CN104263499A - Fast pandalus borealis shrimp sauce extraction method - Google Patents
Fast pandalus borealis shrimp sauce extraction method Download PDFInfo
- Publication number
- CN104263499A CN104263499A CN201410547705.5A CN201410547705A CN104263499A CN 104263499 A CN104263499 A CN 104263499A CN 201410547705 A CN201410547705 A CN 201410547705A CN 104263499 A CN104263499 A CN 104263499A
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- Prior art keywords
- shrimp
- arctic
- sweet
- sauce
- extracting method
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
Abstract
The invention discloses a fast pandalus borealis shrimp sauce extraction method. The method is simple to operate, is particularly suitable for operating and processing the pandalus borealis on a fishing boat, and comprises the following steps: the freshly fished pandalus borealis is heated and sterilized, drained off and homogenized, certain volume of n-hexane is added, extraction is performed for a period, an extract liquor is subjected to rotary evaporation to obtain the pandalus borealis shrimp sauce. The method is mild in extraction condition and simple and fast to operate, n-hexane can be recycled, the phospholipid content in the extracted shrimp sauce is 30%-40%, and the nutritional value is high.
Description
Technical field
The present invention relates to the extracting method of the sweet shrimp shrimp sauce in a kind of arctic, utilize the method for the sweet shrimp shrimp sauce in the organic solvent rapid extraction arctic specifically.
Background technology
The sweet shrimp in the arctic (Pandalus borealis), mainly originates from the surrounding waters, the arctic such as the North Atlantic and marine site, the Arctic Ocean.The estimated value of its stock on hand is about 3 ~ 1,300,000,000 tons, every year can nearly 100,000,000 tons of quantity of the catch.Sweet shrimp is comprehensively nutritious in the arctic, and in new fresh and sweet shrimp, moisture is about 65-75%, and crude protein is about 7-12%, and crude fat is about 7-15%, carbohydrate about 2%, ash content about 3%, vitamin A, B, E, and the much the same trace element also containing needed by human body.
The arctic sweet shrimp shrimp sauce has high nutritive value and medical value.Correlative study finds, and sweet shrimp shrimp sauce lipid acid composition in the arctic is rich and varied, and proportion shared by unsaturated fatty acid content is very large, polyunsaturated fatty acid EPA and DHA content high.There is reduction cholesterol, adjusting blood lipid, prevention senile dementia, prevention of arterial sclerosis, anti-inflammatory, prevention visual deterioration and improve the different physiological roles such as brain learning function.But the domestic research for the sweet shrimp shrimp sauce in the arctic is also in a primary stage at present.Method provided by the invention can realize the rapid extraction of the sweet shrimp shrimp sauce in the arctic, and working method is simple simultaneously, mild condition.The difficult problems such as the effective solution arctic sweet shrimp shrimp sauce extraction time length, complicated operation, directly can carry out shrimp sauce extraction fishing for ship.
Summary of the invention
The invention discloses a kind of method utilizing organic solvent rapid extraction shrimp sauce from the sweet shrimp in the arctic.The advantage utilizing method of the present invention to extract shrimp sauce is that extraction conditions is gentle, fast simple to operation, and normal hexane recoverable extracts phospholipids content in shrimp sauce high, is of high nutritive value.
The present invention for solving the problems of the technologies described above adopted technical scheme is:
Sweet for the arctic after fresh fishing for shrimp 75-115 DEG C poach or steam heating or microwave heating or pressurized, heated 3-20min are reached the object of sterilization enzyme inactivation.After being drained away the water by the sweet shrimp in the arctic after heating, it is rotten that refiner homogenate 1-15min obtains the sweet shrimp shrimp in the arctic.Normal hexane 15-30 DEG C that adds 2-10 times of volume in the sweet shrimp shrimp gruel of the arctic extracts 2 times, and each time 30-120min, period 5-10min hybrid extraction liquid once.Merge 2 extraction liquids, under 30-70 DEG C of condition, reduce pressure rotary evaporation to constant weight, obtain the sweet shrimp shrimp sauce in the arctic.The normal hexane collecting rotary evaporation gained can be reused for the sweet shrimp shrimp sauce in the arctic and extract.
The invention provides a kind of method utilizing organic solvent rapid extraction from the sweet shrimp in the arctic, utilize normal hexane for extraction solvent, the nutritive ingredient such as phosphatide, unsaturated fatty acids, astaxanthin in the gruel of sweet for arctic shrimp shrimp is extracted, be separated with shrimp sauce after decompression rotary evaporation, the normal hexane obtained after rotary evaporation can continue on for the extraction of shrimp sauce, greatly reduces shrimp sauce extraction cost.
