CN104309185A - Method for preparing red mud-expanded perlite multi-face colored decoration lightweight wall material - Google Patents

Method for preparing red mud-expanded perlite multi-face colored decoration lightweight wall material Download PDF

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Publication number
CN104309185A
CN104309185A CN201410535330.0A CN201410535330A CN104309185A CN 104309185 A CN104309185 A CN 104309185A CN 201410535330 A CN201410535330 A CN 201410535330A CN 104309185 A CN104309185 A CN 104309185A
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raw material
red mud
expanded perlite
preparation
wall material
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CN201410535330.0A
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CN104309185B (en
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唐竹兴
刘坤
刘敏
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Shandong University of Technology
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Shandong University of Technology
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B37/00Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/14Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the properties of the layers
    • B32B37/24Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the properties of the layers with at least one layer not being coherent before laminating, e.g. made up from granular material sprinkled onto a substrate
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B33/00Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings; Layered products designed for particular purposes not covered by another single class
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B30/00Compositions for artificial stone, not containing binders
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2264/00Composition or properties of particles which form a particulate layer or are present as additives
    • B32B2264/10Inorganic particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00Properties of the layers or laminate
    • B32B2307/10Properties of the layers or laminate having particular acoustical properties
    • B32B2307/102Insulating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00Properties of the layers or laminate
    • B32B2307/30Properties of the layers or laminate having particular thermal properties
    • B32B2307/304Insulating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00Properties of the layers or laminate
    • B32B2307/50Properties of the layers or laminate having particular mechanical properties
    • B32B2307/56Damping, energy absorption
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2607/00Walls, panels

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)
  • Glass Compositions (AREA)
  • Finishing Walls (AREA)

Abstract

The invention discloses a method for preparing a red mud-expanded perlite multi-face colored decoration lightweight wall material. The red mud-expanded perlite multi-face colored decoration lightweight wall material is characterized by consisting of three parts, namely a colored decoration layer (1), a transition layer (2) and a thermal insulation layer (3). The red mud-expanded perlite multi-face colored decoration lightweight wall material disclosed by the invention is subjected to once-firing, and the transition layer is added between the colored decoration layer and the thermal insulation layer, so that the defects that the pore diameter is extremely large and the bonding strength and thermal shock resistance are reduced between the colored decoration layer and the thermal insulation layer due to inconsistent melting points of materials are effectively overcome. Ceramic colorants are added, so that interior and exterior wall decoration materials of a single color, composite colors and various colors and patterns are prepared, and extra decoration is not needed. The method is simple in production process and low in cost and has a good building heat preservation effect and energy-saving and environment-friendly effects, and the produced red mud-expanded perlite multi-face colored decoration lightweight wall material integrates multiple functions such as decoration, heat preservation, heat insulation, sound insulation, shock resistance and the like.

