CN104278426A - Manufacturing method of anti-microbial functional refinement jute fiber printing blanket - Google Patents
Manufacturing method of anti-microbial functional refinement jute fiber printing blanket Download PDFInfo
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- CN104278426A CN104278426A CN201410513515.1A CN201410513515A CN104278426A CN 104278426 A CN104278426 A CN 104278426A CN 201410513515 A CN201410513515 A CN 201410513515A CN 104278426 A CN104278426 A CN 104278426A
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Abstract
The invention provides a manufacturing method of an anti-microbial functional refinement jute fiber printing blanket. The manufacturing method is characterized by including steps of fabricating; polishing; shaping; processing before printing; printing and self-cleaning; steaming and fixing color; washing; drying; polishing and cutting a base blanket; finishing and packaging. The manufacturing method is high in antimicrobial rate, good in color fastness and excellent in mechanical property.
Description
Technical field
The present invention relates to the preparation method of refining jute fiber antiseptic printing woollen blanket, belong to textile material technical field.
Background technology
Tossa is the second largest native cellulose fibre being only second to cotton fiber, whole world total amount about 4,000,000 tons, aboundresources, characteristic are outstanding, and require low to growth conditions, ground is not striven with grain and cotton, without the need to fertilising, spray medicine in growth course, environmentally safe is the extremely potential novel ecological textile raw material of one.Common tossa is thick and stiff, dyeability is poor, product has prodding and itching feeling, after process of refinement, fibre fineness and pliability significantly improve, and maintain the original natural antibacterial of fiber and excellent moisture adsorption and releasing function, be expected to be applied to exploitation comfortableness functionalization printing woollen blanket.
Summary of the invention
The object of this invention is to provide the preparation method of refining jute fiber antiseptic printing woollen blanket, make refining jute fiber can be used in preparing new type functional printing woollen blanket.
In order to achieve the above object, invention provides a kind of preparation method of refining jute fiber antiseptic printing woollen blanket, it is characterized in that, concrete steps comprise:
The first step: weave: the blended yarn employing of refining jute fiber and cotton fiber is woven into woollen blanket through braiding technology for making, and weaving tension is 5 ~ 10g, and workshop temperature is 20 ± 2 DEG C, and humidity is 65 ± 3%;
Second step: hot light: the woollen blanket be woven into is carried out hot light, hot light temperature is 170 ~ 190 DEG C, and cloth rewinder roll speed is 6 ~ 10m/min;
3rd step: sizing: shaped by the woollen blanket after hot light, setting temperature is 110 ~ 130 DEG C, and cloth rewinder roll speed is 12 ~ 15m/min;
4th step: stamp pre-treatment: use the woollen blanket after pretreatment liquid process sizing, described pretreatment liquid contains NaOH and modifier, modifier concentration is 35 ~ 45g/L, the concentration of NaOH is 7 ~ 10g/L; bath raio is 1: 6 ~ 1: 8; treatment temperature is 55 ~ 65 DEG C, and the processing time is 40 ~ 50min;
5th step: stamp and self-cleaning finishing: use slurry to carry out stamp on the woollen blanket after pre-treatment, printing temperature is 70 ~ 80 DEG C, containing dyestuff in described slurry, modified nano-titanium dioxide, emulsion thickening, softener, shrink-resistant agent, sodium carbonate and dyeing assistant, self-cleaning finishing can be carried out to woollen blanket while stamp, wherein dye strength is 2.4 ~ 2.6%, modified nano-titanium dioxide concentration is 0.5 ~ 0.7%, emulsion thickening concentration is 550 ~ 650g/L, softer consistency is 14 ~ 16g/L, shiinkproof finish agent concentration is 18 ~ 22g/L, concentration of sodium carbonate is 1.5 ~ 2.5g/L, dyeing assistant concentration is 8 ~ 12g/L,
6th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, steam temperature is 140 ~ 160 DEG C, and steaming time is 70 ~ 85min;
7th step: washing: adopted by the woollen blanket after vapour steaming colour fixing 3 groove washing process to wash, 1st rinsing bowl temperature is 40 DEG C ~ 50 DEG C, 2nd rinsing bowl temperature is 50 DEG C ~ 60 DEG C, 3rd rinsing bowl temperature is 40 DEG C ~ 50 DEG C, and composite soft finishing agent is added in the 2nd rinsing bowl, described composite soft finishing agent comprises softener and smooth agent, and in the 2nd rinsing bowl, the concentration of softener is 10 ~ 15g/L, and the concentration of smooth agent is 15 ~ 20g/L;
8th step: dry: temperature is 90 ~ 100 DEG C, and cloth rewinder roll speed is 5 ~ 10m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying is carried out hot light and scald cutting, and hot light temperature is 140 ~ 160 DEG C, scalds that to cut temperature be 130 ~ 150 DEG C, and cloth rewinder roll speed is all 6 ~ 10m/min;
Tenth step: arrange packing.
