CN104222888B - A kind of former dew of tuberous plant, preparation method and application - Google Patents

A kind of former dew of tuberous plant, preparation method and application Download PDF

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Publication number
CN104222888B
CN104222888B CN201410429253.0A CN201410429253A CN104222888B CN 104222888 B CN104222888 B CN 104222888B CN 201410429253 A CN201410429253 A CN 201410429253A CN 104222888 B CN104222888 B CN 104222888B
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former dew
material
composition
vacuum chamber
dew
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CN201410429253.0A
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Chinese (zh)
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CN104222888A (en
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金湘范
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金湘范
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/06Fungi, e.g. yeasts
    • A61K36/07Basidiomycota, e.g. Cryptococcus
    • A61K36/076Poria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/31Brassicaceae or Cruciferae (Mustard family), e.g. broccoli, cabbage or kohlrabi
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/896Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
    • A61K36/8962Allium, e.g. garden onion, leek, garlic or chives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/896Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
    • A61K36/8969Polygonatum (Solomon's seal)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/898Orchidaceae (Orchid family)
    • A61K36/8984Dendrobium
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/906Zingiberaceae (Ginger family)
    • A61K36/9068Zingiber, e.g. garden ginger
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/02Cosmetics or similar toilet preparations characterised by special physical form
    • A61K8/0241Containing particulates characterized by their shape and/or structure
    • A61K8/0275Containing agglomerated particulates
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/96Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/96Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs

Abstract

This application discloses a kind of former dew of tuberous plant, by the volatile material composition in plant, water-soluble substances composition, and/or the extracting solution of liposoluble substance composition composition subset form.The invention have the benefit that first, the herbal stock solution of extraction is subset liquid, remains the original composition proportion of plant, the characteristic such as organic mineral substance and activation so that plant can enter human body with liquid and quickly be absorbed, and penetrates into intracellular, alleviate metabolic disease, promote growth.Second, it is possible to strand group is broken up and makes the former dew being more easy to absorb, it is applied to book on Chinese herbal medicine beauty treatment, daily use chemicals product, special dietary seafood, seasoning dew, former alcoholic drink mixed with fruit juice, book on Chinese herbal medicine function product, health product.Average about the 50Hz of 3rd, NMR value, forms the most former dew of small molecule, strengthens rapidly human metabolism's level, accelerates active nutritional material in former dew and be absorbed by the body, and absorbance is up to 99%.

Description

A kind of former dew of tuberous plant, preparation method and application

Technical field

The present invention relates to a kind of former dew of tuberous plant, preparation method and application.

Background technology

Tuber is botany vocabulary of terms.It is a species transformation of axis, in bulk, therefore named.Since It is stem, the most just there is the principal character of axis, such as bud, leaf scar etc..Tuberous plant generally pushes up Portion is loose, has the parenchyma of prosperity, the nutrient substance that storage is abundant.There are many eyes on the surface of tuber, Typically making helical arrangement, have 2~3 axillalry buds in eye, only one axillalry bud is easily sprouted, and can grow Go out shoot, therefore tuber is available for breeding and is used.The top of tuber has a terminal bud, such as the tuber of Rhizoma Solani tuber osi More typical case.Rhizoma Solani tuber osi undergland shoot sprawl growth in soil layer, when extending 9~12 centimetres, end Expand, formed and there is the plump tuber between pipe nipple.On the tuber grown up to, there is perithelium on top layer, above has few Number hole skin.The cross section of tuber still can separate cortex, outer phloem, xylem, endophloem and The marrow of central authorities.

Tuberous plant has characteristics that in terms of nutritional labeling water content is high, mostly is 75~90%, Dry is relatively fewer;In dry, crude fiber content is low, is 2~4%, and crude protein is 7~15%, Crude fat is less than 9%, and nitrogen-free extract is up to 67.5~88.15%, and is that digestible starch or penta gathers Sugar.Prior art does not also have to carry out effective extracting method for the nutritional labeling of tuberous plant, to pass As a example by the way of distillation of system is extracted, its significant drawback is: steam allogenic water applies, it is impossible to whole part extracts, Hydrone solution, steam is carried secretly, is book on Chinese herbal medicine aqueous solution, and, the limitation of traditional handicraft is, It is difficult to breaking cellular wall because of itself nutrient and strand group is too big, thus extract is difficult to be absorbed by the body.

Summary of the invention

It is an object of the invention to overcome above-mentioned deficiency, it is provided that a kind of former dew of tuberous plant, preparation method And application, to realize whole part extraction.

To achieve these goals, the technical solution used in the present invention is:

A kind of former dew of tuberous plant, it is characterised in that by the volatile material composition in plant, water-soluble Property Matter Composition, and/or liposoluble substance composition composition subset form extracting solution.

Further, described tuberous plant includes: Rhizoma Zingiberis Recens, Bulbus Allii, Maca, Poria, Rhizoma Polygonati, Fructus Arctii, and/or Herba Dendrobii.

Further, the described hexagonal structure of subset form.

Further, described former dew is configured to water preparation, granule, bagged steeping drug, syrup, capsule Or tablet.

Another object of the present invention is to provide the preparation method of the former dew of a kind of tuberous plant, its feature to exist In, including:

A) at a certain temperature, the volatile material using out-phase liquid ultramicrotechnique to extract in plant becomes Part, water-soluble substances composition, and/or liposoluble substance composition;

B) product of step A is carried out homogeneous polymerization, to prepare former dew.

