CN104224565A - Alfalfa leaf protein moistening facial mask and preparation method thereof - Google Patents
Alfalfa leaf protein moistening facial mask and preparation method thereof Download PDFInfo
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- CN104224565A CN104224565A CN201410410162.2A CN201410410162A CN104224565A CN 104224565 A CN104224565 A CN 104224565A CN 201410410162 A CN201410410162 A CN 201410410162A CN 104224565 A CN104224565 A CN 104224565A
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- leaf protein
- alfalfa leaf
- alfalfa
- facial mask
- herba medicaginis
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Abstract
The invention provides an alfalfa leaf protein moistening facial mask. The facial mask is a transparent collagen moistening facial mask and is prepared from the following components in parts by mass: 0.05-5 parts of alfalfa leaf protein serving as a functional raw material, 0.2-10 parts of sodium carboxymethylcellulose, 0.2-10 parts of humectant, 0.05-10 parts of starch and 1-20 parts of a glutaraldehyde crosslinking agent, wherein the sodium carboxymethylcellulose, humectant, starch and glutaraldehyde crosslinking agent are used as auxiliary raw materials. The preparation method comprises the following steps: firstly, extracting alfalfa leaf protein from alfalfa leaves in a fermenting manner; then mixing the alfalfa leaf protein and the auxiliary raw materials; and finally, putting the mixture in a die, heating and forming a film. The alfalfa leaf protein moistening facial mask is mainly prepared from macromolecular substances in natural animal and plant, is non-toxic and odorless, and does not have side effect. The facial mask has the effects of double moistening effect, good toughness, good ductility and good adhesion, and has functions of better skin feeling and deep skin cleaning, thus being an economical, practical and effective skin-care beautifying cosmetic. The facial mask preparation process is simple, is convenient to operate, and does not pollute the environment.
Description
Technical field
The present invention relates to a kind of daily cosmetics and preparation method thereof, particularly moisture saver mask and preparation method thereof.
Background technology
Along with improving constantly of living standards of the people, cosmetics occupy more and more important position in people's life, thus have driven the development of cosmetic science technology.In recent years, the kind of cosmetics is on the increase, and facial film is then more and more by cosmetics that people favor.Facial film class cosmetics mainly powdery, paste or the pureed of selling in the market.Paste or pureed facial film can directly be coated on the face, and powdery stirs into pasty state and can be coated on the face after adding water, through washing off after a period of time.This facial film uses cumbersome; Also the facial film being soaked with wetting agent above carrier made by useful non-woven fabrics, and this facial film still retains many effective ingredient with on rear nonwoven carrier, causes the waste of effective ingredient.
Summary of the invention
The object of the present invention is to provide a kind ofly to ultraviolet damage, there is good repair, have human body skin dual moistening effect, increase substantially cuticular accretion rate, repair damaged cell and reduce alfalfa leaf protein moisture saver mask and preparation method thereof that wrinkle of skin increases elasticity, efficient lock water.
Alfalfa leaf protein moisture saver mask of the present invention is using 0.05 ~ 5 part of alfalfa leaf protein as function raw material, using 0.2 ~ 10 part of sodium carboxymethyl cellulose, 0.2 ~ 10 part of wetting agent, 0.05 ~ 10 part of starch and 1 ~ 20 part of glutaraldehyde cross-linking agent as auxiliary material, the outward appearance made is transparent collagen wet-retaining face mask.Each raw material is all in mass fraction, and wetting agent is the one in sorbitol or lactic acid.
The preparation method of alfalfa leaf protein moisture saver mask of the present invention is specific as follows:
1. extract alfalfa leaf protein
(1) Herba Medicaginis leaf getting Herba Medicaginis in squaring period is raw material, pulls an oar after cleaning.
(2) Herba Medicaginis leaf step 1 being broken into pulpous state filters, and gets filtrate and Herba Medicaginis leaf slurry.
(3) Herba Medicaginis leaf obtained to step 2 adds fermented bacterium and lactobacillus in starching, and dosage of inoculation is that every milliliter of Herba Medicaginis leaf slurry is with 10
7~ 10
9individual lactobacillus is lived, and in 30 ~ 39 DEG C of temperature, ferments 8 ~ 10 hours.
(4) on the centrifuge tunning that step 3 obtains being placed in 3000 revs/min, process 8 ~ 12 minutes, then static, makes it flocculation, the alfalfa leaf protein crude extract below separation of supernatant.
(5) alfalfa leaf protein crude extract step 4 obtained carries out lyophilization process 1-2 hour in-4 DEG C of temperature, namely obtains alfalfa leaf protein product.