Preferably, described refining jute fiber and the blended yarn of cotton fiber are cotton 70 blended yarns of jute 30/.
Preferably, the modifier in the 4th described step is polyepichlorohydrin amine compound.
Preferably, the dyestuff of the 5th described step is Remazol RGB Red.
Preferably, the emulsion thickening of the 5th described step is emulsion thickening EL-80.
Preferably, the softener of the 5th described step is softener Hans LSE.
Preferably, the shrink-resistant agent of the 5th described step is shrink-resistant agent BF-588.
Preferably, the dyeing assistant of the 5th described step is alkyl sulfate salt.
Preferably, the softener in the 7th described step is Goon1201.
Preferably, the smooth agent in the 7th described step is two amido functional group organic silicon emulsions.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention adopts the blended yarn of refining jute fiber and cotton fiber, high according to refining jute fiber degree of crystallinity, initial modulus is high and the feature that jhouta blended yarn intensity is lower, suitable reduction weaving tension, improve hot light temperature, carry out cation-modified to grey cloth, improve the coloring of grey cloth, configuration concentrator can realize stamp under lower temperature conditions, strengthening gas is adopted to steam technique, adopt 3 groove washing process, and composite soft finishing agent is added in the 2nd rinsing bowl, to ensure the sense of touch comfortableness of matte, exploitation has natural antibacterial, the printing woollen blanket of excellent comfortableness, woollen blanket bacteriostasis rate obtained by the present invention is high, COLOR FASTNESS is good, mechanical property is good, the successful exploitation of this product and applying, improve the use proportion of tossa in grade textiles, make full use of resource, realize the diversification of textile product raw material, enhance our international competitiveness, good impetus is played in sustainable development for textile industry.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
A preparation method for refining jute fiber antiseptic printing woollen blanket, concrete steps are:
The first step: weave: blended yarn (cotton 70 blended yarns of the refinement jhouta 30/) employing of refining jute fiber and cotton fiber is woven into woollen blanket through braiding technology for making, and weaving tension is 6g, and workshop temperature is 20 ± 2 DEG C, and humidity is 65 ± 3%;
Second step: hot light: the woollen blanket be woven into is carried out hot light, hot light temperature is 180 DEG C, and cloth rewinder roll speed is 8m/min;
3rd step: sizing: shaped by the woollen blanket after hot light, setting temperature is 120 DEG C, and cloth rewinder roll speed is 15m/min;
4th step: stamp pre-treatment: use the woollen blanket after pretreatment liquid process sizing, described pretreatment liquid is made up of NaOH, modifier and water, and modifier concentration is 40g/L, naoh concentration is 8g/L; bath raio is 1: 6, and treatment temperature is 60 DEG C, and the processing time is 45min; Described modifier is polyepichlorohydrin amine compound, is produced by Shanghai Fang Ye Chemical Co., Ltd..
5th step: stamp and self-cleaning finishing: use slurry to carry out stamp on the woollen blanket after pre-treatment, printing temperature is 70 DEG C, described slurry is by dyestuff, modified nano-titanium dioxide, emulsion thickening, softener, shrink-resistant agent, sodium carbonate, dyeing assistant and water composition, self-cleaning finishing can be carried out to woollen blanket while stamp, wherein dye strength is 2.5%, modified nano-titanium dioxide concentration is 0.6%, emulsion thickening concentration is 600g/L, softer consistency is 15g/L, shiinkproof finish agent concentration is 20g/L, concentration of sodium carbonate is 2g/L, dyeing assistant concentration is 10g/L, described dyestuff is Remazol RGB Red, De Sida company produces, modified nano-titanium dioxide is produced by Haitai Nano Material Co., Ltd., Nanjing, model is HTTi03-F, average grain diameter is 20nm, emulsion thickening is produced by Fine Chemical Works federal in Guangdong, model is EL-80, softener is by Changzhou Mei Sheng biomaterial Co., Ltd, and model is Hans LSE, shrink-resistant agent by Dongyang City make the country prosperous Chemical Co., Ltd. produce, model is BF-588, dyeing assistant composition is alkyl sulfate salt, and pacify Kodak Chemical Co., Ltd. by Xiamen and produce, model is AKD.
