets described Hair grooming powder solid shape compositions;
2nd operation, with finger tip or use applicator, is applied on hair by wiping the described Hair grooming powder solid shape compositions taken off; With
3rd operation, uses finger tip or palm, rubs the described Hair grooming powder solid shape compositions be applied on hair on hair, implements thus to haircut.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012216962 | 2012-09-28 | ||
| JP2012-216962 | 2012-09-28 | ||
| PCT/JP2013/075240 WO2014050679A1 (en) | 2012-09-28 | 2013-09-19 | Powdery solid composition for hair, powdery solid cosmetic for hair, method for manufacturing powdery solid cosmetic for hair, method for hairdressing using powdery solid cosmetic for hair |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104321047A true CN104321047A (en) | 2015-01-28 |
| CN104321047B CN104321047B (en) | 2017-02-15 |
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| CN201380025975.3A Expired - Fee Related CN104321047B (en) | 2012-09-28 | 2013-09-19 | Powdery solid composition for hair, powdery solid cosmetic for hair, method for manufacturing powdery solid cosmetic for hair, method for hairdressing using powdery solid cosmetic for hair |
Country Status (4)
| Country | Link |
|---|---|
| JP (1) | JP6166730B2 (en) |
| KR (1) | KR101676554B1 (en) |
| CN (1) | CN104321047B (en) |
| WO (1) | WO2014050679A1 (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPWO2015105128A1 (en) * | 2014-01-08 | 2017-03-23 | アース製薬株式会社 | Bed bug control agent, bed bug control composition, and bed bug control method |
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| JP2008106050A (en) * | 2006-09-29 | 2008-05-08 | Kose Corp | Oily cake cosmetic |
| CN102198052A (en) * | 2010-03-25 | 2011-09-28 | 株式会社漫丹 | Powdery hair-arranging agent |
| US20110243866A1 (en) * | 2010-02-23 | 2011-10-06 | Art Cosmetics S.R.L. | Cosmetic composition for make-up and process for making same |
| JP2011219455A (en) * | 2010-03-25 | 2011-11-04 | Mandom Corp | Powdery hair dressing agent |
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| JPH09301838A (en) | 1996-05-14 | 1997-11-25 | Pola Chem Ind Inc | Liquid hairdressing |
| JP2000204025A (en) | 1999-01-11 | 2000-07-25 | Kose Corp | Foamy hair-dressing preparation |
| JP3917352B2 (en) * | 2000-02-25 | 2007-05-23 | 株式会社資生堂 | Hairdressing fee |
| JP4101437B2 (en) | 2000-05-31 | 2008-06-18 | 株式会社コーセー | Gel cosmetic |
| JP2002114652A (en) | 2000-10-02 | 2002-04-16 | Nakano Seiyaku Kk | Waxy hair dressing |
| JP2002234817A (en) * | 2001-02-08 | 2002-08-23 | Tsuyako Uehara | Foundation for border of hair and method using the same |
| JP2003026550A (en) * | 2001-07-12 | 2003-01-29 | Kanebo Ltd | Hair cosmetic |
| JP2006089470A (en) * | 2004-08-26 | 2006-04-06 | Kose Corp | Colorant for hair |
| JP5276793B2 (en) * | 2007-03-15 | 2013-08-28 | 紀伊産業株式会社 | Molding head and solid powder cosmetic molding method using the same |
| JP5022140B2 (en) * | 2007-08-20 | 2012-09-12 | 株式会社トキワ | Solid powder cosmetic |
| JP5582555B2 (en) | 2008-01-25 | 2014-09-03 | 株式会社 資生堂 | Oil-in-water emulsified hair conditioner |
| JP2009242291A (en) * | 2008-03-31 | 2009-10-22 | Shiseido Co Ltd | Hair dressing agent |
| JP5623790B2 (en) | 2010-05-31 | 2014-11-12 | 花王株式会社 | Mist-like hair conditioner |
| JP2012056916A (en) * | 2010-09-13 | 2012-03-22 | Mandom Corp | Powdery cosmetic |
| JP5497243B2 (en) * | 2012-03-28 | 2014-05-21 | 株式会社マンダム | Powdered solid hair composition, powdered solid hair cosmetic, method for producing powdered solid hair cosmetic, and hair styling method using powdered solid hair cosmetic |
-
2013
- 2013-09-19 JP JP2014538428A patent/JP6166730B2/en active Active
- 2013-09-19 WO PCT/JP2013/075240 patent/WO2014050679A1/en active Application Filing
- 2013-09-19 CN CN201380025975.3A patent/CN104321047B/en not_active Expired - Fee Related
- 2013-09-19 KR KR1020147033216A patent/KR101676554B1/en active IP Right Grant
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008106050A (en) * | 2006-09-29 | 2008-05-08 | Kose Corp | Oily cake cosmetic |
| US20110243866A1 (en) * | 2010-02-23 | 2011-10-06 | Art Cosmetics S.R.L. | Cosmetic composition for make-up and process for making same |
| CN102198052A (en) * | 2010-03-25 | 2011-09-28 | 株式会社漫丹 | Powdery hair-arranging agent |
| JP2011219455A (en) * | 2010-03-25 | 2011-11-04 | Mandom Corp | Powdery hair dressing agent |
Also Published As
| Publication number | Publication date |
|---|---|
| JPWO2014050679A1 (en) | 2016-08-22 |
| KR101676554B1 (en) | 2016-11-15 |
| JP6166730B2 (en) | 2017-07-19 |
| WO2014050679A1 (en) | 2014-04-03 |
| KR20150035551A (en) | 2015-04-06 |
| CN104321047B (en) | 2017-02-15 |
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