Description

The preparation method of red mud-expanded perlite multiaspect illuminated light wall material
Technical field
The present invention relates to the preparation method of red mud-expanded perlite multiaspect illuminated light wall material, belong to field of ceramic preparation technology.
Background technology
Red mud-expanded perlite multiaspect illuminated light wall material collection decoration, heat insulation integrated New Type Light-weight Wall Material, being adopt colored microcrystalline glass decorating wall material, is a kind of novel wall material with decoration, insulation, waterproof, sound insulation and the function integration such as shockproof.Current construction material generally adopts structural clay tile, cement hollow building blocks and air-entrained concrete building block etc., these construction material heat-insulating properties and decorate properties poor, needing when being applied to inner, external wall additionally to add tiling or wallpaper, is the building and ornament materials that manufacturing cost is high.
Summary of the invention
The object of this invention is to provide the preparation method of red mud-expanded perlite multiaspect illuminated light wall material that a kind of serviceability is excellent, production cost is low, its technical scheme is:
The preparation method of red mud-expanded perlite multiaspect illuminated light wall material, red mud-expanded perlite multiaspect illuminated light wall material is made up of color coat (1), transition zone (2), heat-insulation layer (3) three part, and concrete grammar comprises the following steps:
A. the preparation of color coat (1) raw material: by ceramic raw materials such as clay, quartz sand, borax, zircon sand, zinc oxide, albite, potassic feldspar, lithium feldspar, tin oxide, brium carbonates, by chemical composition be: SiO 2be 12 ~ 32%, B 2o 3be 10 ~ 25%, Al 2o 3be 3 ~ 6%, K 2o is 6 ~ 11%, Li 2o is 1 ~ 6%, Na 2o is 12 ~ 1%, ZnO be 11 ~ 21%, BaO is 6 ~ 11%, TiO 2be 4 ~ 11%, SnO be 0 ~ 5%, ZrO 2be 0 ~ 6% batching and frit raw material is made in fine grinding, then be 50 ~ 95% being 5 ~ 50% with ceramic pigment weight ratio by frit raw material with weight ratio, ratio uniform mixes, and makes 850 ~ 1000 DEG C of melt process the colored frit particle that granularity is 1 ~ 3mm;
B. the preparation of transition zone (2) raw material: be 50 ~ 95% make transition zone raw material with clay 5 ~ 50% Homogeneous phase mixing with weight ratio by the frit raw material of preparation in step (a);
C. the preparation of heat-insulation layer (3) raw material: red mud being added weight ratio is that red mud mud made by the water of 30 ~ 60% and the waterglass of 5 ~ 20%, be 10 ~ 40% Homogeneous phase mixing by red mud mud and expanded perlite granule with volume ratio again, after drying, make heat-insulation layer raw material;
The preparation of d. red mud-expanded perlite multiaspect illuminated light wall material: first adopt load bearing board (4) left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and apply releasing agent, then by the colored frit particle (1) of preparation in step (a) evenly plain cloth in holding the bottom of burning mould, and the medial surface being evenly distributed in and holding and burn mould is separated with external partition (5), thickness is 1 ~ 10mm, profile height is 25 ~ 35mm, use internal partition (6) that the transition zone raw material of preparation in step (b) is evenly distributed in the inner side of colored frit particle again, thickness is 1 ~ 5mm, then the even plain cloth of heat-insulation layer raw material step (c) prepared is inside transition zone raw material, the gross thickness of vertically holding the inner plane direction, bottom of burning mould is made to reach 25 ~ 35mm, then the external partition (5) of surrounding is taken out, internal partition (6), 1 ~ 5 hour is incubated at the temperature of 800 ~ 1100 DEG C, crystallization at the temperature of 400 ~ 750 DEG C, anneal 5 ~ 15 hours, through cooling, come out of the stove, cutting and surface grinding make red mud-expanded perlite multiaspect illuminated light wall material.
Compared with prior art, its advantage is in the present invention:
1, technique is simple, and the red mud-expanded perlite multiaspect illuminated light wall material of production has stronger decoration, waterproof, insulation, heat insulation, sound insulation and antiknock quality;
2, red mud-expanded perlite multiaspect illuminated light wall material can be prepared into the interior and exterior decoration material of the colors such as monochrome, tertiary colour and pattern by adding ceramic toner;
3, in the middle of color coat and heat-insulation layer, add transition zone, efficiently solve that the hole diameter caused because material melting point is inconsistent between color coat and heat-insulation layer is excessive, shortcoming that bond strength and thermal shock resistance reduce;
4, the present invention is owing to have employed once-firing, and without the need to additional decoration, reduces cost significantly, and building heat preservation is effective, energy-saving and environmental protection.
Accompanying drawing explanation
Fig. 1 is that holding of red mud-expanded perlite multiaspect illuminated light wall material burns mould and assembly structure schematic diagram;
1, color coat; 2, transition zone; 3, heat-insulation layer; 4, burning version is held; 5, external partition; 6, internal partition.
Detailed description of the invention
embodiment 1
A. the preparation of color coat (1) raw material: by ceramic raw materials such as clay, quartz sand, borax, zircon sand, zinc oxide, albite, potassic feldspar, lithium feldspar, tin oxide, brium carbonates, by chemical composition be: SiO 2be 32%, B 2o 3be 25%, Al 2o 3be 3%, K 2o is 6%, Li 2o is 1%, Na 2o is 12%, ZnO be 11%, BaO is 6%, TiO 2be 4% batching and frit raw material is made in fine grinding, then be 50% being 50% with ceramic pigment weight ratio by frit raw material with weight ratio, ratio uniform mixes, and makes 850 DEG C of melt process the colored frit particle that granularity is 1mm;
B. the preparation of transition zone (2) raw material: be 50% make transition zone raw material with clay 50% Homogeneous phase mixing with weight ratio by the frit raw material of preparation in step (a);
