CN104304240A - Method for making fresh flower embedded specimen - Google Patents

Method for making fresh flower embedded specimen Download PDF

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Publication number
CN104304240A
CN104304240A CN201410513678.XA CN201410513678A CN104304240A CN 104304240 A CN104304240 A CN 104304240A CN 201410513678 A CN201410513678 A CN 201410513678A CN 104304240 A CN104304240 A CN 104304240A
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CN
China
Prior art keywords
flower
silica gel
gel particle
fresh flower
flowers
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Pending
Application number
CN201410513678.XA
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Chinese (zh)
Inventor
隋鸿锦
盛金菊
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DALIAN HOFFEN BIO-TECHNIQUE Co Ltd
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DALIAN HOFFEN BIO-TECHNIQUE Co Ltd
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Priority to CN201410513678.XA priority Critical patent/CN104304240A/en
Publication of CN104304240A publication Critical patent/CN104304240A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a method for making a fresh flower embedded specimen. The method comprises the steps of: taking out fresh flowers, and mixing a silica gel particle drying agent and a metal salt according to the mass ratio of (1-3) to 1; placing the flowers on the drying agent, scattering the silica gel particle drying agent mixed with the metal salt onto the fresh flowers to embed the flowers, placing the embedded flowers in an oven at 40 DEG C to 45 DEG C, heating for 4 to 20 hours, increasing the temperature from 50 DEG C to 70 DEG C, heating for 2 to 4 hours to change the silica gel particle drying agent into blue, taking out the dried flowers, removing the silica gel particle drying agent and the metal salt attached onto petals, placing the petals into a drying vessel for later use, placing liquid epoxy resin into a mold, immersing the dried flowers into the liquid epoxy resin, vacummizing by using a vacuum pump to remove air bubbles, and directly demolding after the liquid epoxy resin is completely solidified. The method for making the fresh flower embedded specimen, disclosed by the invention, is simple in production flow, economic in cost, and available for better preserving the color and shape of the original flowers without leaving dents on the surfaces of the petals.