Further, described out-phase liquid ultramicrotechnique includes: moment produces vacuum and allows described tubers The step that plant is the most expanded.

Further, the temperature of described step A is at 45~250 DEG C.

Further, described former dew is the extracting solution of subset form.

Further, the magnetic resonance detection index of the extracting solution of described subset form is 46~70Hz.

The a further object of the present invention is to provide described former being exposed at of tuberous plant to prepare food, daily use chemicals product With the application in health product.

The invention have the benefit that

First, the herbal stock solution of extraction is subset liquid, remains the original composition proportion of plant, Make the characteristics such as the full and uniform polymerization of out-phase liquid and activation so that plant can enter human body quickly with liquid Absorbed, penetrated into intracellular, strengthen rapidly human metabolism's level, accelerate active nutritional thing in former dew Matter is absorbed by the body, and absorbance is up to 99%.Alleviate metabolic disease, promote growth.

Second, it is possible to strand group is broken up and makes the former dew being more easy to absorb, it is applied to book on Chinese herbal medicine beauty treatment, day Change product, special dietary seafood, seasoning dew, former alcoholic drink mixed with fruit juice, book on Chinese herbal medicine function product, health product, cmm of simple prescription, Chinese medicine Compound recipe.

3rd, NMR value average 49~60HZ, the molecular chain length convergence making out-phase liquid is identical, promotees Enter the abundant of out-phase liquid being originally difficult to merge to be polymerized, form the former dew of small micel, improve former dew and gather The uniformity of conjunction, stability, antitypy, give full play to the effect of all kinds of oxidant, the antioxygen on Shi Yuan road Change performance to significantly improve.

Detailed description of the invention

As employed some vocabulary in the middle of description and claim to censure specific components.This area skill Art personnel are it is to be appreciated that hardware manufacturer may call same assembly with different nouns.This explanation In the way of book and claim not difference by title is used as distinguishing assembly, but with assembly in function On difference be used as distinguish criterion." bag as mentioned by the middle of description in the whole text and claim Contain " it is an open language, therefore " comprise but be not limited to " should be construed to." substantially " refer to receivable In range of error, those skilled in the art can solve described technical problem, base in the range of certain error Originally described technique effect is reached.Description subsequent descriptions is to implement the better embodiment of the application, right institute State description be the rule so that the application to be described for the purpose of, be not limited to scope of the present application.This The protection domain of application is when being as the criterion depending on the defined person of claims.

Embodiment 1

A kind of former dew of Bulbus Allii, by the volatile material composition in Bulbus Allii, water-soluble substances composition, and/or fat The extracting solution of soluble substance composition composition subset form.

Preferably, the described hexagonal structure of subset form.

Preferably, described former dew be configured to water preparation, granule, bagged steeping drug, syrup, capsule or Tablet.

The preparation method of the former dew of a kind of Bulbus Allii, it is characterised in that including:

A) at a certain temperature, the volatile material using out-phase liquid ultramicrotechnique to extract in Bulbus Allii becomes Part, water-soluble substances composition, and/or liposoluble substance composition;

B) product of step A is carried out homogeneous polymerization, to prepare former dew.

Described out-phase liquid ultramicrotechnique includes that moment produces vacuum and allows the most expanded step of described material Suddenly.Specifically, including the first stage, in vacuum chamber, central authorities' container perimeter is placed material and enters Row heating;Second stage, moment generation vacuum, the material making needs extract is the most expanded;3rd rank Section, forms low temperature on center vessel top, and the environment of high temperature is formed at bottom, to form convection current;Fourth order Section, discharges stock solution by hight atmospheric molecular motion;In 5th stage, stock solution is slowly drawn out of, in being pooled to Centre container.

Preferably, the mode of heating of employing has infrared heating, microwave heating etc., and the heat provided was both Quickly to make material expanded, material surface can not be made again to sustain damage.

Preferably, by heating, material internal moisture is constantly evaporated, made the pore of material by vacuum Open, the air of the pore in material is extracted out simultaneously, make material internal moisture flash distillation, cause material Surface is formed uniformly, alveolate texture.

Preferably, the temperature of described step A is at 45~250 DEG C.

Preferably, the device of described out-phase liquid ultramicrotechnique includes vacuum chamber, sets at internal vacuum chamber Putting center vessel, material is placed in vacuum chamber, is on heating plate, in the particular embodiment, and profit By Far-infrared Heating, it is ensured that uniform drying, the temperature of heating plate is accurately controlled by heating curves.

Preferably, the top of vacuum chamber is provided with heat sink, such as fan so that material is in heating During, low temperature is formed on center vessel top, the environment of high temperature is formed at bottom, to form molecular motion Convection current.

Preferably, being moved by hight atmospheric molecular, stock solution is slowly drawn out of, the volatile material in material Composition, water-soluble substances composition, and/or liposoluble substance composition carry out homogeneous polymerization, are pooled to central authorities' appearance Device, it is achieved whole part extracts, to form the extracting solution of subset form.

Preferably, described former dew is the extracting solution of subset form.

Preferably, described former dew is the extracting solution of subset form, and subset form is hexagonal Structure.In human body cell, the structure of institute's water content is mainly hexagonal annular structure, so former dew and human body Cell most affinity, also most beneficial for health.

Preferably, the magnetic resonance detection index of the extracting solution of described subset form is 46~70Hz.

The present embodiment is to provide described former being exposed at of Bulbus Allii to prepare food, answering in daily use chemicals product and health product With.