Embodiment
Below in conjunction with specific embodiment, the invention will be further described, to help understanding content of the present invention.
embodiment 1
By sweet for the arctic after fresh fishing for shrimp 85 DEG C heating 20min sterilization enzyme inactivation.After being drained away the water by the sweet shrimp in the arctic after heating, it is rotten that refiner homogenate 5min obtains the sweet shrimp shrimp in the arctic.The normal hexane 25 DEG C adding 5 times of volumes in the sweet shrimp shrimp gruel of the arctic extracts 2 times, and each time 40min, period 5-10min hybrid extraction liquid once.Merge 2 extraction liquids, under 30-70 DEG C of condition, reduce pressure rotary evaporation to constant weight, obtain the sweet shrimp shrimp sauce in the arctic.The normal hexane collecting rotary evaporation gained can be reused for the sweet shrimp shrimp sauce in the arctic and extract.
embodiment 2
By sweet for the arctic after fresh fishing for shrimp 90 DEG C, 500-900W microwave heating 10min sterilization enzyme inactivation.After being drained away the water by the sweet shrimp in the arctic after heating, it is rotten that refiner homogenate 10min obtains the sweet shrimp shrimp in the arctic.The normal hexane 30 DEG C adding 2 times of volumes in the sweet shrimp shrimp gruel of the arctic extracts 2 times, and each time 120min, period 5-10min hybrid extraction liquid once.Merge 2 extraction liquids, under 30-70 DEG C of condition, reduce pressure rotary evaporation to constant weight, obtain the sweet shrimp shrimp sauce in the arctic.The normal hexane collecting rotary evaporation gained can be reused for the sweet shrimp shrimp sauce in the arctic and extract.
embodiment 3
By sweet for the arctic after fresh fishing for shrimp 115 DEG C of steam heating 10min sterilization enzyme inactivations.After being drained away the water by the sweet shrimp in the arctic after heating, it is rotten that refiner homogenate 2min obtains the sweet shrimp shrimp in the arctic.The normal hexane 20 DEG C adding 10 times of volumes in the sweet shrimp shrimp gruel of the arctic extracts 2 times, and each time 30min, period 5-10min hybrid extraction liquid once.Merge 2 extraction liquids, under 30-70 DEG C of condition, reduce pressure rotary evaporation to constant weight, obtain the sweet shrimp shrimp sauce in the arctic.The normal hexane collecting rotary evaporation gained can be reused for the sweet shrimp shrimp sauce in the arctic and extract.
embodiment 4
By sweet for the arctic after fresh fishing for shrimp 75 DEG C, pressurized, heated 3min sterilization enzyme inactivation under 35kpa-80kpa condition.After being drained away the water by the sweet shrimp in the arctic after heating, it is rotten that refiner homogenate 1min obtains the sweet shrimp shrimp in the arctic.The normal hexane 30 DEG C adding 8 times of volumes in the sweet shrimp shrimp gruel of the arctic extracts 2 times, and each time 60min, period 5-10min hybrid extraction liquid once.Merge 2 extraction liquids, under 30-70 DEG C of condition, reduce pressure rotary evaporation to constant weight, obtain the sweet shrimp shrimp sauce in the arctic.The normal hexane collecting rotary evaporation gained can be reused for the sweet shrimp shrimp sauce in the arctic and extract.
embodiment 5
By sweet for the arctic after fresh fishing for shrimp 100 DEG C of poach or steam heating or microwave heating or pressurized, heated 5min sterilization enzyme inactivation.After being drained away the water by the sweet shrimp in the arctic after heating, it is rotten that refiner homogenate 20min obtains the sweet shrimp shrimp in the arctic.The normal hexane 15 DEG C adding 3 times of volumes in the sweet shrimp shrimp gruel of the arctic extracts 2 times, and each time 90min, period 5-10min hybrid extraction liquid once.Merge 2 extraction liquids, under 30-70 DEG C of condition, reduce pressure rotary evaporation to constant weight, obtain the sweet shrimp shrimp sauce in the arctic.The normal hexane collecting rotary evaporation gained can be reused for the sweet shrimp shrimp sauce in the arctic and extract.
embodiment 6
By sweet for the arctic after fresh fishing for shrimp 95 DEG C of poach or steam heating or microwave heating or pressurized, heated 8min sterilization enzyme inactivation.After being drained away the water by the sweet shrimp in the arctic after heating, it is rotten that refiner homogenate 5min obtains the sweet shrimp shrimp in the arctic.The normal hexane 25 DEG C adding 6 times of volumes in the sweet shrimp shrimp gruel of the arctic extracts 2 times, and each time 80min, period 5-10min hybrid extraction liquid once.Merge 2 extraction liquids, under 30-70 DEG C of condition, reduce pressure rotary evaporation to constant weight, obtain the sweet shrimp shrimp sauce in the arctic.The normal hexane collecting rotary evaporation gained can be reused for the sweet shrimp shrimp sauce in the arctic and extract.
Claims (7)
1. the sweet shrimp shrimp sauce in an arctic rapid extracting method, is characterized in that carrying out according to following processing step:
(1) heat: go out sweet for the arctic after fresh fishing for shrimp heat sterilization enzyme;
(2) homogenate: after the sweet shrimp in the arctic after heating is drained away the water, it is rotten that refiner homogenate obtains the sweet shrimp shrimp in the arctic;
(3) extract: the n-hexane extraction 2 times adding certain volume in the sweet shrimp shrimp gruel of the arctic, each time 30-120min, period 5-10min hybrid extraction liquid once;
(4) evaporate: merge twice extraction liquid, under 30-70 DEG C of condition, reduce pressure rotary evaporation to constant weight.