2. make facial film
(1) sodium carboxymethyl cellulose is added in deionized water, stir and make it to become clear viscous shape;
(2) in the container filling alfalfa leaf protein, wetting agent, cross-linking agent glutaraldehyde and starch is added, in the even resulting mixture of stirred at ambient temperature;
(3) by step 1) product and the sodium carboxymethyl cellulose of clear viscous shape be added to step 2) mixture in, 40-50 DEG C of temperature stirs to obtain complex liquid;
(4) complex liquid is poured in the mould of facial film, the drier 4-7 hour of baking oven mould being placed in 60-70 DEG C of temperature, take off film afterwards, namely obtaining outward appearance is transparent alfalfa leaf protein moisture saver mask.
Alfalfa leaf protein moisture saver mask is a kind of native protein facial film, and 72% of application on human skin has albumen.Albumen forms elasticated net in skin, supports skin and pins moisture.During women 20 years old, collagen protein starts to run off, and within 25 years old, enters collagen protein Loss-peak, and when 40 years old, collagen content was less than the half of 18 years old.Collagen protein runs off and causes supporting the elasticated net fracture of skin, skin histology atrophy, subsides, the aging phenomenon such as scaly dry skin, coarse, lax, wrinkle, corse sweat pore, skin dark stain, mottle.After the composition of alfalfa leaf protein facial film enters dermal tissue, local collapse can be filled up rapidly, improve lax, tighten up skin, reduce deep wrinkle, the microgroove that calms down.Fracture, aging elastic fibrous web can be repaired, skin elasticity is recovered, pliable and tough full.
The present invention compared with prior art tool has the following advantages:
1, facial film of the present invention is mainly made up of natural plants, nontoxic, tasteless, have no side effect, and has good toughness, ductility and cementability, and skinfeel is splendid.
2, contain the hydrophilic groups such as amino, hydroxyl in alfalfa leaf protein, to human body skin, there is unique moisture-keeping function, cuticular accretion rate can be increased substantially, repair damaged cell, reduce wrinkle of skin, increase elasticity, efficiently lock water.
3, function raw material alfalfa leaf protein of the present invention and skin have fabulous adsorptivity and the compatibility, have the function blocking brown pigment and generate, therefore have good repair to ultraviolet damage.
4, directly use, very convenient; From as carrier, reduce effective ingredient waste.
5, raw material sources are extensive, and the cost of product is low.
6, simple, easy to operate, the non-environmental-pollution of preparation method.
Detailed description of the invention
Example 1
The Herba Medicaginis leaf getting Herba Medicaginis in squaring period is raw material, pulls an oar after cleaning; The Herba Medicaginis leaf breaking into pulpous state is filtered, gets filtrate and Herba Medicaginis leaf slurry; Add lactobacillus again to the Herba Medicaginis leaf slurry obtained, dosage of inoculation is that every milliliter of Herba Medicaginis leaf slurry is with 10
9individual lactobacillus was lived, in 30 DEG C of temperature fermentation 10 hours; The centrifuge tunning of acquisition being placed in 3000 revs/min continues process 8 minutes, then staticly makes it flocculation, then without after flocculation sediment, removing supernatant gets the alfalfa leaf protein crude extract of flocculation sediment; Alfalfa leaf protein crude extract is placed in-4 DEG C and carries out lyophilization process 1 hour, namely obtain the alfalfa leaf protein product that outward appearance is clear viscous.
Get 0.2 gram of sodium carboxymethyl cellulose and be placed in container, add deionized water, stir and make it to become clear viscous shape; Get 0.05 gram of above-mentioned alfalfa leaf protein, add in beaker, then add 0.2 gram of sorbitol wetting agent respectively in this beaker, 1 gram of glutaraldehyde cross-linking agent and 0.05 gram of starch, in the even resulting mixture of stirred at ambient temperature; Again the sodium carboxymethyl cellulose of above-mentioned clear viscous shape is added in mixture, the complex liquid that stirs to obtain is continued in 50 DEG C of temperature, complex liquid is poured in the mould of facial film, then mould is placed in baking oven, take off film 60 DEG C of temperature after dry 7 hours, namely obtaining outward appearance is transparent alfalfa leaf protein moisture saver mask.