Test

Subset diameter about 0.5 nanometer extracted, and the cell wall conduit aperture of human body is 2 nanometers, After drinking, directly can not enter blood by cells of vascular wall film by digestive system, penetrate arrival Pathogen, can supplement rapidly human nutrition and energy in one second, rapidly can be by shrivelled erythrocyte Activate, be obviously enhanced human metabolism's level, accelerate active nutritional material and directly effectively absorbed by human body, Absorbance is up to 99%.

Subset liquid is extremely continual and steady, and antioxidation is strong, the most still presents small point Sub-bulk state, the shelf-life is longer, after the former dew of the present invention enters human body, it is not necessary to dissolve, directly by the intestines and stomach Overall absorption, in contrast to common solid-state tablet or capsule, can only dissolve 20% after entering human body, additionally 80% the most digested part can cause get angry, abdominal distention, constipation, the side effect such as the toxin remains.

Embodiment 2

A kind of former dew of Poria, by the volatile material composition in Poria, water-soluble substances composition, and/or fat The extracting solution of soluble substance composition composition subset form.

Preferably, the described hexagonal structure of subset form.

Preferably, described former dew be configured to water preparation, granule, bagged steeping drug, syrup, capsule or Tablet.

The preparation method of the former dew of a kind of Poria, it is characterised in that including:

A) at a certain temperature, the volatile material using out-phase liquid ultramicrotechnique to extract in Poria becomes Part, water-soluble substances composition, and/or liposoluble substance composition;

B) product of step A is carried out homogeneous polymerization, to prepare former dew.

Described out-phase liquid ultramicrotechnique includes that moment produces vacuum and allows the most expanded step of described material Suddenly.Specifically, including the first stage, in vacuum chamber, central authorities' container perimeter is placed material and enters Row heating;Second stage, moment generation vacuum, the material making needs extract is the most expanded;3rd rank Section, forms low temperature on center vessel top, and the environment of high temperature is formed at bottom, to form convection current;Fourth order Section, discharges stock solution by hight atmospheric molecular motion;In 5th stage, stock solution is slowly drawn out of, in being pooled to Centre container.

Preferably, the mode of heating of employing has infrared heating, microwave heating etc., and the heat provided was both Quickly to make material expanded, material surface can not be made again to sustain damage.

Preferably, by heating, material internal moisture is constantly evaporated, made the pore of material by vacuum Open, the air of the pore in material is extracted out simultaneously, make material internal moisture flash distillation, cause material Surface is formed uniformly, alveolate texture.

Preferably, the temperature of described step A is at 45~250 DEG C.

Preferably, the device of described out-phase liquid ultramicrotechnique includes vacuum chamber, sets at internal vacuum chamber Putting center vessel, material is placed in vacuum chamber, is on heating plate, in the particular embodiment, and profit By Far-infrared Heating, it is ensured that uniform drying, the temperature of heating plate is accurately controlled by heating curves.

Preferably, the top of vacuum chamber is provided with heat sink, such as fan so that material is in heating During, low temperature is formed on center vessel top, the environment of high temperature is formed at bottom, to form molecular motion Convection current.

Preferably, being moved by hight atmospheric molecular, stock solution is slowly drawn out of, the volatile material in material Composition, water-soluble substances composition, and/or liposoluble substance composition carry out homogeneous polymerization, are pooled to central authorities' appearance Device, it is achieved whole part extracts, to form the extracting solution of subset form.

Preferably, described former dew is the extracting solution of subset form, and subset form is hexagonal Structure.In human body cell, the structure of institute's water content is mainly hexagonal annular structure, so former dew and human body Cell most affinity, also most beneficial for health.

Preferably, the magnetic resonance detection index of the extracting solution of described subset form is 46~70Hz.

The present embodiment is to provide described former being exposed at of Poria to prepare food, answering in daily use chemicals product and health product With.

Test

Subset diameter about 0.5 nanometer extracted, and the cell wall conduit aperture of human body is 2 nanometers, After drinking, directly can not enter blood by cells of vascular wall film by digestive system, penetrate arrival Pathogen, can supplement rapidly human nutrition and energy in one second, rapidly can be by shrivelled erythrocyte Activate, be obviously enhanced human metabolism's level, accelerate active nutritional material and directly effectively absorbed by human body, Absorbance is up to 99%.

Subset liquid is extremely continual and steady, and antioxidation is strong, the most still presents small point Sub-bulk state, the shelf-life is longer, after the former dew of the present invention enters human body, it is not necessary to dissolve, directly by the intestines and stomach Overall absorption, in contrast to common solid-state tablet or capsule, can only dissolve 20% after entering human body, additionally 80% the most digested part can cause get angry, abdominal distention, constipation, the side effect such as the toxin remains.

Embodiment 3

A kind of former dew of Maca, by the volatile material composition in Maca, water-soluble substances composition, and/or fat The extracting solution of soluble substance composition composition subset form.

Preferably, the described hexagonal structure of subset form.

Preferably, described former dew be configured to water preparation, granule, bagged steeping drug, syrup, capsule or Tablet.

The preparation method of the former dew of a kind of Maca, it is characterised in that including:

A) at a certain temperature, the volatile material using out-phase liquid ultramicrotechnique to extract in Maca becomes Part, water-soluble substances composition, and/or liposoluble substance composition;

B) product of step A is carried out homogeneous polymerization, to prepare former dew.