Description

A kind of preparation method of fresh flower specimen embedding
Technical field the present invention relates to a kind of preparation method of fresh flower sample.
Background technology is current, the delicate and charming fragility of existing flower, is difficult to preserve its original color and luster and shape.After original store method is through chemical staining methods, after physical dryness is dewatered completely, carry out normal temperature preservation or resin embedding preservation.Its weak point: production procedure is complicated, and cost is high, and can not retain color and the shape of former flower preferably, petal surface often has impression.
It is simple that summary of the invention the object of this invention is to provide a kind of production procedure, and cost-saving, better can retain color and the shape of former flower, petal surface is without the preparation method of a kind of fresh flower specimen embedding of impression.
The preparation method of fresh flower specimen embedding realizes according to the following steps:
(1) together with flower base of a fruit clip fresh flower;
(2) after by silica gel particle desiccant and slaine, 1-3:1 mixes in mass ratio, for subsequent use.Fresh flower is directly placed on desiccant, then be sprinkling upon uniformly on fresh flower with the silica gel particle desiccant being mixed with slaine, after flower embeds by mixture completely, be placed in the baking oven of 40 DEG C to 70 DEG C, heat 4 to 24 hours, best heating mode, start to be placed in the baking oven of 40 DEG C to 45 DEG C, heat 4 to 20 hours, temperature is increased to 50 DEG C to 70 DEG C, heats 2 to 4 hours, after silica gel particle desiccant becomes blueness, take out dried flower, take off and be attached to silica gel particle desiccant on petal and slaine, be placed in drying basin for subsequent use;
(3) liquid-state epoxy resin is placed in a mold, dried flower is immersed in liquid-state epoxy resin, preferably uses vacuum pump evacuation, remove bubble;
(4) after liquid-state epoxy resin solidifies completely, direct demold.
Compared with prior art, tool has the following advantages in the present invention: production procedure is simple, and cost-saving, better can retain color and the shape of former flower, petal surface is without impression.
Accompanying drawing explanation
Fig. 1 is the fresh flower specimen embedding figure that the existing production and processing mode for using is processed;
Fig. 2 is the fresh flower specimen embedding figure processed for the production and processing mode of this patent.
Embodiment
Embodiment 1
The preparation method of fresh flower specimen embedding realizes according to the following steps:
(1) together with flower base of a fruit clip fresh flower, the diameter 25mm of flower, the thickness 0.5mm of petal;
(2) after by silica gel particle desiccant and sodium chloride, 1:1 mixes in mass ratio, for subsequent use.Fresh flower is directly placed on silica gel particle desiccant, then be sprinkling upon uniformly on fresh flower with the silica gel particle desiccant being mixed with sodium chloride, after flower embeds by mixture completely, be placed in the baking oven of 70 DEG C, heat 4 hours, after silica gel particle desiccant becomes blueness, take out dried flower, take off and be attached to silica gel particle desiccant on petal and sodium chloride, be placed in drying basin for subsequent use;
(3) liquid-state epoxy resin is placed in a mold, dried flower is immersed in liquid-state epoxy resin, use vacuum pump evacuation, remove bubble;
(4) after liquid-state epoxy resin solidifies completely, direct demold.
Embodiment 2
The preparation method of fresh flower specimen embedding realizes according to the following steps:
(1) together with flower base of a fruit clip fresh flower, the diameter 40mm of flower, the thickness 1mm of petal;
(2) after by silica gel particle desiccant and potassium chloride, 2:1 mixes in mass ratio, for subsequent use.Fresh flower is directly placed on silica gel particle desiccant, then be sprinkling upon uniformly on fresh flower with the silica gel particle desiccant being mixed with potassium chloride, after flower embeds by mixture completely, be placed in the baking oven of 60 DEG C, heat 7 hours, after silica gel particle desiccant becomes blueness, take out dried flower, take off and be attached to silica gel particle desiccant on petal and potassium chloride, the local back up being placed on drying at room temperature is placed in drying basin for subsequent use;
(3) liquid-state epoxy resin is placed in a mold, dried flower is immersed in liquid-state epoxy resin, use vacuum pump evacuation, remove bubble;
(4) after liquid-state epoxy resin solidifies completely, direct demold.
Embodiment 3
The preparation method of fresh flower specimen embedding realizes according to the following steps:
(1) together with flower base of a fruit clip fresh flower, the diameter 10cm of flower and the thickness 2.2mm of petal;
(2) after by silica gel particle desiccant and anhydrous sodium bromide, 3:1 mixes in mass ratio, for subsequent use.Fresh flower is directly placed on silica gel particle desiccant, then be sprinkling upon uniformly on fresh flower with the silica gel particle desiccant being mixed with anhydrous sodium bromide, mixture is placed in the baking oven of 40 DEG C, heats 20 hours after being embedded by flower completely, be warming up to 70 DEG C again, heat 2 hours, after silica gel particle desiccant becomes blueness, take out dried flower, take off and be attached to silica gel particle desiccant on petal and anhydrous sodium bromide, be placed in drying basin for subsequent use;
(3) liquid-state epoxy resin is placed in a mold, dried flower is immersed in liquid-state epoxy resin, use vacuum pump evacuation, remove bubble;
(4) after liquid-state epoxy resin solidifies completely, direct demold.
Embodiment 4
The preparation method of fresh flower specimen embedding realizes according to the following steps:
(1) together with flower base of a fruit clip fresh flower, the diameter 10cm of flower and the thickness 2.2mm of petal;
(2) after by silica gel particle desiccant and anhydrous cupric sulfate, 3:1 mixes in mass ratio, for subsequent use.Fresh flower is directly placed on silica gel particle desiccant, then be sprinkling upon uniformly on fresh flower with the silica gel particle desiccant being mixed with anhydrous cupric sulfate, mixture is placed in the baking oven of 45 DEG C, heats 4 hours after being embedded by flower completely, be warming up to 50 DEG C again, heat 20 hours, after silica gel particle desiccant becomes blueness, take out dried flower, take off and be attached to silica gel particle desiccant on petal and anhydrous cupric sulfate, be placed in drying basin for subsequent use;
(3) liquid-state epoxy resin is placed in a mold, dried flower is immersed in liquid-state epoxy resin, use vacuum pump evacuation, remove bubble;
(4) after liquid-state epoxy resin solidifies completely, direct demold.
Embodiment 5
The preparation method of fresh flower specimen embedding realizes according to the following steps:
(1) together with flower base of a fruit clip fresh flower, the diameter 40mm of flower and the thickness 1mm of petal;
(2) after by silica gel particle desiccant and anhydrous calcium chloride, 2:1 mixes in mass ratio, for subsequent use.Fresh flower is directly placed on silica gel particle desiccant, then be sprinkling upon uniformly on fresh flower with the silica gel particle desiccant being mixed with anhydrous calcium chloride, after flower embeds by mixture completely, be placed in the baking oven of 40 DEG C, heat 24 hours, after silica gel particle desiccant becomes blueness, take out dried flower, take off and be attached to silica gel particle desiccant on petal and anhydrous calcium chloride, be placed in drying basin for subsequent use;
(3) liquid-state epoxy resin is placed in a mold, dried flower is immersed in liquid-state epoxy resin, use vacuum pump evacuation, remove bubble;
(4) after liquid-state epoxy resin solidifies completely, direct demold.
Product of the present invention is tested as follows:
(1) experiment content:
The production and processing mode of prior art, after fresh flower is plucked, first to be bleached to flower by chemical dyeing method and dye desired color again, after sizing, through physical dryness (natural seasoning, freeze-day with constant temperature, microwave drying, freeze drying) method removing flower internal moisture, prevent the generation of corruption, finally directly show preservation in atmosphere or persistence after resin embedding.
Use the preparation method of prior art and this patent to make fresh flower specimen embedding respectively respectively, its result is compared.
(2) judgment criteria:
1. production procedure 2. cost 3. retain color and the shape of former flower, petal surface impression.
(3) experimental result:
Production procedure is simple, and cost is low, and better can retain color and the shape of former flower, petal surface is without impression.
(4) type testing example:
A: the production and processing mode of prior art:
1. production procedure: the collection of fresh flower, the dyeing of fresh flower, the drying of fresh flower, the embedding of fresh flower;
2. cost: use microwave drying to be difficult to control the microwave time, the microwave time is inadequate, then flower dehydration is insufficient, corruption easy to change when the later stage preserves; Microwave overlong time, easily cause flower to be out of shape or flower local burned, the wasting phenomenon of raw material fresh flower is very serious, and wastes a large amount of manpowers.Freeze-drying uses vacuum refrigeration case, vacuumized by fresh flower when freezing, and to reach the object of fresh flower dehydration, this equipment cost is higher;
3. color and the shape of former flower is retained, petal surface impression: Figure of description 1 is the fresh flower specimen embedding that the existing production and processing mode used is processed.
B: the production and processing mode of this patent:
1. production procedure: the embedding of the collection of fresh flower, guarantor's look drying of fresh flower, fresh flower;
2. cost: slaine is nontoxic, reusable, save material cost;
3. retain color and the shape of former flower, petal surface is almost without impression: Figure of description 2 is the fresh flower specimen embedding using the production and processing mode of this patent to process.