Example 2
The Herba Medicaginis leaf getting Herba Medicaginis in squaring period is raw material, pulls an oar after cleaning; The Herba Medicaginis leaf breaking into pulpous state is filtered, gets filtrate and Herba Medicaginis leaf slurry; Add lactobacillus again to the Herba Medicaginis leaf slurry obtained, dosage of inoculation is that every milliliter of Herba Medicaginis leaf slurry is with 10
7individual lactobacillus was lived, in 39 DEG C of temperature fermentation 8 hours; The centrifuge tunning of acquisition being placed in 3000 revs/min continues process 12 minutes, then staticly makes it flocculation, then without after flocculation sediment, removing supernatant gets the alfalfa leaf protein crude extract of flocculation sediment; Alfalfa leaf protein crude extract is placed in-4 DEG C and carries out lyophilization process 2 hours, namely obtain the alfalfa leaf protein product that outward appearance is clear viscous.
Get 10 grams of sodium carboxymethyl cellulose and be placed in container, add deionized water, stir and make it to become clear viscous shape; Get 5 grams of above-mentioned alfalfa leaf proteins, add in beaker, then add 10 grams of lactic acid wetting agents respectively in this beaker, 20 grams of glutaraldehyde cross-linking agent and 10 grams of starch, in the even resulting mixture of stirred at ambient temperature; Again the sodium carboxymethyl cellulose of above-mentioned clear viscous shape is added in mixture, the complex liquid that stirs to obtain is continued in 40 DEG C of temperature, complex liquid is poured in the mould of facial film, then mould is placed in baking oven, take off film 70 DEG C of temperature after dry 4 hours, namely obtain the alfalfa leaf protein moisture saver mask that outward appearance is clear viscous.
Example 3
The Herba Medicaginis leaf getting Herba Medicaginis in squaring period is raw material, pulls an oar after cleaning; The Herba Medicaginis leaf breaking into pulpous state is filtered, gets filtrate and Herba Medicaginis leaf slurry; Add lactobacillus again to the Herba Medicaginis leaf slurry obtained, dosage of inoculation is that every milliliter of Herba Medicaginis leaf slurry is with 10
8individual lactobacillus was lived, in 35 DEG C of temperature fermentation 9 hours; The centrifuge tunning of acquisition being placed in 3000 revs/min continues process 10 minutes, then staticly makes it flocculation, then without after flocculation sediment, removing supernatant gets the alfalfa leaf protein crude extract of flocculation sediment; Alfalfa leaf protein crude extract is placed in-4 DEG C and carries out lyophilization process 1.5 hours, namely obtain the alfalfa leaf protein product that outward appearance is clear viscous.
Get 5 grams of sodium carboxymethyl cellulose and be placed in container, add deionized water, stir and make it to become clear viscous shape; Get 2 grams of above-mentioned alfalfa leaf proteins, add in beaker, then in this beaker, add 2 grams of lactic acid and 2 grams of sorbitol wetting agents respectively, 10 grams of glutaraldehyde cross-linking agent and 1 gram of starch, in the even resulting mixture of stirred at ambient temperature; Again the sodium carboxymethyl cellulose of above-mentioned clear viscous shape is added in mixture, the complex liquid that stirs to obtain is continued in 40 DEG C of temperature, complex liquid is poured in the mould of facial film, then mould is placed in baking oven, take off film 65 DEG C of temperature after dry 6 hours, namely obtain the alfalfa leaf protein moisture saver mask that outward appearance is clear viscous.
The using method of facial film of the present invention:
1. after thoroughly cleaning clean face, with referring to that abdomen beats easily out facial film, during taking-up, thin film being torn completely, capturing with fingernail or firmly pinching in order to avoid cause facial film to break.
2. facial film is fixed on forehead, chin and nose.Then from the centre of face, with finger, facial film is slowly pushed open toward the surrounding of face, the bubble in facial film is extruded.Use first, without any discomfort reflection in 30 minutes, application time can extend to 1-2 hour.After having applied, the essential ingredient of residual face is massaged a little, then smears emulsion and close as last lock water.1-2 time weekly.If (think that very ice can with using warm water bubble before, note too not hot water, not so can melt away) time will note cleaning, this thing is not reused, except you use facial film skin protection, also will remember rule of working and resting, cooking, like that just can be more comprehensively to the care of skin.
Use rear staining effect:
Thought after the people of 90% used this facial film that moistening effect is fine, and be ready to reuse.
Claims (2)
1. an alfalfa leaf protein moisture saver mask, it is characterized in that: it is that 0.05 ~ 5 part of alfalfa leaf protein is as function raw material using mass fraction, using mass fraction be 0.2 ~ 10 part of sodium carboxymethyl cellulose, 0.2 ~ 10 part of wetting agent, 0.05 ~ 10 part of starch and 1 ~ 20 part of glutaraldehyde cross-linking agent be transparent collagen wet-retaining face mask as the outward appearance that auxiliary material is made, wetting agent is the one in sorbitol or lactic acid.