Described out-phase liquid ultramicrotechnique includes that moment produces vacuum and allows the most expanded step of described material Suddenly.Specifically, including the first stage, in vacuum chamber, central authorities' container perimeter is placed material and enters Row heating;Second stage, moment generation vacuum, the material making needs extract is the most expanded;3rd rank Section, forms low temperature on center vessel top, and the environment of high temperature is formed at bottom, to form convection current;Fourth order Section, discharges stock solution by hight atmospheric molecular motion;In 5th stage, stock solution is slowly drawn out of, in being pooled to Centre container.

Preferably, the mode of heating of employing has infrared heating, microwave heating etc., and the heat provided was both Quickly to make material expanded, material surface can not be made again to sustain damage.

Preferably, by heating, material internal moisture is constantly evaporated, made the pore of material by vacuum Open, the air of the pore in material is extracted out simultaneously, make material internal moisture flash distillation, cause material Surface is formed uniformly, alveolate texture.

Preferably, the temperature of described step A is at 45~250 DEG C.

Preferably, the device of described out-phase liquid ultramicrotechnique includes vacuum chamber, sets at internal vacuum chamber Putting center vessel, material is placed in vacuum chamber, is on heating plate, in the particular embodiment, and profit By Far-infrared Heating, it is ensured that uniform drying, the temperature of heating plate is accurately controlled by heating curves.

Preferably, the top of vacuum chamber is provided with heat sink, such as fan so that material is in heating During, low temperature is formed on center vessel top, the environment of high temperature is formed at bottom, to form molecular motion Convection current.

Preferably, being moved by hight atmospheric molecular, stock solution is slowly drawn out of, the volatile material in material Composition, water-soluble substances composition, and/or liposoluble substance composition carry out homogeneous polymerization, are pooled to central authorities' appearance Device, it is achieved whole part extracts, to form the extracting solution of subset form.

Preferably, described former dew is the extracting solution of subset form, and subset form is hexagonal Structure.In human body cell, the structure of institute's water content is mainly hexagonal annular structure, so former dew and human body Cell most affinity, also most beneficial for health.

Preferably, the magnetic resonance detection index of the extracting solution of described subset form is 46~70Hz.

The present embodiment is to provide described former being exposed at of Maca to prepare food, answering in daily use chemicals product and health product With.

Test

Subset diameter about 0.5 nanometer extracted, and the cell wall conduit aperture of human body is 2 nanometers, After drinking, directly can not enter blood by cells of vascular wall film by digestive system, penetrate arrival Pathogen, can supplement rapidly human nutrition and energy in one second, rapidly can be by shrivelled erythrocyte Activate, be obviously enhanced human metabolism's level, accelerate active nutritional material and directly effectively absorbed by human body, Absorbance is up to 99%.Human body is had the function of nourishing and fit keeping function, make people full of physical strength, spiritual vigorous will not Fatigue, enhances metabolism, renitency promote the Functional Capability of the mankind, eliminate climacteric obstacle, Slow down aging, promote brain vigor.

Subset liquid is extremely continual and steady, and antioxidation is strong, the most still presents small point Sub-bulk state, the shelf-life is longer, after the former dew of the present invention enters human body, it is not necessary to dissolve, directly by the intestines and stomach Overall absorption, in contrast to common solid-state tablet or capsule, can only dissolve 20% after entering human body, additionally 80% the most digested part can cause get angry, abdominal distention, constipation, the side effect such as the toxin remains.

Embodiment 4

A kind of former dew of Rhizoma Polygonati, by the volatile material composition in Rhizoma Polygonati, water-soluble substances composition, and/or fat The extracting solution of soluble substance composition composition subset form.

Preferably, the described hexagonal structure of subset form.

Preferably, described former dew be configured to water preparation, granule, bagged steeping drug, syrup, capsule or Tablet.

The preparation method of the former dew of a kind of Rhizoma Polygonati, it is characterised in that including:

A) at a certain temperature, the volatile material using out-phase liquid ultramicrotechnique to extract in Rhizoma Polygonati becomes Part, water-soluble substances composition, and/or liposoluble substance composition;

B) product of step A is carried out homogeneous polymerization, to prepare former dew.

Described out-phase liquid ultramicrotechnique includes that moment produces vacuum and allows the most expanded step of described material Suddenly.Specifically, including the first stage, in vacuum chamber, central authorities' container perimeter is placed material and enters Row heating;Second stage, moment generation vacuum, the material making needs extract is the most expanded;3rd rank Section, forms low temperature on center vessel top, and the environment of high temperature is formed at bottom, to form convection current;Fourth order Section, discharges stock solution by hight atmospheric molecular motion;In 5th stage, stock solution is slowly drawn out of, in being pooled to Centre container.

Preferably, the mode of heating of employing has infrared heating, microwave heating etc., and the heat provided was both Quickly to make material expanded, material surface can not be made again to sustain damage.

Preferably, by heating, material internal moisture is constantly evaporated, made the pore of material by vacuum Open, the air of the pore in material is extracted out simultaneously, make material internal moisture flash distillation, cause material Surface is formed uniformly, alveolate texture.

Preferably, the temperature of described step A is at 45~250 DEG C.

Preferably, the device of described out-phase liquid ultramicrotechnique includes vacuum chamber, sets at internal vacuum chamber Putting center vessel, material is placed in vacuum chamber, is on heating plate, in the particular embodiment, and profit By Far-infrared Heating, it is ensured that uniform drying, the temperature of heating plate is accurately controlled by heating curves.