Claims (3)

1. a preparation method for fresh flower specimen embedding, is characterized in that:
(1) together with flower base of a fruit clip fresh flower;
(2) after by silica gel particle desiccant and slaine, 1-3:1 mixes in mass ratio, for subsequent use, fresh flower is directly placed on desiccant, is then sprinkling upon uniformly on fresh flower with the silica gel particle desiccant being mixed with slaine, after flower embeds by mixture completely, be placed in the baking oven of 40 DEG C to 70 DEG C, heat 4 to 24 hours, after silica gel particle desiccant becomes blueness, take out dried flower, take off and be attached to silica gel particle desiccant on petal and slaine, be placed in drying basin for subsequent use;
(3) liquid-state epoxy resin is placed in a mold, dried flower is immersed in liquid-state epoxy resin;
(4) after liquid-state epoxy resin solidifies completely, direct demold.
2. the preparation method of fresh flower specimen embedding according to claim 1, is characterized in that: after in step 2, flower embeds by mixture completely, be placed in the baking oven of 40 DEG C to 45 DEG C, heat 4 to 20 hours, temperature is increased to 50 DEG C to 70 DEG C, heats 2 to 4 hours.
3. the preparation method of fresh flower specimen embedding according to claim 1, is characterized in that: immerse in liquid-state epoxy resin by dried flower in step 3, use vacuum pump evacuation, remove bubble.
CN201410513678.XA 2014-09-29 2014-09-29 Method for making fresh flower embedded specimen Pending CN104304240A (en)