2. the preparation method of the alfalfa leaf protein moisture saver mask of claim 1, is characterized in that:
1) alfalfa leaf protein is extracted
(1) Herba Medicaginis leaf getting Herba Medicaginis in squaring period is raw material, pulls an oar after cleaning,
(2) Herba Medicaginis leaf step 1 being broken into pulpous state filters, and gets filtrate and Herba Medicaginis leaf slurry,
(3) Herba Medicaginis leaf obtained to step 2 adds fermented bacterium and lactobacillus in starching, and dosage of inoculation is that every milliliter of Herba Medicaginis leaf slurry is with 10
7~ 10
9individual lactobacillus is lived, and in 30 ~ 39 DEG C of temperature, ferments 8 ~ 10 hours,
(4) on the centrifuge tunning that step 3 obtains being placed in 3000 revs/min, process 8 ~ 12 minutes, then static, makes it flocculation, the alfalfa leaf protein crude extract below separation of supernatant,
(5) alfalfa leaf protein crude extract step 4 obtained carries out cryostat dried 1 ~ 2 hour in-4 DEG C of temperature, namely obtains alfalfa leaf protein product;
2) facial film is made
(1) sodium carboxymethyl cellulose is added in deionized water, stirs and make it to become clear viscous shape,
(2) in the container filling alfalfa leaf protein, wetting agent, cross-linking agent glutaraldehyde and starch is added, in the even resulting mixture of stirred at ambient temperature,
(3) by step 1) product and the sodium carboxymethyl cellulose of clear viscous shape be added to step 2) mixture in, to stir to obtain complex liquid in 40-50 DEG C of temperature,
(4) complex liquid is poured in the mould of facial film, the drier 4-7 hour of baking oven mould being placed in 60-70 DEG C of temperature, take off film afterwards, namely obtaining outward appearance is transparent alfalfa leaf protein moisture saver mask.
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| CN201410410162.2A CN104224565A (en) | 2014-08-19 | 2014-08-19 | Alfalfa leaf protein moistening facial mask and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104940120A (en) * | 2015-07-08 | 2015-09-30 | 青岛嘉瑞生物技术有限公司 | Process for preparing anti-skin-aging skin moisturizer adopting alfalfa |
| CN105168044A (en) * | 2015-09-01 | 2015-12-23 | 广州赛莱拉干细胞科技股份有限公司 | Collagen composition and collagen membrane sticker |
| CN107789260A (en) * | 2017-12-24 | 2018-03-13 | 姚佑灿 | A kind of replenishing water and preserving moisture facial mask |
| CN107854372A (en) * | 2017-12-26 | 2018-03-30 | 大连民族大学 | A kind of beautifying facial mask preparation method of the zymotic fluid containing alfalfa |
| CN107929211A (en) * | 2017-12-26 | 2018-04-20 | 大连民族大学 | A kind of alfalfa leaf protein moisture saver mask |
| CN107998027A (en) * | 2017-12-24 | 2018-05-08 | 姚佑灿 | A kind of antiradiation injury repairs breast |
| KR102605467B1 (en) * | 2023-05-04 | 2023-11-23 | 한국콜마주식회사 | Cosmetic composition for skin improvement comprising an extract of alfalfa seed-derived glycoprotein |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104940120A (en) * | 2015-07-08 | 2015-09-30 | 青岛嘉瑞生物技术有限公司 | Process for preparing anti-skin-aging skin moisturizer adopting alfalfa |
| CN104940120B (en) * | 2015-07-08 | 2017-11-14 | 张宝祥 | A kind of technique for preparing anti aging effect shin moisturizer using clover |
| CN105168044A (en) * | 2015-09-01 | 2015-12-23 | 广州赛莱拉干细胞科技股份有限公司 | Collagen composition and collagen membrane sticker |
| CN107789260A (en) * | 2017-12-24 | 2018-03-13 | 姚佑灿 | A kind of replenishing water and preserving moisture facial mask |
| CN107998027A (en) * | 2017-12-24 | 2018-05-08 | 姚佑灿 | A kind of antiradiation injury repairs breast |
| CN107854372A (en) * | 2017-12-26 | 2018-03-30 | 大连民族大学 | A kind of beautifying facial mask preparation method of the zymotic fluid containing alfalfa |
| CN107929211A (en) * | 2017-12-26 | 2018-04-20 | 大连民族大学 | A kind of alfalfa leaf protein moisture saver mask |
| KR102605467B1 (en) * | 2023-05-04 | 2023-11-23 | 한국콜마주식회사 | Cosmetic composition for skin improvement comprising an extract of alfalfa seed-derived glycoprotein |
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Application publication date: 20141224 |