Preferably, the top of vacuum chamber is provided with heat sink, such as fan so that material is in heating During, low temperature is formed on center vessel top, the environment of high temperature is formed at bottom, to form molecular motion Convection current.

Preferably, being moved by hight atmospheric molecular, stock solution is slowly drawn out of, the volatile material in material Composition, water-soluble substances composition, and/or liposoluble substance composition carry out homogeneous polymerization, are pooled to central authorities' appearance Device, it is achieved whole part extracts, to form the extracting solution of subset form.

Preferably, described former dew is the extracting solution of subset form, and subset form is hexagonal Structure.In human body cell, the structure of institute's water content is mainly hexagonal annular structure, so former dew and human body Cell most affinity, also most beneficial for health.

Preferably, the magnetic resonance detection index of the extracting solution of described subset form is 46~70Hz.

The present embodiment is to provide described former being exposed at of Rhizoma Polygonati to prepare food, answering in daily use chemicals product and health product With.

Test

Subset diameter about 0.5 nanometer extracted, and the cell wall conduit aperture of human body is 2 nanometers, After drinking, directly can not enter blood by cells of vascular wall film by digestive system, penetrate arrival Pathogen, can supplement rapidly human nutrition and energy in one second, rapidly can be by shrivelled erythrocyte Activate, be obviously enhanced human metabolism's level, accelerate active nutritional material and directly effectively absorbed by human body, Absorbance is up to 99%.

Subset liquid is extremely continual and steady, and antioxidation is strong, the most still presents small point Sub-bulk state, the shelf-life is longer, after the former dew of the present invention enters human body, it is not necessary to dissolve, directly by the intestines and stomach Overall absorption, in contrast to common solid-state tablet or capsule, can only dissolve 20% after entering human body, additionally 80% the most digested part can cause get angry, abdominal distention, constipation, the side effect such as the toxin remains.

Embodiment 5

A kind of former dew of Fructus Arctii, by the volatile material composition in Fructus Arctii, water-soluble substances composition, and/or fat The extracting solution of soluble substance composition composition subset form.

Preferably, the described hexagonal structure of subset form.

Preferably, described former dew be configured to water preparation, granule, bagged steeping drug, syrup, capsule or Tablet.

The preparation method of the former dew of a kind of Fructus Arctii, it is characterised in that including:

A) at a certain temperature, the volatile material using out-phase liquid ultramicrotechnique to extract in Fructus Arctii becomes Part, water-soluble substances composition, and/or liposoluble substance composition;

B) product of step A is carried out homogeneous polymerization, to prepare former dew.

Described out-phase liquid ultramicrotechnique includes that moment produces vacuum and allows the most expanded step of described material Suddenly.Specifically, including the first stage, in vacuum chamber, central authorities' container perimeter is placed material and enters Row heating;Second stage, moment generation vacuum, the material making needs extract is the most expanded;3rd rank Section, forms low temperature on center vessel top, and the environment of high temperature is formed at bottom, to form convection current;Fourth order Section, discharges stock solution by hight atmospheric molecular motion;In 5th stage, stock solution is slowly drawn out of, in being pooled to Centre container.

Preferably, the mode of heating of employing has infrared heating, microwave heating etc., and the heat provided was both Quickly to make material expanded, material surface can not be made again to sustain damage.

Preferably, by heating, material internal moisture is constantly evaporated, made the pore of material by vacuum Open, the air of the pore in material is extracted out simultaneously, make material internal moisture flash distillation, cause material Surface is formed uniformly, alveolate texture.

Preferably, the temperature of described step A is at 45~250 DEG C.

Preferably, the device of described out-phase liquid ultramicrotechnique includes vacuum chamber, sets at internal vacuum chamber Putting center vessel, material is placed in vacuum chamber, is on heating plate, in the particular embodiment, and profit By Far-infrared Heating, it is ensured that uniform drying, the temperature of heating plate is accurately controlled by heating curves.

Preferably, the top of vacuum chamber is provided with heat sink, such as fan so that material is in heating During, low temperature is formed on center vessel top, the environment of high temperature is formed at bottom, to form molecular motion Convection current.

Preferably, being moved by hight atmospheric molecular, stock solution is slowly drawn out of, the volatile material in material Composition, water-soluble substances composition, and/or liposoluble substance composition carry out homogeneous polymerization, are pooled to central authorities' appearance Device, it is achieved whole part extracts, to form the extracting solution of subset form.

Preferably, described former dew is the extracting solution of subset form, and subset form is hexagonal Structure.In human body cell, the structure of institute's water content is mainly hexagonal annular structure, so former dew and human body Cell most affinity, also most beneficial for health.

Preferably, the magnetic resonance detection index of the extracting solution of described subset form is 46~70Hz.

The present embodiment is to provide described former being exposed at of Fructus Arctii to prepare food, answering in daily use chemicals product and health product With.

Test

Subset diameter about 0.5 nanometer extracted, and the cell wall conduit aperture of human body is 2 nanometers, After drinking, directly can not enter blood by cells of vascular wall film by digestive system, penetrate arrival Pathogen, can supplement rapidly human nutrition and energy in one second, rapidly can be by shrivelled erythrocyte Activate, be obviously enhanced human metabolism's level, accelerate active nutritional material and directly effectively absorbed by human body, Absorbance is up to 99%.