6th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, steam temperature is 150 DEG C, and steaming time is 75min;
7th step: washing: adopted by the woollen blanket after vapour steaming colour fixing 3 groove washing process to wash, 1st rinsing bowl temperature is 45 DEG C, 2nd rinsing bowl temperature is 55 DEG C, 3rd rinsing bowl temperature is 45 DEG C, and composite soft finishing agent is added in the 2nd rinsing bowl, be water in the 1st described rinsing bowl and the 3rd rinsing bowl, rinsing solution in the 2nd described rinsing bowl is that water adds composite soft finishing agent and obtains, described composite soft finishing agent is made up of softener and smooth agent, in 2nd rinsing bowl, the concentration of softener is 12g/L, and the concentration of smooth agent is 18g/L; Described softener is produced by Dongguan Jiahong Silicone Technology Co., Ltd., and model is Goon1201, and smooth agent is two amido functional group organic silicon emulsions, is produced by upper Haikang Pei Er Industrial Co., Ltd..
8th step: dry: temperature is 90 DEG C, and cloth rewinder roll speed is 5m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying is carried out hot light and scald cutting, and hot light temperature is 150 DEG C, scalds that to cut temperature be 140 DEG C, and cloth rewinder roll speed is all 8m/min;
Tenth step: arrange packing.
The performance test of the refining jute fiber antiseptic printing woollen blanket of gained is as follows:
Ultimate strength (GB/T3923.1-1997): 202N;
Colour fastness to rubbing (GB/T 3920-1997): resistance to dry, wet friction COLOR FASTNESS is 4-5 level;
Colour fasteness to sunlight (GB/T 8427-1998): 4-5 level;
Water-fastness COLOR FASTNESS (GB/T 12490-1990): 4-5 level;
Bacteriostasis rate (FZ/T 73023-2006, GB/T 20944.3-2008): 98%.
Embodiment 2
A preparation method for refining jute fiber antiseptic printing woollen blanket, concrete steps are:
The first step: weave: blended yarn (cotton 70 blended yarns of the jute 30/) employing of refining jute fiber and cotton fiber is woven into woollen blanket through braiding technology for making, and weaving tension is 8g, and workshop temperature is 20 ± 2 DEG C, and humidity is 65 ± 3%;
Second step: hot light: the woollen blanket be woven into is carried out hot light, hot light temperature is 170 DEG C, and cloth rewinder roll speed is 10m/min;
3rd step: sizing: shaped by the woollen blanket after hot light, setting temperature is 110 DEG C, and cloth rewinder roll speed is 12m/min;
4th step: stamp pre-treatment: use the woollen blanket after pretreatment liquid process sizing, described pretreatment liquid is made up of NaOH, modifier and water, and modifier concentration is 45g/L, naoh concentration is 9g/L; bath raio is 1: 6, and treatment temperature is 55 DEG C, and the processing time is 50min; Described modifier is polyepichlorohydrin amine compound, is produced by Shanghai Fang Ye Chemical Co., Ltd..