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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105109263A (en) * 2015-07-08 2015-12-02 南宁千年工艺有限公司 Flower ambroid accessory manufacturing method
CN105900977A (en) * 2016-04-29 2016-08-31 青岛农业大学 Manufacturing method of plant resin specimen for teaching
CN106218300A (en) * 2016-08-30 2016-12-14 张丽莉 A kind of manufacture method of crystal flower
CN107183002A (en) * 2017-05-10 2017-09-22 广西柳州中嘉知识产权服务有限公司 Butterfly specimen preparation method
CN107727479A (en) * 2017-09-30 2018-02-23 福建中医药大学 A kind of method that cast moulds embedding preserves
CN108077246A (en) * 2017-12-25 2018-05-29 重庆尔麟农业开发有限公司 A kind of production method of flower specimen
CN108902134A (en) * 2018-07-04 2018-11-30 武夏夏 A kind of production method of medicinal plant epoxy resin permant preparation
CN110178837A (en) * 2019-06-11 2019-08-30 滁州学院 A kind of manufacture craft of chu chrysanthemum sample
CN110447638A (en) * 2019-08-23 2019-11-15 湖南省林业科学院 A kind of Slide processing of transparent embedding production camellia
CN110637811A (en) * 2019-08-23 2020-01-03 湖南省林业科学院 Method for preparing transparent embedded oil-tea camellia fruit specimen
CN110884284A (en) * 2019-11-29 2020-03-17 内蒙古蒙草生态环境(集团)股份有限公司 Method for making three-dimensional dried trollius chinensis flowers
CN110884285A (en) * 2019-11-29 2020-03-17 内蒙古蒙草生态环境(集团)股份有限公司 Making method of three-dimensional dried red lily flower
CN110915798A (en) * 2019-11-29 2020-03-27 内蒙古蒙草生态环境(集团)股份有限公司 Plant specimen embedding agent and application thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0311001A (en) * 1989-06-05 1991-01-18 Daikure:Kk Drying and drying device
CN101925298A (en) * 2008-04-01 2010-12-22 三得利控股株式会社 Method of producing color-unchangeable dry flowers from easily color-changeable flowers
CN103882488A (en) * 2014-03-15 2014-06-25 沈阳师范大学 Natural plant electroplating and finishing technique

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0311001A (en) * 1989-06-05 1991-01-18 Daikure:Kk Drying and drying device
CN101925298A (en) * 2008-04-01 2010-12-22 三得利控股株式会社 Method of producing color-unchangeable dry flowers from easily color-changeable flowers
CN103882488A (en) * 2014-03-15 2014-06-25 沈阳师范大学 Natural plant electroplating and finishing technique

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
李海泉 等: "红色花标本保存技术研究", 《中国现代中药》 *
葛皓: "干燥花制作方法综述", 《海南师范学院学报》 *

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105109263A (en) * 2015-07-08 2015-12-02 南宁千年工艺有限公司 Flower ambroid accessory manufacturing method
CN105900977A (en) * 2016-04-29 2016-08-31 青岛农业大学 Manufacturing method of plant resin specimen for teaching
CN106218300A (en) * 2016-08-30 2016-12-14 张丽莉 A kind of manufacture method of crystal flower
CN107183002A (en) * 2017-05-10 2017-09-22 广西柳州中嘉知识产权服务有限公司 Butterfly specimen preparation method
CN107727479A (en) * 2017-09-30 2018-02-23 福建中医药大学 A kind of method that cast moulds embedding preserves
CN108077246A (en) * 2017-12-25 2018-05-29 重庆尔麟农业开发有限公司 A kind of production method of flower specimen
CN108902134A (en) * 2018-07-04 2018-11-30 武夏夏 A kind of production method of medicinal plant epoxy resin permant preparation
CN110178837A (en) * 2019-06-11 2019-08-30 滁州学院 A kind of manufacture craft of chu chrysanthemum sample
CN110447638A (en) * 2019-08-23 2019-11-15 湖南省林业科学院 A kind of Slide processing of transparent embedding production camellia
CN110637811A (en) * 2019-08-23 2020-01-03 湖南省林业科学院 Method for preparing transparent embedded oil-tea camellia fruit specimen
CN110884284A (en) * 2019-11-29 2020-03-17 内蒙古蒙草生态环境(集团)股份有限公司 Method for making three-dimensional dried trollius chinensis flowers
CN110884285A (en) * 2019-11-29 2020-03-17 内蒙古蒙草生态环境(集团)股份有限公司 Making method of three-dimensional dried red lily flower
CN110915798A (en) * 2019-11-29 2020-03-27 内蒙古蒙草生态环境(集团)股份有限公司 Plant specimen embedding agent and application thereof

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Application publication date: 20150128