C. the preparation of heat-insulation layer (3) raw material: red mud being added weight ratio is that red mud mud made by the water of 30% and the waterglass of 20%, then be 10% Homogeneous phase mixing by red mud mud and expanded perlite granule with volume ratio, make heat-insulation layer raw material after drying;
The preparation of d. red mud-expanded perlite multiaspect illuminated light wall material: first adopt load bearing board (4) left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and apply releasing agent, then by the colored frit particle (1) of preparation in step (a) evenly plain cloth in holding the bottom of burning mould, and the medial surface being evenly distributed in and holding and burn mould is separated with external partition (5), thickness is 1mm, profile height is 25mm, use internal partition (6) that the transition zone raw material of preparation in step (b) is evenly distributed in the inner side of colored frit particle again, thickness is 1mm, then the even plain cloth of heat-insulation layer raw material step (c) prepared is inside transition zone raw material, the gross thickness of vertically holding the inner plane direction, bottom of burning mould is made to reach 25mm, then the external partition (5) of surrounding is taken out, internal partition (6), 1 hour is incubated at the temperature of 800 DEG C, crystallization at the temperature of 400 DEG C, anneal 5 hours, through cooling, come out of the stove, cutting and surface grinding make red mud-expanded perlite multiaspect illuminated light wall material.
The purity of testing proportion material used is technical pure.
embodiment 2
A. the preparation of color coat (1) raw material: by ceramic raw materials such as clay, quartz sand, borax, zircon sand, zinc oxide, albite, potassic feldspar, lithium feldspar, tin oxide, brium carbonates, by chemical composition be: SiO 2be 22%, B 2o 3be 17.5%, Al 2o 3be 4.5%, K 2o is 8.5%, Li 2o is 3.5%, Na 2o is 6.5%, ZnO be 16%, BaO is 8.5%, TiO 2be 7.5%, SnO be 2.5%, ZrO 2be 3% batching and frit raw material is made in fine grinding, then be 72% being 28% with ceramic pigment weight ratio by frit raw material with weight ratio, ratio uniform mixes, and makes 920 DEG C of melt process the colored frit particle that granularity is 2mm;
B. the preparation of transition zone (2) raw material: be 75% make transition zone raw material with clay 25% Homogeneous phase mixing with weight ratio by the frit raw material of preparation in step (a);
C. the preparation of heat-insulation layer (3) raw material: red mud being added weight ratio is that red mud mud made by the water of 45% and the waterglass of 13%, then be 25% Homogeneous phase mixing by red mud mud and expanded perlite granule with volume ratio, make heat-insulation layer raw material after drying;
The preparation of d. red mud-expanded perlite multiaspect illuminated light wall material: first adopt load bearing board (4) left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and apply releasing agent, then by the colored frit particle (1) of preparation in step (a) evenly plain cloth in holding the bottom of burning mould, and the medial surface being evenly distributed in and holding and burn mould is separated with external partition (5), thickness is 5mm, profile height is 30mm, use internal partition (6) that the transition zone raw material of preparation in step (b) is evenly distributed in the inner side of colored frit particle again, thickness is 3mm, then the even plain cloth of heat-insulation layer raw material step (c) prepared is inside transition zone raw material, the gross thickness of vertically holding the inner plane direction, bottom of burning mould is made to reach 30mm, then the external partition (5) of surrounding is taken out, internal partition (6), 3 hours are incubated at the temperature of 950 DEG C, crystallization at the temperature of 600 DEG C, anneal 10 hours, through cooling, come out of the stove, cutting and surface grinding make red mud-expanded perlite multiaspect illuminated light wall material.
The purity of testing proportion material used is technical pure.
embodiment 3
A. the preparation of color coat (1) raw material: by ceramic raw materials such as clay, quartz sand, borax, zircon sand, zinc oxide, albite, potassic feldspar, lithium feldspar, tin oxide, brium carbonates, by chemical composition be: SiO 2be 12%, B 2o 3be 10%, Al 2o 3be 6%, K 2o is 11%, Li 2o is 6%, Na 2o is 1%, ZnO be 21%, BaO is 11%, TiO 2be 11%, SnO be 5%, ZrO 2be 6% batching and frit raw material is made in fine grinding, then be 95% being 5% with ceramic pigment weight ratio by frit raw material with weight ratio, ratio uniform mixes, and makes 1000 DEG C of melt process the colored frit particle that granularity is 3mm;
B. the preparation of transition zone (2) raw material: be 95% make transition zone raw material with clay 5% Homogeneous phase mixing with weight ratio by the frit raw material of preparation in step (a);
C. the preparation of heat-insulation layer (3) raw material: red mud being added weight ratio is that red mud mud made by the water of 60% and the waterglass of 5%, then be 40% Homogeneous phase mixing by red mud mud and expanded perlite granule with volume ratio, make heat-insulation layer raw material after drying;
The preparation of d. red mud-expanded perlite multiaspect illuminated light wall material: first adopt load bearing board (4) left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and apply releasing agent, then by the colored frit particle (1) of preparation in step (a) evenly plain cloth in holding the bottom of burning mould, and the medial surface being evenly distributed in and holding and burn mould is separated with external partition (5), thickness is 10mm, profile height is 35mm, use internal partition (6) that the transition zone raw material of preparation in step (b) is evenly distributed in the inner side of colored frit particle again, thickness is 5mm, then the even plain cloth of heat-insulation layer raw material step (c) prepared is inside transition zone raw material, the gross thickness of vertically holding the inner plane direction, bottom of burning mould is made to reach 35mm, then the external partition (5) of surrounding is taken out, internal partition (6), 5 hours are incubated at the temperature of 1100 DEG C, crystallization at the temperature of 750 DEG C, anneal 15 hours, through cooling, come out of the stove, cutting and surface grinding make red mud-expanded perlite multiaspect illuminated light wall material.
The purity of testing proportion material used is technical pure.