5th step: stamp and self-cleaning finishing: use slurry to carry out stamp on the woollen blanket after pre-treatment, printing temperature is 80 DEG C, described slurry is by dyestuff, modified nano-titanium dioxide, emulsion thickening, softener, shrink-resistant agent, sodium carbonate, dyeing assistant and water composition, self-cleaning finishing can be carried out to woollen blanket while stamp, wherein dye strength is 2.4%, modified nano-titanium dioxide concentration is 0.5%, emulsion thickening concentration is 580g/L, softer consistency is 16g/L, shiinkproof finish agent concentration is 22g/L, concentration of sodium carbonate is 2g/L, dyeing assistant concentration is 10g/L, described dyestuff is Remazol RGB Red, De Sida company produces, modified nano-titanium dioxide is produced by Haitai Nano Material Co., Ltd., Nanjing, model is HTTi03-F, average grain diameter is 20nm, emulsion thickening is produced by Fine Chemical Works federal in Guangdong, model is EL-80, softener is by Changzhou Mei Sheng biomaterial Co., Ltd, and model is Hans LSE, shrink-resistant agent by Dongyang City make the country prosperous Chemical Co., Ltd. produce, model is BF-588, dyeing assistant composition is alkyl sulfate salt, and pacify Kodak Chemical Co., Ltd. by Xiamen and produce, model is AKD.
6th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, steam temperature is 140 DEG C, and steaming time is 85min;
7th step: washing: adopted by the woollen blanket after vapour steaming colour fixing 3 groove washing process to wash, 1st rinsing bowl temperature is 45 DEG C, 2nd rinsing bowl temperature is 55 DEG C, 3rd rinsing bowl temperature is 45 DEG C, be water in the 1st described rinsing bowl and the 3rd rinsing bowl, rinsing solution in the 2nd described rinsing bowl is that water adds composite soft finishing agent and obtains, described composite soft finishing agent is made up of softener and smooth agent, described composite soft finishing agent is made up of softener and smooth agent, in 2nd rinsing bowl, the concentration of softener is 12g/L, and the concentration of smooth agent is 18g/L; Described softener is produced by Dongguan Jiahong Silicone Technology Co., Ltd., and model is Goon1201, and smooth agent is two amido functional group organic silicon emulsions, is produced by upper Haikang Pei Er Industrial Co., Ltd..
8th step: dry: temperature is 90 DEG C, and cloth rewinder roll speed is 5m/min;
9th step: flower base scalds to be cut: hot light temperature is 150 DEG C, scalds that to cut temperature be 140 DEG C, and cloth rewinder roll speed is 8m/min;
Tenth step: arrange packing.
The performance test of the refining jute fiber antiseptic printing woollen blanket of embodiment 2 is as follows:
Ultimate strength (GB/T3923.1-1997): 215N;
Colour fastness to rubbing (GB/T 3920-1997): resistance to dry, wet friction COLOR FASTNESS is 4-5 level;
Colour fasteness to sunlight (GB/T 8427-1998): 4-5 level;
Water-fastness COLOR FASTNESS (GB/T 12490-1990): 4-5 level; Bacteriostasis rate (FZ/T 73023-2006, GB/T20944.3-2008): 98%
Above-mentioned adopted formula of size, functional treatment agents useful for same formula, composite soft finish agent prescription, working process parameter etc. are only preferred embodiment of the present invention, are not used for limiting practical range of the present invention.Namely all equivalences done according to the content of the present patent application the scope of the claims change and modify, and all should be technology category of the present invention.
Claims (10)
1. a preparation method for refining jute fiber antiseptic printing woollen blanket, is characterized in that, concrete steps comprise:
The first step: weave: the blended yarn employing of refining jute fiber and cotton fiber is woven into woollen blanket through braiding technology for making, and weaving tension is 5 ~ 10g, and workshop temperature is 20 ± 2 DEG C, and humidity is 65 ± 3%;
Second step: hot light: the woollen blanket be woven into is carried out hot light, hot light temperature is 170 ~ 190 DEG C, and cloth rewinder roll speed is 6 ~ 10m/min
3rd step: sizing: shaped by the woollen blanket after hot light, setting temperature is 110 ~ 130 DEG C, and cloth rewinder roll speed is 12 ~ 15m/min;
4th step: stamp pre-treatment: use the woollen blanket after pretreatment liquid process sizing, described pretreatment liquid contains NaOH and modifier, modifier concentration is 35 ~ 45g/L, the concentration of NaOH is 7 ~ 10g/L; bath raio is 1: 6 ~ 1: 8; treatment temperature is 55 ~ 65 DEG C, and the processing time is 40 ~ 50min;