Subset liquid is extremely continual and steady, and antioxidation is strong, the most still presents small point Sub-bulk state, the shelf-life is longer, after the former dew of the present invention enters human body, it is not necessary to dissolve, directly by the intestines and stomach Overall absorption, in contrast to common solid-state tablet or capsule, can only dissolve 20% after entering human body, additionally 80% the most digested part can cause get angry, abdominal distention, constipation, the side effect such as the toxin remains.

Embodiment 6

A kind of former dew of Rhizoma Zingiberis Recens, by the volatile material composition in Rhizoma Zingiberis Recens, water-soluble substances composition, and/or fat The extracting solution of soluble substance composition composition subset form.

Preferably, the described hexagonal structure of subset form.

Preferably, described former dew be configured to water preparation, granule, bagged steeping drug, syrup, capsule or Tablet.

The preparation method of the former dew of a kind of Rhizoma Zingiberis Recens, it is characterised in that including:

A) at a certain temperature, the volatile material using out-phase liquid ultramicrotechnique to extract in Rhizoma Zingiberis Recens becomes Part, water-soluble substances composition, and/or liposoluble substance composition;

B) product of step A is carried out homogeneous polymerization, to prepare former dew.

Described out-phase liquid ultramicrotechnique includes that moment produces vacuum and allows the most expanded step of described material Suddenly.Specifically, including the first stage, in vacuum chamber, central authorities' container perimeter is placed material and enters Row heating;Second stage, moment generation vacuum, the material making needs extract is the most expanded;3rd rank Section, forms low temperature on center vessel top, and the environment of high temperature is formed at bottom, to form convection current;Fourth order Section, discharges stock solution by hight atmospheric molecular motion;In 5th stage, stock solution is slowly drawn out of, in being pooled to Centre container.

Preferably, the mode of heating of employing has infrared heating, microwave heating etc., and the heat provided was both Quickly to make material expanded, material surface can not be made again to sustain damage.

Preferably, by heating, material internal moisture is constantly evaporated, made the pore of material by vacuum Open, the air of the pore in material is extracted out simultaneously, make material internal moisture flash distillation, cause material Surface is formed uniformly, alveolate texture.

Preferably, the temperature of described step A is at 45~250 DEG C.

Preferably, the device of described out-phase liquid ultramicrotechnique includes vacuum chamber, sets at internal vacuum chamber Putting center vessel, material is placed in vacuum chamber, is on heating plate, in the particular embodiment, and profit By Far-infrared Heating, it is ensured that uniform drying, the temperature of heating plate is accurately controlled by heating curves.

Preferably, the top of vacuum chamber is provided with heat sink, such as fan so that material is in heating During, low temperature is formed on center vessel top, the environment of high temperature is formed at bottom, to form molecular motion Convection current.

Preferably, being moved by hight atmospheric molecular, stock solution is slowly drawn out of, the volatile material in material Composition, water-soluble substances composition, and/or liposoluble substance composition carry out homogeneous polymerization, are pooled to central authorities' appearance Device, it is achieved whole part extracts, to form the extracting solution of subset form.

Preferably, described former dew is the extracting solution of subset form, and subset form is hexagonal Structure.In human body cell, the structure of institute's water content is mainly hexagonal annular structure, so former dew and human body Cell most affinity, also most beneficial for health.

Preferably, the magnetic resonance detection index of the extracting solution of described subset form is 46~70Hz.

The present embodiment is to provide described former being exposed at of Rhizoma Zingiberis Recens to prepare food, answering in daily use chemicals product and health product With.

Test

Subset diameter about 0.5 nanometer extracted, and the cell wall conduit aperture of human body is 2 nanometers, After drinking, directly can not enter blood by cells of vascular wall film by digestive system, penetrate arrival Pathogen, can supplement rapidly human nutrition and energy in one second, rapidly can be by shrivelled erythrocyte Activate, be obviously enhanced human metabolism's level, accelerate active nutritional material and directly effectively absorbed by human body, Absorbance is up to 99%.

Subset liquid is extremely continual and steady, and antioxidation is strong, the most still presents small point Sub-bulk state, the shelf-life is longer, after the former dew of the present invention enters human body, it is not necessary to dissolve, directly by the intestines and stomach Overall absorption, in contrast to common solid-state tablet or capsule, can only dissolve 20% after entering human body, additionally 80% the most digested part can cause get angry, abdominal distention, constipation, the side effect such as the toxin remains.

Embodiment 7

A kind of former dew of Herba Dendrobii, by the volatile material composition in Herba Dendrobii, water-soluble substances composition, and/or fat The extracting solution of soluble substance composition composition subset form.

Preferably, the described hexagonal structure of subset form.

Preferably, described former dew be configured to water preparation, granule, bagged steeping drug, syrup, capsule or Tablet.

The preparation method of the former dew of a kind of Herba Dendrobii, it is characterised in that including:

A) at a certain temperature, the volatile material using out-phase liquid ultramicrotechnique to extract in Herba Dendrobii becomes Part, water-soluble substances composition, and/or liposoluble substance composition;

B) product of step A is carried out homogeneous polymerization, to prepare former dew.

Described out-phase liquid ultramicrotechnique includes that moment produces vacuum and allows the most expanded step of described material Suddenly.Specifically, including the first stage, in vacuum chamber, central authorities' container perimeter is placed material and enters Row heating;Second stage, moment generation vacuum, the material making needs extract is the most expanded;3rd rank Section, forms low temperature on center vessel top, and the environment of high temperature is formed at bottom, to form convection current;Fourth order Section, discharges stock solution by hight atmospheric molecular motion;In 5th stage, stock solution is slowly drawn out of, in being pooled to Centre container.