2. the sweet shrimp shrimp sauce rapid extracting method of the arctic as described in claim 1, is characterized in that, is poach or steam heating or microwave heating or pressurized, heated to the sweet shrimp type of heating in the arctic.
3. the sweet shrimp shrimp sauce rapid extracting method of the arctic as described in claim 1, is characterized in that, is 75-115 DEG C to the sweet shrimp Heating temperature in the arctic.
4. the sweet shrimp shrimp sauce rapid extracting method of the arctic as described in claim 1, is characterized in that, is 3-20min to the sweet shrimp in arctic heat-up time.
5. the arctic as claimed in claim 1 sweet shrimp shrimp sauce rapid extracting method, it is characterized in that, the sweet shrimp Homogenization time in the arctic is 1-15min.
6. the arctic as claimed in claim 1 sweet shrimp shrimp sauce rapid extracting method, is characterized in that, during extraction, shrimp is rotten is 1:2-1:10 with the solid-liquid ratio of normal hexane.
7. the arctic as claimed in claim 1 sweet shrimp shrimp sauce rapid extracting method, is characterized in that, extraction temperature 15-30 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410547705.5A CN104263499A (en) | 2014-10-16 | 2014-10-16 | Fast pandalus borealis shrimp sauce extraction method |
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| CN201410547705.5A CN104263499A (en) | 2014-10-16 | 2014-10-16 | Fast pandalus borealis shrimp sauce extraction method |
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| CN104263499A true CN104263499A (en) | 2015-01-07 |
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| CN201410547705.5A Pending CN104263499A (en) | 2014-10-16 | 2014-10-16 | Fast pandalus borealis shrimp sauce extraction method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105670779A (en) * | 2016-03-09 | 2016-06-15 | 湛江市博泰生物化工科技实业有限公司 | Method for extracting euphausia superba oil through nitrogen pressurizing water vapor |
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| CN102041166A (en) * | 2011-01-20 | 2011-05-04 | 山东师范大学 | Method for extracting krill oil with high phosphatide content from Antarctic krills |
| CN102143690A (en) * | 2008-08-11 | 2011-08-03 | 雀巢产品技术援助有限公司 | Oil containing one or more long-chain polyunsaturated fatty acids phospholipids derived from biomass |
| US20120088831A1 (en) * | 2009-03-19 | 2012-04-12 | Apt Kirk E | Thraustochytrids, Fatty Acid Compositions, and Methods of Making and Uses Thereof |
| CN102492545A (en) * | 2011-12-28 | 2012-06-13 | 中国水产科学研究院黄海水产研究所 | Methods for extracting high-quality shrimp oil from Antarctic krill and for preparing defatted krill protein powder |
| WO2012079219A1 (en) * | 2010-12-14 | 2012-06-21 | 大连工业大学 | Methods for preparing shrimp grease and preparing shrimp concentrate or shrimp med from euphausia superba |
| CN102559369A (en) * | 2010-12-14 | 2012-07-11 | 大连工业大学 | Preparation method of antarctic krill oil |
| CN103320217A (en) * | 2013-07-11 | 2013-09-25 | 日照海大博远海洋生物科技有限公司 | Method for extracting krill oil rich in phospholipid from euphausia superba |
-
2014
- 2014-10-16 CN CN201410547705.5A patent/CN104263499A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102143690A (en) * | 2008-08-11 | 2011-08-03 | 雀巢产品技术援助有限公司 | Oil containing one or more long-chain polyunsaturated fatty acids phospholipids derived from biomass |
| US20120088831A1 (en) * | 2009-03-19 | 2012-04-12 | Apt Kirk E | Thraustochytrids, Fatty Acid Compositions, and Methods of Making and Uses Thereof |
| WO2012079219A1 (en) * | 2010-12-14 | 2012-06-21 | 大连工业大学 | Methods for preparing shrimp grease and preparing shrimp concentrate or shrimp med from euphausia superba |
| CN102559369A (en) * | 2010-12-14 | 2012-07-11 | 大连工业大学 | Preparation method of antarctic krill oil |
| CN102041166A (en) * | 2011-01-20 | 2011-05-04 | 山东师范大学 | Method for extracting krill oil with high phosphatide content from Antarctic krills |
| CN102492545A (en) * | 2011-12-28 | 2012-06-13 | 中国水产科学研究院黄海水产研究所 | Methods for extracting high-quality shrimp oil from Antarctic krill and for preparing defatted krill protein powder |
| CN103320217A (en) * | 2013-07-11 | 2013-09-25 | 日照海大博远海洋生物科技有限公司 | Method for extracting krill oil rich in phospholipid from euphausia superba |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105670779A (en) * | 2016-03-09 | 2016-06-15 | 湛江市博泰生物化工科技实业有限公司 | Method for extracting euphausia superba oil through nitrogen pressurizing water vapor |
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