5th step: stamp and self-cleaning finishing: use slurry to carry out stamp on the woollen blanket after pre-treatment, printing temperature is 70 ~ 80 DEG C, containing dyestuff in described slurry, modified nano-titanium dioxide, emulsion thickening, softener, shrink-resistant agent, sodium carbonate and dyeing assistant, self-cleaning finishing can be carried out to woollen blanket while stamp, wherein dye strength is 2.4 ~ 2.6%, modified nano-titanium dioxide concentration is 0.5 ~ 0.7%, emulsion thickening concentration is 550 ~ 650g/L, softer consistency is 14 ~ 16g/L, shiinkproof finish agent concentration is 18 ~ 22g/L, concentration of sodium carbonate is 1.5 ~ 2.5g/L, dyeing assistant concentration is 8 ~ 12g/L,
6th step: vapour steaming colour fixing: the woollen blanket after stamp is carried out vapour steaming colour fixing, steam temperature is 140 ~ 160 DEG C, and steaming time is 70 ~ 85min;
7th step: washing: adopted by the woollen blanket after vapour steaming colour fixing 3 groove washing process to wash, 1st rinsing bowl temperature is 40 DEG C ~ 50 DEG C, 2nd rinsing bowl temperature is 50 DEG C ~ 60 DEG C, 3rd rinsing bowl temperature is 40 DEG C ~ 50 DEG C, and composite soft finishing agent is added in the 2nd rinsing bowl, described composite soft finishing agent comprises softener and smooth agent, and in the 2nd rinsing bowl, the concentration of softener is 10 ~ 15g/L, and the concentration of smooth agent is 15 ~ 20g/L;
8th step: dry: temperature is 90 ~ 100 DEG C, and cloth rewinder roll speed is 5 ~ 10m/min;
9th step: flower base scalds to be cut: the woollen blanket after drying is carried out hot light and scald cutting, and hot light temperature is 140 ~ 160 DEG C, scalds that to cut temperature be 130 ~ 150 DEG C, and cloth rewinder roll speed is all 6 ~ 10m/min;
Tenth step: arrange packing.
2. the preparation method of refining jute fiber antiseptic printing woollen blanket as claimed in claim 1, it is characterized in that, described refining jute fiber and the blended yarn of cotton fiber are cotton 70 blended yarns of jute 30/.
3. the preparation method of refining jute fiber antiseptic printing woollen blanket as claimed in claim 1, it is characterized in that, the modifier in the 4th described step is polyepichlorohydrin amine compound.
4. the preparation method of refining jute fiber antiseptic printing woollen blanket as claimed in claim 1, it is characterized in that, the dyestuff of the 5th described step is Remazol RGB Red.
5. the preparation method of refining jute fiber antiseptic printing woollen blanket as claimed in claim 1, it is characterized in that, the emulsion thickening of the 5th described step is emulsion thickening EL-80.
6. the preparation method of refining jute fiber antiseptic printing woollen blanket as claimed in claim 1, it is characterized in that, the softener of the 5th described step is softener Hans LSE.
7. the preparation method of refining jute fiber antiseptic printing woollen blanket as claimed in claim 1, it is characterized in that, the shrink-resistant agent of the 5th described step is shrink-resistant agent BF-588.
8. the preparation method of refining jute fiber antiseptic printing woollen blanket as claimed in claim 1, it is characterized in that, the dyeing assistant of the 5th described step is alkyl sulfate salt.
9. the preparation method of refining jute fiber antiseptic printing woollen blanket as claimed in claim 1, it is characterized in that, the softener in the 7th described step is Goon1201.
10. the preparation method of refining jute fiber antiseptic printing woollen blanket as claimed in claim 1, is characterized in that, the smooth agent in the 7th described step is two amido functional group organic silicon emulsions.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105063946A (en) * | 2015-08-27 | 2015-11-18 | 宿迁市神龙家纺有限公司 | Economical dyeing method through heating drying and ironing |
| CN109023997A (en) * | 2018-09-14 | 2018-12-18 | 桐乡市濮院毛针织技术服务中心 | A kind of yarn-dyed color method of cotton ramie blended spinning |
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| CN109023997A (en) * | 2018-09-14 | 2018-12-18 | 桐乡市濮院毛针织技术服务中心 | A kind of yarn-dyed color method of cotton ramie blended spinning |
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| CN104278426B (en) | 2016-07-13 |
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Granted publication date: 20160713 Termination date: 20180929 |