Preferably, the mode of heating of employing has infrared heating, microwave heating etc., and the heat provided was both Quickly to make material expanded, material surface can not be made again to sustain damage.

Preferably, by heating, material internal moisture is constantly evaporated, made the pore of material by vacuum Open, the air of the pore in material is extracted out simultaneously, make material internal moisture flash distillation, cause material Surface is formed uniformly, alveolate texture.

Preferably, the temperature of described step A is at 45~250 DEG C.

Preferably, the device of described out-phase liquid ultramicrotechnique includes vacuum chamber, sets at internal vacuum chamber Putting center vessel, material is placed in vacuum chamber, is on heating plate, in the particular embodiment, and profit By Far-infrared Heating, it is ensured that uniform drying, the temperature of heating plate is accurately controlled by heating curves.

Preferably, the top of vacuum chamber is provided with heat sink, such as fan so that material is in heating During, low temperature is formed on center vessel top, the environment of high temperature is formed at bottom, to form molecular motion Convection current.

Preferably, being moved by hight atmospheric molecular, stock solution is slowly drawn out of, the volatile material in material Composition, water-soluble substances composition, and/or liposoluble substance composition carry out homogeneous polymerization, are pooled to central authorities' appearance Device, it is achieved whole part extracts, to form the extracting solution of subset form.

Preferably, described former dew is the extracting solution of subset form, and subset form is hexagonal Structure.In human body cell, the structure of institute's water content is mainly hexagonal annular structure, so former dew and human body Cell most affinity, also most beneficial for health.

Preferably, the magnetic resonance detection index of the extracting solution of described subset form is 46~70Hz.

The present embodiment is to provide described former being exposed at of Herba Dendrobii to prepare food, answering in daily use chemicals product and health product With.

Test

Subset diameter about 0.5 nanometer extracted, and the cell wall conduit aperture of human body is 2 nanometers, After drinking, directly can not enter blood by cells of vascular wall film by digestive system, penetrate arrival Pathogen, can supplement rapidly human nutrition and energy in one second, rapidly can be by shrivelled erythrocyte Activate, be obviously enhanced human metabolism's level, accelerate active nutritional material and directly effectively absorbed by human body, Absorbance is up to 99%.

Subset liquid is extremely continual and steady, and antioxidation is strong, the most still presents small point Sub-bulk state, the shelf-life is longer, after the former dew of the present invention enters human body, it is not necessary to dissolve, directly by the intestines and stomach Overall absorption, in contrast to common solid-state tablet or capsule, can only dissolve 20% after entering human body, additionally 80% the most digested part can cause get angry, abdominal distention, constipation, the side effect such as the toxin remains.

Embodiment 8

The tuber materials that the present embodiment is selected is Bulbus Allii, step B of the preparation method of its former dew and enforcement Example 1 is identical, and the temperature of step A, at 45 DEG C, tests the nuclear-magnetism of the extracting solution of the subset form recorded Resonance detection index is 46.1Hz.

Embodiment 9

The tuber materials that the present embodiment is selected is Bulbus Allii, step B of the preparation method of its former dew and enforcement Example 1 is identical, and the temperature of step A, at 250 DEG C, tests the core of the extracting solution of the subset form recorded Magnetic resonance detection index is 69Hz.

Embodiment 10

The tuber materials that the present embodiment is selected is Poria, step B of the preparation method of its former dew and enforcement Example 2 is identical, and the temperature of step A, at 102 DEG C, tests the core of the extracting solution of the subset form recorded Magnetic resonance detection index is 57Hz.

Embodiment 11

The tuber materials that the present embodiment is selected is Poria, step B of the preparation method of its former dew and enforcement Example 2 is identical, and the temperature of step A, at 45 DEG C, tests the nuclear-magnetism of the extracting solution of the subset form recorded Resonance detection index is 48.1Hz.

Embodiment 12

The tuber materials that the present embodiment is selected is Poria, step B of the preparation method of its former dew and enforcement Example 2 is identical, and the temperature of step A, at 243 DEG C, tests the core of the extracting solution of the subset form recorded Magnetic resonance detection index is 65Hz.

Embodiment 13

The tuber materials that the present embodiment is selected is Maca, step B of the preparation method of its former dew and enforcement Example 3 is identical, and the temperature of step A, at 250 DEG C, tests the core of the extracting solution of the subset form recorded Magnetic resonance detection index is 70Hz.

Embodiment 14

The tuber materials that the present embodiment is selected is Maca, step B of the preparation method of its former dew and enforcement Example 3 is identical, and the temperature of step A, at 223 DEG C, tests the core of the extracting solution of the subset form recorded Magnetic resonance detection index is 55.1Hz.

Embodiment 15

The tuber materials that the present embodiment is selected is Maca, step B of the preparation method of its former dew and enforcement Example 3 is identical, and the temperature of step A, at 45 DEG C, tests the nuclear-magnetism of the extracting solution of the subset form recorded Resonance detection index is 46.9Hz.

Embodiment 16

The tuber materials that the present embodiment is selected is Rhizoma Polygonati, step B of the preparation method of its former dew and enforcement Example 4 is identical, and the temperature of step A, at 248 DEG C, tests the core of the extracting solution of the subset form recorded Magnetic resonance detection index is 63.1Hz.