Claims (1)

1. the preparation method of red mud-expanded perlite multiaspect illuminated light wall material, it is characterized in that: red mud-expanded perlite multiaspect illuminated light wall material is made up of color coat (1), transition zone (2), heat-insulation layer (3) three part, and concrete grammar comprises the following steps:
A. the preparation of color coat (1) raw material: by ceramic raw materials such as clay, quartz sand, borax, zircon sand, zinc oxide, albite, potassic feldspar, lithium feldspar, tin oxide, brium carbonates, by chemical composition be: SiO 2be 12 ~ 32%, B 2o 3be 10 ~ 25%, Al 2o 3be 3 ~ 6%, K 2o is 6 ~ 11%, Li 2o is 1 ~ 6%, Na 2o is 12 ~ 1%, ZnO be 11 ~ 21%, BaO is 6 ~ 11%, TiO 2be 4 ~ 11%, SnO be 0 ~ 5%, ZrO 2be 0 ~ 6% batching and frit raw material is made in fine grinding, then be 50 ~ 95% being 5 ~ 50% with ceramic pigment weight ratio by frit raw material with weight ratio, ratio uniform mixes, and makes 850 ~ 1000 DEG C of melt process the colored frit particle that granularity is 1 ~ 3mm;
B. the preparation of transition zone (2) raw material: be 50 ~ 95% make transition zone raw material with clay 5 ~ 50% Homogeneous phase mixing with weight ratio by the frit raw material of preparation in step (a);
C. the preparation of heat-insulation layer (3) raw material: red mud being added weight ratio is that red mud mud made by the water of 30 ~ 60% and the waterglass of 5 ~ 20%, be 10 ~ 40% Homogeneous phase mixing by red mud mud and expanded perlite granule with volume ratio again, after drying, make heat-insulation layer raw material;
The preparation of d. red mud-expanded perlite multiaspect illuminated light wall material: first adopt load bearing board (4) left, right, before, the cube that rear and bottom surface surrounds top-open holds burning mould, and apply releasing agent, then by the colored frit particle (1) of preparation in step (a) evenly plain cloth in holding the bottom of burning mould, and the medial surface being evenly distributed in and holding and burn mould is separated with external partition (5), thickness is 1 ~ 10mm, profile height is 25 ~ 35mm, use internal partition (6) that the transition zone raw material of preparation in step (b) is evenly distributed in the inner side of colored frit particle again, thickness is 1 ~ 5mm, then the even plain cloth of heat-insulation layer raw material step (c) prepared is inside transition zone raw material, the gross thickness of vertically holding the inner plane direction, bottom of burning mould is made to reach 25 ~ 35mm, then the external partition (5) of surrounding is taken out, internal partition (6), 1 ~ 5 hour is incubated at the temperature of 800 ~ 1100 DEG C, crystallization at the temperature of 400 ~ 750 DEG C, anneal 5 ~ 15 hours, through cooling, come out of the stove, cutting and surface grinding make red mud-expanded perlite multiaspect illuminated light wall material.
CN201410535330.0A 2014-10-13 2014-10-13 The preparation method of red mud-expanded perlite multiaspect illuminated light wall material Expired - Fee Related CN104309185B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105967654A (en) * 2016-05-17 2016-09-28 岑溪市新建球陶瓷有限公司 Preparation method of thermal-insulation external tile

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004072397A1 (en) * 2003-02-11 2004-08-26 Saint-Gobain Isover Double-shelled separating wall with a lining made of mineral wool
CN102875112A (en) * 2012-09-15 2013-01-16 汉寿县永兴砖厂 Sludge poured colorful building board
CN103641437A (en) * 2013-11-25 2014-03-19 大连创达技术交易市场有限公司 Preparation method of composite heat insulation material
CN103669773A (en) * 2013-11-22 2014-03-26 徐花 Outer wall decorative wallboard made of heat preservation energy-saving composite materials

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004072397A1 (en) * 2003-02-11 2004-08-26 Saint-Gobain Isover Double-shelled separating wall with a lining made of mineral wool
CN102875112A (en) * 2012-09-15 2013-01-16 汉寿县永兴砖厂 Sludge poured colorful building board
CN103669773A (en) * 2013-11-22 2014-03-26 徐花 Outer wall decorative wallboard made of heat preservation energy-saving composite materials
CN103641437A (en) * 2013-11-25 2014-03-19 大连创达技术交易市场有限公司 Preparation method of composite heat insulation material

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105967654A (en) * 2016-05-17 2016-09-28 岑溪市新建球陶瓷有限公司 Preparation method of thermal-insulation external tile

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