Embodiment 17

The tuber materials that the present embodiment is selected is Rhizoma Polygonati, step B of the preparation method of its former dew and enforcement Example 4 is identical, and the temperature of step A, at 45 DEG C, tests the nuclear-magnetism of the extracting solution of the subset form recorded Resonance detection index is 47.1Hz.

Embodiment 18

The tuber materials that the present embodiment is selected is Rhizoma Polygonati, step B of the preparation method of its former dew and enforcement Example 4 is identical, and the temperature of step A, at 250 DEG C, tests the core of the extracting solution of the subset form recorded Magnetic resonance detection index is 65Hz.

Embodiment 19

The tuber materials that the present embodiment is selected is Fructus Arctii, step B of the preparation method of its former dew and enforcement Example 5 is identical, and the temperature of step A, at 210 DEG C, tests the core of the extracting solution of the subset form recorded Magnetic resonance detection index is 55Hz.

Embodiment 20

The tuber materials that the present embodiment is selected is Fructus Arctii, step B of the preparation method of its former dew and enforcement Example 5 is identical, and the temperature of step A, at 45 DEG C, tests the nuclear-magnetism of the extracting solution of the subset form recorded Resonance detection index is 46.1Hz.

Embodiment 21

The tuber materials that the present embodiment is selected is Fructus Arctii, step B of the preparation method of its former dew and enforcement Example 5 is identical, and the temperature of step A, at 50 DEG C, tests the nuclear-magnetism of the extracting solution of the subset form recorded Resonance detection index is 62Hz.

Embodiment 22

The tuber materials that the present embodiment is selected is Rhizoma Zingiberis Recens, step B of the preparation method of its former dew and enforcement Example 6 is identical, and the temperature of step A, at 250 DEG C, tests the core of the extracting solution of the subset form recorded Magnetic resonance detection index is 67Hz.

Embodiment 23

The tuber materials that the present embodiment is selected is Rhizoma Zingiberis Recens, step B of the preparation method of its former dew and enforcement Example 6 is identical, and the temperature of step A, at 45 DEG C, tests the nuclear-magnetism of the extracting solution of the subset form recorded Resonance detection index is 46.2Hz.

The invention have the benefit that

First, the herbal stock solution of extraction is subset liquid, remains the original composition proportion of plant, Make the characteristics such as the full and uniform polymerization of out-phase liquid and activation so that plant can enter human body quickly with liquid Absorbed, penetrated into intracellular, strengthen rapidly human metabolism's level, accelerate active nutritional thing in former dew Matter is absorbed by the body, and absorbance is up to 99%.Alleviate metabolic disease, promote growth.

Second, it is possible to strand group is broken up and makes the former dew being more easy to absorb, it is applied to book on Chinese herbal medicine beauty treatment, day Change product, special dietary seafood, seasoning dew, former alcoholic drink mixed with fruit juice, book on Chinese herbal medicine function product, health product, cmm of simple prescription, Chinese medicine Compound recipe.

3rd, NMR value average 49~60HZ, the molecular chain length convergence making out-phase liquid is identical, promotees Enter the abundant of out-phase liquid being originally difficult to merge to be polymerized, form the former dew of small micel, improve former dew and gather The uniformity of conjunction, stability, antitypy, give full play to the effect of all kinds of oxidant, the antioxygen on Shi Yuan road Change performance to significantly improve.

Described above illustrate and describes some preferred embodiments of the application, but as previously mentioned, it should reason Solve the application and be not limited to form disclosed herein, be not to be taken as the eliminating to other embodiments, And can be used for various other combination, amendment and environment, and can in application contemplated scope described herein, It is modified by above-mentioned teaching or the technology of association area or knowledge.And those skilled in the art are carried out changes Move and change is without departing from spirit and scope, the most all should be in the protection of the application claims In the range of.

Claims (2)

1. the preparation method of the former dew of tuberous plant, it is characterised in that including:
A) at a certain temperature, out-phase liquid ultramicrotechnique is used to extract the volatile material composition in plant, Water-soluble substances composition, and/or liposoluble substance composition;
Described out-phase liquid ultramicrotechnique includes: the first stage, in vacuum chamber, to center vessel week Limit is placed material and is heated;Second stage, moment generation vacuum, make the material quilt completely that needs extract Expanded;Phase III, forming low temperature on center vessel top, the environment of high temperature is formed at bottom, to be formed Convection current;Fourth stage, discharges stock solution by hight atmospheric molecular motion;In 5th stage, stock solution is slowly taken out Go out, be pooled to center vessel;
B) product of step A is carried out homogeneous polymerization, to prepare former dew;
The device of described out-phase liquid ultramicrotechnique includes vacuum chamber, arranges central authorities' appearance at internal vacuum chamber Device, material is placed in vacuum chamber, is on heating plate, and the top of vacuum chamber is provided with heat sink, Making material during heating, form low temperature on center vessel top, the environment of high temperature is formed at bottom, To form the convection current of molecular motion.
Preparation method the most according to claim 1, it is characterised in that described former dew is little molecule The extracting solution of glob state, the magnetic resonance detection index of the extracting solution of described subset form is 46~70Hz.
CN201410429253.0A 2014-08-27 2014-08-27 A kind of former dew of tuberous plant, preparation method and application CN104222888B (en)

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CN105169726A (en) * 2015-09-02 2015-12-23 陈�峰 Heterogeneous and synchronous ultramicro original liquid extraction method and apparatus thereof
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CN107189921A (en) * 2017-07-26 2017-09-22 金湘范 A kind of white spirit based on plant former dew and preparation method thereof
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